CN209612960U - A kind of Chemical Manufacture mixed reactor - Google Patents

A kind of Chemical Manufacture mixed reactor Download PDF

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Publication number
CN209612960U
CN209612960U CN201920217194.9U CN201920217194U CN209612960U CN 209612960 U CN209612960 U CN 209612960U CN 201920217194 U CN201920217194 U CN 201920217194U CN 209612960 U CN209612960 U CN 209612960U
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China
Prior art keywords
stirring
autoclave body
liquid
liquid storage
chemical manufacture
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Application number
CN201920217194.9U
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Chinese (zh)
Inventor
何诚亮
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Yibin Jintong Chemical Technology Co Ltd
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Yibin Jintong Chemical Technology Co Ltd
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Abstract

The utility model relates to chemical production fields, specifically disclose a kind of Chemical Manufacture mixed reactor, including autoclave body, and the upper lumen of the autoclave body is equipped at least two liquid storage chambers;The lower lumen of the autoclave body is equipped with stirring bar assembly;At least two liquid outlets are offered on the bottom plate of each liquid storage chamber, and the adjustable putty mechanism blocked for the liquid outlet to its bottom is provided in each described liquid storage chamber.The utility model can adjust the rate that feed liquid is discharged by liquid outlet in liquid storage chamber by adjustable putty mechanism, feed liquid is added in autoclave body lower lumen so that realization is controllable, feed liquid is slowly gradually added into autoclave body, the reactivity between differential responses feed liquid can be improved, and in the stirring bar assembly of the utility model, by the agitating auger paddle that is arranged on stirring shaft, inclination stirring mobile jib, inclination stirring strut and arc stirring rod, enable to reaction solution in autoclave body lower lumen is sufficiently mixed reaction.

