CN209362480U - Fast sampling reaction kettle - Google Patents
Fast sampling reaction kettle Download PDFInfo
- Publication number
- CN209362480U CN209362480U CN201821892679.XU CN201821892679U CN209362480U CN 209362480 U CN209362480 U CN 209362480U CN 201821892679 U CN201821892679 U CN 201821892679U CN 209362480 U CN209362480 U CN 209362480U
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- CN
- China
- Prior art keywords
- sampling
- agitating shaft
- probe tube
- reaction kettle
- balance pipe
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
A kind of fast sampling reaction kettle provided by the utility model, including autoclave body, agitating shaft is equipped in the autoclave body, rapid sampling attachment is housed on the agitating shaft, the rapid sampling attachment includes balance pipe, and the balance pipe is horizontally fixed on agitating shaft, is hinged with probe tube on the downside of described balance pipe one end, sampling hose is equipped in the probe tube, the balance pipe, which is provided with, inhales sample component；Described sampling hose one end is protruded into probe tube, and sample component is inhaled in other end connection, and the suction sample component is for drawing reaction solution.The utility model is mounted on agitating shaft, with the rotation of agitating shaft, hinged probe tube is under the influence of centrifugal force, expansion, since probe tube samples deeper with the rotation of agitating shaft so that probe tube can be set in the side close to agitating shaft, closer to agitating shaft, the immutable bring error in position is down-sampled；Sampling operation is simplified, automatic operation is easy to implement.
Description
Technical field
The utility model relates to field of chemical equipment, and in particular to a kind of fast sampling reaction kettle.
Background technique
Currently, existing reaction kettle its sample during the reaction, existing probe tube can only protrude into reaction kettle and close on side
The sampling of wall side, the depth of sampling and position can not change, reaction solution biggish for viscosity, the liquid of reactor bottom position
It is more viscous, test sample there are certain sampling errors.
Such as patent document disclosed in a kind of " the reaction kettle sampler " of the non-CN201721035577.1 of application number,
Including sampler, sampler includes probe tube, the sampling valve for generating negative pressure, and one end of probe tube passes through taking on sealing cover
Sample hole enters in reaction kettle ontology, and the other end is connect with sample tank is received, and receives sample tank for the feed liquid sampling valve in collecting and sampling pipe pipe
It is arranged on probe tube, probe tube is arranged far near the reaction kettle inner sidewall of agitating shaft；The depth of sampling and position without
Method changes, and reaction solution biggish for viscosity, the liquid of reactor bottom position is more viscous, and the presence of test sample centainly samples mistake
Difference.
Utility model content
(1) technical problems to be solved
The purpose of the utility model is to provide a kind of fast sampling reaction kettle, solves existing reaction kettle and be unable to control and take
The depth of sample and position, have the defects that sampling error.
(2) technical solution
In order to solve the above-mentioned technical problem, a kind of fast sampling reaction kettle provided by the utility model, including autoclave body, it is described
It is equipped with agitating shaft in autoclave body, rapid sampling attachment is housed on the agitating shaft, the rapid sampling attachment includes balance pipe, institute
It states balance pipe to be horizontally fixed on agitating shaft, probe tube is hinged on the downside of described balance pipe one end, is equipped with and takes out in the probe tube
Sample hose, the balance pipe, which is provided with, inhales sample component；Described sampling hose one end is protruded into probe tube, and sample group is inhaled in other end connection
Part, the suction sample component is for drawing reaction solution.The utility model is mounted on agitating shaft, with the rotation of agitating shaft, hingedly
Probe tube under the influence of centrifugal force, expansion, since probe tube is with the rotation of agitating shaft, leaned on so that probe tube can be set
The side of nearly agitating shaft, sampling is deeper, closer to agitating shaft, down-samples the immutable bring error in position；It simplifies
Sampling operation is easy to implement automatic operation.
