CN209362502U - A kind of synthesizer of Fluoxastrobin - Google Patents
A kind of synthesizer of Fluoxastrobin Download PDFInfo
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- CN209362502U CN209362502U CN201822279040.0U CN201822279040U CN209362502U CN 209362502 U CN209362502 U CN 209362502U CN 201822279040 U CN201822279040 U CN 201822279040U CN 209362502 U CN209362502 U CN 209362502U
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- autoclave body
- pipe
- feed pipe
- synthesizer
- fluoxastrobin
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Abstract
The utility model discloses a kind of synthesizers of Fluoxastrobin, including autoclave body, the autoclave body top is provided with toluene feed pipe, salicylonitrile feed pipe, potassium carbonate feed pipe and catalyst charge mechanism, the autoclave body inner tip is provided with rabbling mechanism, the autoclave body inner bottom is provided with auxiliary rabbling mechanism, the autoclave body bottom end is provided with discharge nozzle, the toluene feed pipe, salicylonitrile feed pipe, valve is mounted on potassium carbonate feed pipe and discharge nozzle, the interior of the autoclave body is provided with heating mechanism, the utility model stirring efficiency is high, mixing effect is good, plurality of raw materials can be sufficiently stirred, improve the production efficiency and the quality of production of Fluoxastrobin.
Description
Technical field
The utility model relates to Fluoxastrobin production equipment technology, specially a kind of synthesizer of Fluoxastrobin.
Background technique
Fluoxastrobin, Chinese nickname: (E)-{ 2- [6- (2- cyano-benzene oxygen) pyrimidine-4-yl oxygen] phenyl } -3- methoxy propyl
E pioic acid methyl ester；Amici reaches；(E) -2- { 2- [6 (2- cyano-benzene oxygen) pyrimidine-4-yl oxygen] phenyl } -3- methoxy acrylic acid first
Ester etc..Photolysis Half is 2 weeks in aqueous solution, to hydrolysis-stable.Raw medicine be off-white color to yellow solid (content is higher, fineness
It is better, color is more shallow).The product is methoxy acrylate (Strobilurin) class sterilization pesticide, efficient, wide spectrum, to almost
All mycota (Ascomycotina, Basidiomycotina, Mastigomycotina and Deuteromycotina) diseases for example powdery mildew, rust,
Glume blight, net blotch, downy mildew, rice blast etc. have good activity.It can be used for that cauline leaf is spraying, seed treatment, can also carry out
Soil treatment is mainly used for cereal, rice, peanut, grape, potato, fruit tree, vegetables, coffee, lawn etc..In Fluoxastrobin
In synthesis process, need the progress Hybrid Heating reaction of toluene, salicylonitrile, potassium carbonate and multiple catalysts, but at present phonetic
Bacterium Lipase absobed kettle there are mixing effects the problems such as bad, material is difficult to uniform stirring, production efficiency is low.
Utility model content
The purpose of this utility model is to provide a kind of synthesizers of Fluoxastrobin, to solve to propose in above-mentioned background technique
The problem of.
To achieve the above object, the utility model provides the following technical solutions:
A kind of synthesizer of Fluoxastrobin, including autoclave body, the autoclave body top are provided with toluene feed pipe, salicylonitrile charging
Pipe, potassium carbonate feed pipe and catalyst charge mechanism, the autoclave body inner tip are provided with rabbling mechanism, the autoclave body inner bottom
End is provided with auxiliary rabbling mechanism, and the autoclave body bottom end is provided with discharge nozzle, the toluene feed pipe, salicylonitrile feed pipe, carbon
Valve is mounted on sour potassium feed pipe and discharge nozzle, the interior of the autoclave body is provided with heating mechanism.
Preferably, the catalyst charge mechanism includes shower plate, and the shower plate is fixed on autoclave body inner tip, described
Shower plate bottom end is equipped with several equally distributed spray heads, offers cavity inside the shower plate, the spray head it is defeated
Enter end to be connected in cavity, the shower plate top is connected with input pipe, and one end of the input pipe is connected in cavity, separately
One end extends to outside autoclave body, and is connected with extraneous catalyst storage tank.
