CN209548895U - A kind of methyl esters removes glycerol device - Google Patents
A kind of methyl esters removes glycerol device Download PDFInfo
- Publication number
- CN209548895U CN209548895U CN201920093235.8U CN201920093235U CN209548895U CN 209548895 U CN209548895 U CN 209548895U CN 201920093235 U CN201920093235 U CN 201920093235U CN 209548895 U CN209548895 U CN 209548895U
- Authority
- CN
- China
- Prior art keywords
- filter
- methyl esters
- knockout drum
- plate
- glycerol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 title claims abstract description 90
- 150000004702 methyl esters Chemical class 0.000 title claims abstract description 28
- 235000019387 fatty acid methyl ester Nutrition 0.000 claims abstract description 8
- 239000000706 filtrate Substances 0.000 claims abstract description 8
- 238000001125 extrusion Methods 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims 1
- 239000000440 bentonite Substances 0.000 abstract description 22
- 229910000278 bentonite Inorganic materials 0.000 abstract description 22
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 abstract description 22
- 238000001179 sorption measurement Methods 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 5
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 235000015895 biscuits Nutrition 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 230000010148 water-pollination Effects 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
Abstract
The utility model discloses a kind of methyl esters to remove glycerol device, including knockout drum and filter press, the upper cover of knockout drum is equipped with the feed inlet for glycerinated fatty acid methyl ester solution to be added and for bentonitic plus Tu Kou to be added, the tank base of knockout drum is equipped with discharge port, discharge port is equipped with discharge nozzle and is connected with filter press, the lower section of knockout drum is equipped with air pump, and the bottom in knockout drum is equipped with gas outlet, is connected with air pump；Filter press is plate and frame type filter-press, is made of multilayer fixed plate, filter frame, filter plate, pressure plate and extrusion pump, and filter plate lower end is equipped with the duct being discharged for filtrate, and the filtrate of each piece of filter plate is converged outside a liquid outlet pipe discharge machine.The utility model is isolated methyl esters and bentonite with plate and frame type filter-press, complete machine high degree of automation using the glycerol in bentonite adsorption methyl esters, using bentonite adsorption glycerol, removal effect is good, can completely remove the glycerol in methyl esters, and high production efficiency.
Description
Technical field
The utility model relates to fine chemistry industry production fields more particularly to a kind of methyl esters to remove glycerol device.
Background technique
Natural oil and methanol react under the action of catalyst generates fatty acid methyl ester, obtained fatty acid methyl ester
In contain glycerol, pure fatty acid methyl ester in order to obtain, it is necessary to separate glycerol, existing is to utilize methyl esters and glycerol
Specific gravity is different and intersolubility is little, is separated methyl esters and glycerol using settling methods, but this separation method is only capable of point
From a part of glycerol, the glycerol in methyl esters can not be removed completely, and settle waiting for a long time, low separation efficiency.
Utility model content
The purpose of the utility model is to provide a kind of methyl esters to remove glycerol device, can thoroughly remove glycerol from methyl esters, point
From high-efficient.
The technical issues of the utility model is solved can be realized using following technical scheme:
A kind of methyl esters removes glycerol device, it is characterized in that: including knockout drum and filter press, the upper cover of the knockout drum, which is equipped with, to be used
In the feed inlet that glycerinated fatty acid methyl ester solution is added and for bentonitic plus Tu Kou, the tank body of the knockout drum to be added
Bottom is equipped with discharge port, and the discharge port is equipped with discharge nozzle and is connected with filter press, and the lower section of the knockout drum is equipped with air pump, described
Bottom in knockout drum is equipped with gas outlet, is connected with air pump；The filter press is plate and frame type filter-press, by multilayer fixed plate, filter
Frame, filter plate, pressure plate and extrusion pump composition, filter plate lower end are equipped with the duct that is discharged for filtrate, the filtrate of each piece of filter plate converge from
Outside one liquid outlet pipe discharge machine.
Preferably, the lower section of the filter press be equipped with disintegrating machine, the disintegrating machine include material-falling hopper, smash stick, strainer and
Collecting bag, the material-falling hopper are docked with filter press, and the stick that smashes is arranged in the lower exit of material-falling hopper, the smashings stick at
Enclose more horizontally disposed cross bars, it is agitating shaft in the middle part of the more cross bars that cross bar is parallel with material-falling hopper long side, the cross bar with
There is connecting rod to be connected between agitating shaft, the agitating shaft is connected with external stirring motor, and the lower section for smashing stick is equipped with strainer, institute
Stating strainer is arc-shaped, and lower section is collecting bag.