Preferably, the suction sample component includes imbibition cylinder and servo electric jar, is equipped with piston, the work in the imbibition cylinder
Push rod is connect beyond the Great Wall, and the push rod connects servo electric jar.
Preferably, the suction sample component further includes servo electric jar, and the servo electric jar includes piston rod, the piston
Bar one end connects push rod, is used for driving push rod horizontal movement.
Preferably, the fast sampling reaction kettle further includes control unit, and it is single that the servo electric jar is electrically connected control
Member, described control unit are used to control the running of servo electric jar.The utility model controls servo-electric by control unit
Cylinder running, should not manual operation, be convenient for automatic operation.
Preferably, the agitating shaft has cavity；There is sampling hard tube, the sampling hard tube bottom end is protruded into the cavity
In imbibition cylinder, the external sampling inflator of sampling hard tube.
Preferably, the fast sampling reaction kettle further includes driving motor, and the agitating shaft top is equipped with driven disc, described
Driven disc is mounted on the transmission shaft of driving motor by belt transmission connection driving disc spacing pressing, the driving disc spacing pressing.
Preferably, extension spring, the drawing are housed between the sampling pipe end and the balance pipe of separate probe tube side
Spring is stretched for providing the elastic force for driving probe tube to shrink to balance pipe.The utility model setting extension spring drives for providing
The elastic force that probe tube is shunk to balance pipe allows to the size of the rotation dynamics according to reaction kettle, downward to adjust probe tube
The angle of extension, and then control depth and the position of sampling.
(3) beneficial effect
A kind of fast sampling reaction kettle provided by the utility model, has the advantage that
1, the utility model is mounted on agitating shaft, with the rotation of agitating shaft, work of the hinged probe tube in centrifugal force
Under, expansion, since probe tube takes with the rotation of agitating shaft so that probe tube can be set in the side close to agitating shaft
Sample is deeper, closer to agitating shaft, down-samples the immutable bring error in position；Sampling operation is simplified, is easy to implement certainly
Dynamicization operation.
2, the utility model setting extension spring allows to for providing the elastic force for driving probe tube to shrink to balance pipe
According to the size of the rotation dynamics of reaction kettle, to adjust the angle that probe tube extends downwardly, and then depth and the position of sampling are controlled
It sets.
3, the utility model controlled by control unit servo electric jar running, should not manual operation, convenient for automation
Operation.
Detailed description of the invention
Fig. 1 is the fast sampling reaction kettle sectional structure chart of the embodiments of the present invention 1；
Fig. 2 is the part A enlarged drawing of fast sampling reaction kettle Fig. 1 of the embodiments of the present invention 1；
Fig. 3 is the fast sampling reaction kettle figure imbibition barrel structure figure of the embodiments of the present invention 1；
Fig. 4 is the fast sampling reaction kettle figure sampling inflator structure figure of the embodiments of the present invention 1；
Fig. 5 is the control unit flow chart of the embodiments of the present invention 1.
1, autoclave body；2, agitating shaft；3, driving motor；4, driven disc；5, belt；6, driving disc spacing pressing；7, rapid sampling attachment；8,
Balance pipe；9, probe tube；10, sampling hose；11, extension spring；12, imbibition cylinder；13, servo electric jar；14, piston；15, it pushes away
Bar；16, piston rod；17, sampling inflator；18, control unit；19, sampling hard tube.
Specific embodiment
With reference to the accompanying drawings and examples, specific embodiment of the present utility model is described in further detail.Below
Example is not intended to limit the scope of the present invention for illustrating the utility model.
Embodiment 1:
As shown in figure 1, figure 2, figure 3, figure 4 and figure 5, a kind of fast sampling reaction kettle provided by the utility model, including autoclave body
1, agitating shaft 2 is equipped in the autoclave body, the fast sampling reaction kettle further includes driving motor 3, the agitating shaft top dress
There is driven disc 4, the driven disc is mounted on the transmission shaft of driving motor by the transmission connection driving disc spacing pressing 6 of belt 5, the driving disc spacing pressing
On.