Preferably, the rabbling mechanism includes stirring motor, and the autoclave body top is equipped with cylinder, and the cylinder stretches
End is connected with lifter plate, and the autoclave body top is provided with several guide rods, and the top of the guide rod is extended to through lifter plate
Above lifter plate, pilot hole corresponding with guide rod is offered on the lifter plate, the stirring motor is mounted on lifter plate
Top, the output end of the stirring motor are connected with rotating bar, and the bottom end of the rotating bar extends to autoclave body through autoclave body top
Inside, the portion perimeter that the rotating bar is located inside autoclave body are equipped with several equally distributed stirring sheets.
Preferably, the auxiliary rabbling mechanism includes auxiliary stirring motor, and the auxiliary stirring motor is fixedly mounted on kettle
Body bottom end, the autoclave body inner bottom are rotatably equipped with turntable, the output end of the auxiliary stirring motor through autoclave body bottom end with
Turntable is connected, and the turntable periphery is provided with several equally distributed auxiliary stirring sheets.
Preferably, several equally distributed deflectors are provided on the inner sidewall of the autoclave body.
Preferably, the heating mechanism includes heat conducting pipe, and heating chamber, the heat conducting pipe are offered in the side wall of the autoclave body
It is arranged inside heating chamber, the heat conducting pipe uniformly coils autoclave body setting, and one end of the heat conducting pipe is connected with water inlet pipe, another
End is connected with outlet pipe, and the water inlet pipe and outlet pipe all extend to outside autoclave body, and are connected with extraneous thermal water source, the kettle
The outer side wall surface of body is successively covered with insulating layer and thermal insulation layer.
Compared with prior art, the utility model has the beneficial effects that leading to by raw materials such as toluene, salicylonitrile, potassium carbonate
After entering autoclave body inside, then catalyst is sprayed onto inside autoclave body by spray head, the mode of spray expands catalyst and each original
The contact area of material, to improve the reaction rate of raw material；Stirring motor drives rotating bar rotation, by stirring sheet to raw material
It is stirred, while air cylinder drives lifting plate does reciprocal elevating movement, drives stirring sheet to go up and down while rotating, thus into one
Step confuses raw material, promotes the mixing between raw material；Stirring motor driving turntable rotation is assisted, by auxiliary stirring sheet to autoclave body inside
The raw material of bottom end is stirred, and the direction of rotation of turntable and the direction of rotation of stirring sheet are on the contrary, improve mixing effect；In blender
During structure and auxiliary rabbling mechanism are stirred raw material, raw material is collided on deflector, generates turbulent flow, to promote not
Same raw material further mixes；Insulating layer and thermal insulation layer can be avoided the heat losses inside autoclave body to the external world, improve heating effect
Rate reduces energy loss, energy saving.The utility model stirring efficiency is high, and mixing effect is good, and a variety of originals can be sufficiently stirred
Material, improves the production efficiency and the quality of production of Fluoxastrobin.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of the synthesizer of Fluoxastrobin；
Fig. 2 is the structural schematic diagram of autoclave body side wall in a kind of synthesizer of Fluoxastrobin.
In figure: 1- autoclave body, 2- toluene feed pipe, 3- salicylonitrile feed pipe, 4- potassium carbonate feed pipe, 5- rabbling mechanism, 6-
Auxiliary rabbling mechanism, 7- discharge nozzle, 8- valve, 9- shower plate, 10- spray head, 11- input pipe, 12- cylinder, 13- lifter plate,
14- guide rod, 15- stirring motor, 16- rotating bar, 17- stirring sheet, 18- assist stirring motor, 19- turntable, 20- auxiliary stirring
Piece, 21- deflector, 22- heater, 23- heat conducting pipe, 24- water inlet pipe, 25- outlet pipe, 26- insulating layer, 27- thermal insulation layer.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1~2 are please referred to, the utility model provides a kind of technical solution: a kind of synthesizer of Fluoxastrobin, including autoclave body
1,1 top of autoclave body is provided with toluene feed pipe 2, salicylonitrile feed pipe 3, potassium carbonate feed pipe 4 and catalyst charge mechanism,
1 inner tip of autoclave body is provided with rabbling mechanism 5, and 1 inner bottom of autoclave body is provided with auxiliary rabbling mechanism 6, the kettle
1 bottom end of body is provided with discharge nozzle 7, on the toluene feed pipe 2, salicylonitrile feed pipe 3, potassium carbonate feed pipe 4 and discharge nozzle 7
Valve 8 is installed, the interior of the autoclave body 1 is provided with heating mechanism.