Description

A kind of Chemical Manufacture mixed reactor
Technical field
The utility model relates to chemical production field, specifically a kind of Chemical Manufacture mixed reactor.
Background technique
The broad understanding of reaction kettle has the container physically or chemically reacted, is designed by the structure to container and is matched with parameter Set, realize heating, evaporation that technique requires, the mixed function of cooling and low high speed, reaction kettle be widely used in petroleum, chemical industry, Rubber, pesticide, dyestuff, medicine, food, for completing the appearance of the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation Device.
Existing reaction kettle when carrying out hybrid reaction, usually by different chemical industry feed liquids simultaneously be poured into anti-autoclave body into Row reaction, a large amount of chemical industry feed liquid are poured into reaction chamber simultaneously, be easy to cause between chemical industry feed liquid and react insufficient.
In addition, agitating device can generally be arranged in reaction kettle in order to accelerate reaction speed, chemical industry feed liquid is made by stirring What is mixed is more uniform, to accelerate reaction rate.Traditional chemical reaction kettle is typically all that individual blade is leaned on to be stirred, Mixing efficiency is lower, declines so as to cause the reaction rate of raw material.
Utility model content
The purpose of this utility model is to provide a kind of Chemical Manufacture mixed reactors, to solve in above-mentioned background technique The problem of proposition.
To achieve the above object, the utility model provides the following technical solutions:
The upper lumen of a kind of Chemical Manufacture mixed reactor, including autoclave body, the autoclave body is equipped at least two liquid storages Chamber;The lower lumen of the autoclave body is equipped with stirring bar assembly;It is equipped with above the top plate of the autoclave body for driving the stirring The driving motor of bar assembly rotation;At least two liquid outlets, and each are offered on the bottom plate of each liquid storage chamber The adjustable putty mechanism blocked for the liquid outlet to its bottom is provided in the liquid storage chamber;
The adjustable putty mechanism includes rotating the screw rod being set in liquid storage chamber and being connected through a screw thread mode to be set in Lifting swivel nut on screw rod, the top of the screw rod is placed in the tip exterior of autoclave body, and the top of the screw rod is fixedly installed with Operation handle;The lifting swivel nut is fixedly mounted on elevating lever, and the bottom of the elevating lever is fixedly installed with vertical supporting rod, with The putty plug that the liquid outlet matches is fixedly mounted on the bottom end of vertical supporting rod.
As a further solution of the present invention: the trapezoidal knot in the section of mutually matched liquid outlet and putty plug Structure.
As a further solution of the present invention: being provided at the top of the autoclave body multiple one-to-one with liquid storage chamber Feeding port, and the equal open-close type in top of each feeding port is equipped with protective cover, after opening protective cover, it is convenient by feeding port to Feed liquid is added in liquid storage chamber.
As a further solution of the present invention: the lower lumen bottom of the autoclave body is provided with drainage conduit, drainage conduit On blow-off valve is installed, after opening blow-off valve, the product solution that hybrid reaction is completed in autoclave body passes through drainage conduit discharge.
As a further solution of the present invention: the stirring bar assembly include along the autoclave body central axes rotation set The stirring shaft set is disposed with agitating auger paddle from top to bottom on the stirring shaft of the autoclave body lower part, inclination is stirred Mix mobile jib and arc stirring rod.
As a further solution of the present invention: the agitating auger paddle setting in up-narrow and down-wide helicoidal structure is being stirred Mix the surface of shaft;The other end bottom of the inclination stirring mobile jib is fixedly installed inclination stirring strut.
As a further solution of the present invention: the arc stirring rod is fixedly mounted on the bottom end of stirring shaft, and The other end of the arc stirring rod is parallel to each other with the stirring shaft, and the other end of the arc stirring rod is located at inclination Stir the outside of strut.
Compared with prior art, the utility model has the beneficial effects that
The utility model is provided in Chemical Manufacture mixed reactor, can be adjusted in liquid storage chamber by adjustable putty mechanism The rate that feed liquid is discharged by liquid outlet, with realize it is controllable feed liquid is added in autoclave body lower lumen, feed liquid is slowly gradually It is added in autoclave body, the reactivity between differential responses feed liquid can be improved, and the discharge velocity of different feed liquid is individually controllable, flexibly Property is good;
In addition, the driving motor used the power on drives in Chemical Manufacture mixed reactor provided by the utility model Stir bar assembly rotation, wherein by the agitating auger paddle that is arranged on stirring shaft, inclination stirring mobile jib, inclination stirring strut and Arc stirring rod substantially increases the reaction of material in autoclave body so that reaction solution is sufficiently mixed reaction in autoclave body lower lumen Rate.
Detailed description of the invention
It, below will be to embodiment or the prior art in order to illustrate more clearly of the technical scheme in the embodiment of the utility model Attached drawing needed in description is briefly described, it should be apparent that, the accompanying drawings in the following description is only that this is practical new Some embodiments of type.
Fig. 1 is the structural schematic diagram of the utility model Chemical Manufacture mixed reactor.
Fig. 2 is the enlarged structure schematic diagram of part A in Fig. 1.
In figure: 1- autoclave body, 2- supporting leg, 3- feeding port, 4- driving motor, 5- protective cover, 6- liquid storage chamber, 7- screw rod, 8- Elevating lever, 9- stirring shaft, 10- agitating auger paddle, 11- inclination stirring mobile jib, 12- inclination stirring strut, the stirring of 13- arc Bar, 14- drainage conduit, 15- blow-off valve, 16- go up and down swivel nut, 17- vertical supporting rod, 18- liquid outlet, 19- putty plug, 20- manipulator Handle.