Preferably, described plus Tu Kou is also connected with a feeder, and the feeder includes flood dragon and flood dragon motor.
Preferably, the tube wall of the flood dragon is equipped with inflatable mouth, is connected with air pump.
The utility model is divided methyl esters and bentonite using the glycerol in bentonite adsorption methyl esters, and with plate and frame type filter-press
It separates out, complete machine high degree of automation, using bentonite adsorption glycerol, removal effect is good, can completely remove the glycerol in methyl esters
It removes, and high production efficiency.
Detailed description of the invention
Fig. 1 is the overall structure diagram of the utility model.
Fig. 2 is the schematic diagram of internal structure of disintegrating machine 3
In figure, 1 knockout drum, 2 filter presses, 3 disintegrating machines, 4 feeders, 11 feed inlets, 12 plus Tu Kou, 13 discharge ports, 14 gas
Pump, 15 gas outlets, 31 material-falling hoppers, 32 smash stick, 33 strainers, 34 collecting bags, 41 flood dragons, 42 flood dragon motors, 43 inflatable mouths.
Specific embodiment
The utility model is described in detail below in conjunction with drawings and the specific embodiments, but the embodiments of the present invention
It is without being limited thereto.
Fig. 1,2 be the utility model preferred embodiment, including knockout drum 1, filter press 2, disintegrating machine 3 and feeder 4；
Knockout drum 1 is that bentonite is mixed to the mixing tank for carrying out glycerol removal with fatty acid methyl ester, and bentonite has good
Hydrophily, can quick adsorption glycerol, but do not dissolve in methyl esters, after bentonite adsorption glycerol, suspend in methyl ester liquid.
The upper cover of knockout drum 1 is equipped with swollen for the feed inlet 11 of glycerinated fatty acid methyl ester solution to be added and for being added
Profit soil plus native mouth 12, tank base are equipped with discharge port 13, after glycerinated methyl esters is added in tank by feed inlet 11, then pass through
Add native mouth 12 that bentonite is added, bentonite can adsorb glycerol in dropping process, to guarantee that absorption thoroughly, it is mixed to need to stir increasing
It closes, agitating mode, which can be, is arranged poking bar in knockout drum 1, drives Stirring by external motor, or stirring up and down
Mode, air pump 14 is arranged by the way of flow rotation stirring, in the lower section of knockout drum 1 in the present embodiment, the bottom in knockout drum 1
Portion is equipped with gas outlet 15, is connected with air pump 14, and air pump 14 is blown by gas outlet 15 into knockout drum 1, and gas is generated in knockout drum 1
Stream, is stirred methyl ester solution and bentonite in swirling recirculation flow, bentonite is dispersed in whipping process, enables glycerol
Thoroughly it is adsorbed.After stirring stops, having adsorbed the bentonite of glycerol in methyl esters in suspension, opened discharge port 13, methyl esters with
Bentonite suspension is flowed out from discharge port 13.
Discharge port 13 is equipped with discharge nozzle and is connected with filter press 2, and filter press 2 is plate and frame type filter-press, by multilayer fixed plate, filter
Frame, filter plate, pressure plate and extrusion pump composition, pressure plate are connected with extrusion pump, are pressed by extrusion pump and squeeze out methyl esters, methyl esters liquid
It is undercurrent that mode, which is discharged, in body, i.e., filter plate lower end is equipped with the duct being discharged for filtrate, and the filtrate of each piece of filter plate, which is converged from one, goes out liquid
Outside pipeline discharge machine, the bentonite for adsorbing glycerol is squeezed into cake bulk and falls.