The catalyst charge mechanism includes shower plate 9, and the shower plate 9 is fixed on 1 inner tip of autoclave body, the spray
9 bottom end of plate is equipped with several equally distributed spray heads 10, and cavity is offered inside the shower plate 9, the spray head 10
Input terminal is connected in cavity, and 9 top of shower plate is connected with input pipe 11, and one end of the input pipe 11 is connected to sky
In chamber, the other end is extended to outside autoclave body 1, and is connected with extraneous catalyst storage tank, by toluene, salicylonitrile, carbonic acid
After the raw materials such as potassium are passed through 1 inside of autoclave body, then catalyst is passed through into spray head 10 and is sprayed onto inside autoclave body 1, the mode of spray expands
The contact area of catalyst and each raw material, to improve the reaction rate of raw material.
The rabbling mechanism 5 includes stirring motor 15, and 1 top of autoclave body is equipped with cylinder 12, and the cylinder 12 is stretched
Contracting end is connected with lifter plate 13, and 1 top of autoclave body is provided with several guide rods 14, and the top of the guide rod 14 is through lifting
Plate 13 extends to 13 top of lifter plate, offers pilot hole corresponding with guide rod 14, the stirring on the lifter plate 13
Motor 15 is mounted on 13 top of lifter plate, and the output end of the stirring motor 15 is connected with rotating bar 16, the rotating bar 16
Bottom end extends to inside autoclave body 1 through 1 top of autoclave body, if the portion perimeter that the rotating bar 16 is located inside autoclave body 1 is equipped with
Equally distributed stirring sheet 17 is done, stirring motor 15 drives rotating bar 16 to rotate, is stirred by stirring sheet 17 to raw material, together
When cylinder 12 drive lifter plate 13 to do reciprocal elevating movement, drive stirring sheet 17 to go up and down while rotating, to further stir
Random raw material promotes the mixing between raw material.
The auxiliary rabbling mechanism 6 includes auxiliary stirring motor 18, and the auxiliary stirring motor 18 is fixedly mounted on autoclave body 1
Bottom end, 1 inner bottom of autoclave body are rotatably equipped with turntable 19, and the output end of the auxiliary stirring motor 18 runs through 1 bottom of autoclave body
End is connected with turntable 19, and 19 periphery of turntable is provided with several equally distributed auxiliary stirring sheets 20, assists stirring motor
18 driving turntables 19 rotate, by assisting stirring sheet 20 to be stirred the raw material of 1 inner bottom of autoclave body, the rotation side of turntable 19
To the direction of rotation with stirring sheet 17 on the contrary, improving mixing effect.
Several equally distributed deflectors 21 are provided on the inner sidewall of the autoclave body 1, in rabbling mechanism 5 and auxiliary stirring
During mechanism 6 is stirred raw material, raw material is collided on deflector 21, turbulent flow is generated, to promote different raw materials
Further mix.
The heating mechanism includes heat conducting pipe 23, and heating chamber 22, the heat conducting pipe 23 are offered in the side wall of the autoclave body 1
It is arranged inside heating chamber 22, uniformly coiling autoclave body 1 is arranged the heat conducting pipe 23, and one end of the heat conducting pipe 23 is connected with into water
Pipe 24, the other end are connected with outlet pipe 25, and the water inlet pipe 24 all extends to outside autoclave body 1 with outlet pipe 25, and hot with the external world
Water source is connected, and by hot water circuit circulation in heat conducting pipe 23, heats to autoclave body 1, keeps the material in autoclave body 1 suitable
Reaction range in, promote reaction process, the outer side wall surface of the autoclave body 1 is successively covered with insulating layer 26 and thermal insulation layer 27,
Insulating layer 26 and thermal insulation layer 27 can be avoided the heat losses inside autoclave body 1 to the external world, improve heating efficiency, reduce energy damage
Consumption, it is energy saving.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and
And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms
Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new
The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in
All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting
Related claim.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (6)
1. a kind of synthesizer of Fluoxastrobin, including autoclave body (1), it is characterised in that: autoclave body (1) top be provided with toluene into
Expects pipe (2), salicylonitrile feed pipe (3), potassium carbonate feed pipe (4) and catalyst charge mechanism, autoclave body (1) inner tip are set
It is equipped with rabbling mechanism (5), autoclave body (1) inner bottom is provided with auxiliary rabbling mechanism (6), autoclave body (1) the bottom end setting
Have discharge nozzle (7), on the toluene feed pipe (2), salicylonitrile feed pipe (3), potassium carbonate feed pipe (4) and discharge nozzle (7)
It is equipped with valve (8), the interior of the autoclave body (1) is provided with heating mechanism.