Specific embodiment
In order to which technical problem to be solved in the utility model, technical solution and beneficial effect is more clearly understood, with Lower combination accompanying drawings and embodiments, the present invention will be further described in detail.It should be appreciated that specific reality described herein It applies example to be only used to explain the utility model, is not used to limit the utility model.
As shown in Figure 1, in one embodiment provided by the utility model, a kind of Chemical Manufacture mixed reactor, including The upper lumen of autoclave body 1, the autoclave body 1 is equipped at least two liquid storage chambers 6;The lower lumen of the autoclave body 1 is equipped with stirring rod group Part;Driving motor 4 for driving the stirring bar assembly to rotate is installed above the top plate of the autoclave body 1;Further, institute State the supporting leg 2 for being fixedly installed and playing a supportive role on the bottom four corners outer wall of autoclave body 1.
Further, in the utility model embodiment, the top of the autoclave body 1 is provided with multiple and liquid storage chamber 6 one by one Corresponding feeding port 3, and the equal open-close type in top of each feeding port 3 is equipped with protective cover 5, it is convenient logical after opening protective cover 5 It crosses feeding port 3 and adds feed liquid into liquid storage chamber 6;The lower lumen bottom of the autoclave body 1 is provided with drainage conduit 14, in drainage conduit 14 Blow-off valve 15 is installed, after opening blow-off valve 15, the product solution that hybrid reaction is completed in autoclave body 1 is discharged by drainage conduit 14.
Specifically, being opened up on the bottom plate of each liquid storage chamber 6 in one embodiment provided by the utility model There are at least two liquid outlets 18, and is provided in each described liquid storage chamber 6 and is sealed for the liquid outlet 18 to its bottom Stifled adjustable putty mechanism can adjust feed liquid in liquid storage chamber 6 by adjustable putty mechanism and pass through the rate that liquid outlet 18 is discharged, Feed liquid is added in 1 lower lumen of autoclave body so that realization is controllable, feed liquid is slowly gradually added into autoclave body 1, can be improved different anti- The reactivity between feed liquid is answered, and the discharge velocity of different feed liquid is individually controllable, flexibility is good.
Please continue to refer to Fig. 1, in another embodiment provided by the utility model, the stirring bar assembly includes along institute The stirring shaft 9 of rotation setting in central axes in autoclave body 1 is stated, on the stirring shaft 9 of 1 lower part of autoclave body from top to bottom successively It is provided with agitating auger paddle 10, inclination stirring mobile jib 11 and arc stirring rod 13, wherein in up-narrow and down-wide helicoidal structure The surface of stirring shaft 9 is arranged in agitating auger paddle 10;The other end bottom of the inclination stirring mobile jib 11, which is fixedly installed, inclines Tiltedly stirring strut 12;The arc stirring rod 13 is fixedly mounted on the bottom end of stirring shaft 9, and the arc stirring rod 13 is another One end is parallel to each other with the stirring shaft 9, and the other end of the arc stirring rod 13 is located at the outer of inclination stirring strut 12 Side.
In the present embodiment, pass through shaft coupling between the output shaft of the driving motor 4 and the top of the stirring shaft 9 It is drivingly connected, the driving stirring bar assembly rotation of driving motor 4 of energization, wherein passing through the agitating auger being arranged on stirring shaft 9 Paddle 10, inclination stirring mobile jib 11, inclination stirring strut 12 and arc stirring rod 13, so that reaction solution in 1 lower lumen of autoclave body It is sufficiently mixed reaction, substantially increases the reaction rate of material in autoclave body 1.
As shown in Fig. 1~2, in another embodiment provided by the utility model, the adjustable putty mechanism includes turning It moves the screw rod 7 in liquid storage chamber 6 and is connected through a screw thread the lifting swivel nut 16 that mode is set on screw rod 7, the screw rod 7 Top be placed in the tip exterior of autoclave body 1, and the top of the screw rod 7 is fixedly installed with operation handle 20;The lifting swivel nut 16 are fixedly mounted on elevating lever 8, and the bottom of the elevating lever 8 is fixedly installed with vertical supporting rod 17, with 18 phase of liquid outlet The putty plug 19 of cooperation is fixedly mounted on the bottom end of vertical supporting rod 17, rotates screw rod 7 by operating operation handle 20, according to silk The direction of rotation of bar 7 can adjust the height of lifting swivel nut 16, and then adjust the height of putty plug 19.
In the utility model embodiment, the trapezoidal structure in the section of mutually matched liquid outlet 18 and putty plug 19, The position in liquid outlet 18 of putty plug 19 is adjusted, can be realized the adjusting to load in 18 unit time of liquid outlet, by can It adjusts putty mechanism to be gradually added into feed liquid slowly in autoclave body 1, the reactivity between differential responses feed liquid can be improved.
The electric elements occurred in this article are electrically connected with extraneous main controller and 220V alternating current, and main controller can be meter Calculation machine etc. plays the conventionally known equipment of control.
In the description of the present invention, unless otherwise clearly defined and limited, term " installation ", " connected ", " company Connect " it shall be understood in a broad sense, for example, it may be being fixedly connected, it may be a detachable connection, or be integrally connected;It can be machine Tool connection, is also possible to be electrically connected;It can be directly connected, two members can also be can be indirectly connected through an intermediary Connection inside part.For the ordinary skill in the art, it can understand that above-mentioned term is practical new at this with concrete condition Concrete meaning in type.
The above is only the preferred embodiment of the utility model only, is not intended to limit the utility model, all at this Made any modifications, equivalent replacements, and improvements etc., should be included in the utility model within the spirit and principle of utility model Protection scope within.