The lower section of filter press 2 is disintegrating machine 3, and in next floor, disintegrating machine 3 includes material-falling hopper 31, smashes stick 32, filter for setting
Net 33 and collecting bag 34, material-falling hopper 31 are docked with filter press 2, and cake bulk bentonite is fallen into material-falling hopper 31, are smashed stick 32 and are arranged
In the lower exit of material-falling hopper 31, smashing stick 32 is lopping more horizontally disposed cross bars 321, and cross bar and material-falling hopper long side are flat
Row is agitating shaft 322 in the middle part of more cross bars, has connecting rod 323 to be connected between cross bar 321 and agitating shaft 322, agitating shaft 322 with outside
Portion's stirring motor is connected, and motor drives agitating shaft 322 and cross bar 321 to rotate, the cross bar that can be rotated when bentonite biscuit is fallen
321 smash；The lower section for smashing stick 32 is equipped with strainer 33, and strainer 33 is arc-shaped, and the lower section of strainer 33 is collecting bag 34；It is crashed to pieces
Bentonite fall on strainer 33, powdered granule can be fallen into collecting bag 34 by strainer, and blocky bentonite can then be rotated
The drive of cross bar 321 throw, repeatedly fragmentation process again.
Native mouth 12 is added to be connected with feeder 4, feeder 4 send the bentonite of 1 lower section of knockout drum to knockout drum 1 upwards,
In the present embodiment, feeder 4 is flood dragon 41, is driven and is rotated by flood dragon motor 42, bentonite is delivered up, the pipe of flood dragon 41
Wall is equipped with inflatable mouth 43, is connected with air pump, can prevent from blocking while be convenient to clean flood dragon.
The above is only the utility model preferred embodiment, not appoints to the technical scope of the utility model
What is limited, therefore any trickle amendment made by the above technical examples according to the technical essence of the present invention, equivalent variations
With modification, the protection scope of the utility model is still fallen within.
Claims (4)
1. a kind of methyl esters removes glycerol device, it is characterized in that: including knockout drum and filter press, the upper cover of the knockout drum, which is equipped with, to be used for
The feed inlet of glycerinated fatty acid methyl ester solution is added and for bentonitic plus Tu Kou, the tank body bottom of the knockout drum to be added
Portion is equipped with discharge port, and the discharge port is equipped with discharge nozzle and is connected with filter press, and the lower section of the knockout drum is equipped with air pump, and described point
It is equipped with gas outlet from the bottom in tank, is connected with air pump；The filter press be plate and frame type filter-press, by multilayer fixed plate, filter frame,
Filter plate, pressure plate and extrusion pump composition, filter plate lower end are equipped with the duct being discharged for filtrate, and the filtrate of each piece of filter plate is converged from one
Outside liquid outlet pipe discharge machine.
2. a kind of methyl esters according to claim 1 removes glycerol device, it is characterised in that: the lower section of the filter press is equipped with powder
Pure machine, the disintegrating machine include that material-falling hopper, smashing stick, strainer and collecting bag, the material-falling hopper are docked with filter press, the smashing
The lower exit of material-falling hopper is arranged in stick, and the smashing stick is more horizontally disposed cross bars of lopping, cross bar and material-falling hopper long side
In parallel, it is agitating shaft in the middle part of the more cross bars, has connecting rod to be connected between the cross bar and agitating shaft, the agitating shaft and outside
Stirring motor is connected, and the lower section for smashing stick is equipped with strainer, and the strainer is arc-shaped, and lower section is collecting bag.
3. a kind of methyl esters according to claim 1 removes glycerol device, it is characterised in that: described plus Tu Kou is also connected with a feeding
Machine, the feeder include flood dragon and flood dragon motor.
4. a kind of methyl esters according to claim 3 removes glycerol device, it is characterised in that: the tube wall of the flood dragon, which is equipped with, to be blown
Port is connected with air pump.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920093235.8U CN209548895U (en) | 2019-01-21 | 2019-01-21 | A kind of methyl esters removes glycerol device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920093235.8U CN209548895U (en) | 2019-01-21 | 2019-01-21 | A kind of methyl esters removes glycerol device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209548895U true CN209548895U (en) | 2019-10-29 |
Family
ID=68308364
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201920093235.8U Expired - Fee Related CN209548895U (en) | 2019-01-21 | 2019-01-21 | A kind of methyl esters removes glycerol device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209548895U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110812891A (en) * | 2019-11-29 | 2020-02-21 | 江西艾迪尔新能源有限公司 | Efficient fatty acid methyl ester and glycerine autosegregation device |
-
2019
- 2019-01-21 CN CN201920093235.8U patent/CN209548895U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110812891A (en) * | 2019-11-29 | 2020-02-21 | 江西艾迪尔新能源有限公司 | Efficient fatty acid methyl ester and glycerine autosegregation device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20191029 |