2. a kind of synthesizer of Fluoxastrobin according to claim 1, it is characterised in that: catalyst charge mechanism packet
It includes shower plate (9), the shower plate (9) is fixed on autoclave body (1) inner tip, and shower plate (9) bottom end is equipped with several equal
The spray head (10) of even distribution, the shower plate (9) is internal to offer cavity, and the input terminal of the spray head (10) is connected to
In cavity, shower plate (9) top is connected with input pipe (11), and one end of the input pipe (11) is connected in cavity, separately
One end extends to autoclave body (1) outside, and is connected with extraneous catalyst storage tank.
3. a kind of synthesizer of Fluoxastrobin according to claim 1, it is characterised in that: the rabbling mechanism (5) includes
Stirring motor (15), autoclave body (1) top are equipped with cylinder (12), and the telescopic end of the cylinder (12) is connected with lifter plate
(13), autoclave body (1) top is provided with several guide rods (14), and the top of the guide rod (14) is prolonged through lifter plate (13)
It extends to above lifter plate (13), offers pilot hole corresponding with guide rod (14), the stirring on the lifter plate (13)
Motor (15) is mounted on lifter plate (13) top, and the output end of the stirring motor (15) is connected with rotating bar (16), and described turn
The bottom end of lever (16) extends to autoclave body (1) inside through autoclave body (1) top, and it is internal that the rotating bar (16) is located at autoclave body (1)
Portion perimeter several equally distributed stirring sheets (17) are installed.
4. a kind of synthesizer of Fluoxastrobin according to claim 1, it is characterised in that: the auxiliary rabbling mechanism (6)
Including assisting stirring motor (18), the auxiliary stirring motor (18) is fixedly mounted on autoclave body (1) bottom end, and the autoclave body (1) is interior
Portion bottom end is rotatably equipped with turntable (19), and the output end of auxiliary stirring motor (18) runs through autoclave body (1) bottom end and turntable
(19) it is connected, turntable (19) periphery is provided with several equally distributed auxiliary stirring sheets (20).
5. a kind of synthesizer of Fluoxastrobin according to claim 1, it is characterised in that: the inner sidewall of the autoclave body (1)
On be provided with several equally distributed deflectors (21).
6. a kind of synthesizer of Fluoxastrobin according to claim 1, it is characterised in that: the heating mechanism includes thermally conductive
It manages (23), is offered heating chamber (22) in the side wall of the autoclave body (1), heat conducting pipe (23) setting is in heating chamber (22)
Portion, the heat conducting pipe (23) uniformly coil autoclave body (1) setting, and one end of the heat conducting pipe (23) is connected with water inlet pipe (24), separately
One end is connected with outlet pipe (25), and the water inlet pipe (24) and outlet pipe (25) all extend to autoclave body (1) outside, and hot with the external world
Water source is connected, and the outer side wall surface of the autoclave body (1) is successively covered with insulating layer (26) and thermal insulation layer (27).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822279040.0U CN209362502U (en) | 2018-12-29 | 2018-12-29 | A kind of synthesizer of Fluoxastrobin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822279040.0U CN209362502U (en) | 2018-12-29 | 2018-12-29 | A kind of synthesizer of Fluoxastrobin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209362502U true CN209362502U (en) | 2019-09-10 |
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ID=67828869
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201822279040.0U Active CN209362502U (en) | 2018-12-29 | 2018-12-29 | A kind of synthesizer of Fluoxastrobin |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209362502U (en) |
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2018
- 2018-12-29 CN CN201822279040.0U patent/CN209362502U/en active Active
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