Claims (7)

1. a kind of Chemical Manufacture mixed reactor, including autoclave body (1), which is characterized in that the upper lumen of the autoclave body (1) is set There are at least two liquid storage chambers (6);The lower lumen of the autoclave body (1) is equipped with stirring bar assembly;Above the top plate of the autoclave body (1) Driving motor (4) for driving the stirring bar assembly to rotate is installed;It is opened on the bottom plate of each liquid storage chamber (6) It is provided with equipped at least two liquid outlets (18), and in each described liquid storage chamber (6) for the liquid outlet to its bottom (18) the adjustable putty mechanism blocked;
The adjustable putty mechanism includes rotating the screw rod (7) being set in liquid storage chamber (6) and being connected through a screw thread mode to be arranged The top of lifting swivel nut (16) on screw rod (7), the screw rod (7) is placed in the tip exterior of autoclave body (1), and the screw rod (7) top is fixedly installed with operation handle (20);The lifting swivel nut (16) is fixedly mounted on elevating lever (8), the liter The bottom of drop bar (8) is fixedly installed with vertical supporting rod (17), the fixed peace of the putty plug (19) matched with the liquid outlet (18) Mounted in the bottom end of vertical supporting rod (17).
2. Chemical Manufacture mixed reactor according to claim 1, which is characterized in that mutually matched liquid outlet (18) With the trapezoidal structure in section of putty plug (19).
3. Chemical Manufacture mixed reactor according to claim 1, which is characterized in that set at the top of the autoclave body (1) It is equipped with multiple and liquid storage chamber (6) one-to-one feeding port (3), and the equal open-close type in top of each feeding port (3) is equipped with Protective cover (5).
4. Chemical Manufacture mixed reactor according to claim 3, which is characterized in that in the lower part of the autoclave body (1) Bottom of chamber portion is provided with drainage conduit (14), and blow-off valve (15) are equipped in drainage conduit (14).
5. Chemical Manufacture mixed reactor according to any one of claims 1 to 4, which is characterized in that the stirring rod group Part includes the stirring shaft (9) along the interior central axes rotation setting of the autoclave body (1), and the stirring for being located at the autoclave body (1) lower part turns Agitating auger paddle (10), inclination stirring mobile jib (11) and arc stirring rod (13) are disposed on axis (9) from top to bottom.
6. Chemical Manufacture mixed reactor according to claim 5, which is characterized in that in up-narrow and down-wide helical form knot Surface of agitating auger paddle (10) setting of structure in stirring shaft (9);The other end bottom of inclination stirring mobile jib (11) is solid Surely it is provided with inclination stirring strut (12).
7. Chemical Manufacture mixed reactor according to claim 6, which is characterized in that the arc stirring rod (13) is solid Dingan County is mounted in the bottom end of stirring shaft (9), and the other end of the arc stirring rod (13) and the stirring shaft (9) are mutually flat Row, and the other end of the arc stirring rod (13) is located at the outside of inclination stirring strut (12).
CN201920217194.9U 2019-02-20 2019-02-20 A kind of Chemical Manufacture mixed reactor Active CN209612960U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201920217194.9U CN209612960U (en) 2019-02-20 2019-02-20 A kind of Chemical Manufacture mixed reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201920217194.9U CN209612960U (en) 2019-02-20 2019-02-20 A kind of Chemical Manufacture mixed reactor

Publications (1)

Publication Number Publication Date
CN209612960U true CN209612960U (en) 2019-11-12

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Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117551875A (en) * 2023-10-07 2024-02-13 山东彩客新材料有限公司 Lithium iron phosphate battery powder recycling and leaching device and application method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117551875A (en) * 2023-10-07 2024-02-13 山东彩客新材料有限公司 Lithium iron phosphate battery powder recycling and leaching device and application method thereof
CN117551875B (en) * 2023-10-07 2024-05-07 山东彩客新材料有限公司 Lithium iron phosphate battery powder recycling and leaching device and application method thereof

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