Rapid sampling attachment 7 is housed, the rapid sampling attachment includes balance pipe 8, the balance pipe on the agitating shaft
It is horizontally fixed on agitating shaft, probe tube 9 is hinged on the downside of described balance pipe one end, sampling hose is equipped in the probe tube
10, the balance pipe, which is provided with, inhales sample component；Described sampling hose one end is protruded into probe tube, and sample component is inhaled in other end connection,
The suction sample component is for drawing reaction solution.Equipped with stretching between the sampling pipe end and the balance pipe of separate probe tube side
Spring 11, the extension spring is for providing the elastic force for driving probe tube to shrink to balance pipe.
The suction sample component includes imbibition cylinder 12 and servo electric jar 13, is equipped with piston 14, the work in the imbibition cylinder
Push rod 15 is connect beyond the Great Wall, and the push rod connects servo electric jar.The suction sample component further includes servo electric jar, the servo-electric
Cylinder includes piston rod 16, and described piston rod one end connects push rod, is used for driving push rod horizontal movement.The fast sampling reaction kettle
It further include control unit, the servo electric jar is electrically connected control unit 18, and described control unit is for controlling servo-electric
The running of cylinder.PLC(programmable logic controller (PLC) can be used in the control unit of the utility model).The utility model passes through, should not
Automatic operation is convenient in manual operation.The agitating shaft has cavity；There is sampling hard tube, the sampling is hard in the cavity
19 bottom end of pipe is protruded into imbibition cylinder, the external sampling inflator 17 of sampling hard tube.
When the embodiments of the present invention are implemented, control unit operates to control servo electric jar, and then pushes push rod fortune
It is dynamic, piston motion is driven, draws and liquid in reaction kettle is drawn by sampling hose, the revolving speed by adjusting agitating shaft takes to adjust
The depth of sample pipe extended downwardly and position.
The various embodiments described above are merely to illustrate the utility model, wherein the structure of each component, connection type etc. are all can be with
It is varied, all equivalents and improvement carried out on the basis of technical solutions of the utility model should not exclude
Except the protection scope of the utility model.
Claims (7)
1. a kind of fast sampling reaction kettle characterized by comprising autoclave body is equipped with agitating shaft, the stirring in the autoclave body
Rapid sampling attachment is housed on axis, the rapid sampling attachment includes balance pipe, and the balance pipe is horizontally fixed on agitating shaft,
It is hinged with probe tube on the downside of described balance pipe one end, sampling hose is equipped in the probe tube, the balance pipe is provided with suction sample
Component；Described sampling hose one end is protruded into probe tube, and sample component is inhaled in other end connection, and the suction sample component is for drawing reaction
Liquid.
2. fast sampling reaction kettle as described in claim 1, which is characterized in that the suction sample component includes imbibition cylinder and servo
Electric cylinder, the imbibition cylinder is interior to be equipped with piston, the external push rod of piston, the push rod connection servo electric jar.
3. fast sampling reaction kettle as claimed in claim 2, which is characterized in that the suction sample component further includes servo-electric
Cylinder, the servo electric jar include piston rod, and described piston rod one end connects push rod, are used for driving push rod horizontal movement.
4. fast sampling reaction kettle as claimed in claim 3, which is characterized in that it further include control unit, the servo-electric
Cylinder is electrically connected control unit, and described control unit is used to control the running of servo electric jar.
5. fast sampling reaction kettle as claimed in claim 4, which is characterized in that the agitating shaft has cavity；The cavity
Interior to have sampling hard tube, the sampling hard tube bottom end is protruded into imbibition cylinder, the external sampling inflator of sampling hard tube.
6. the fast sampling reaction kettle as described in claims 1 or 2 or 3 or 4 or 5, which is characterized in that it further include driving motor,
The agitating shaft top is equipped with driven disc, and the driven disc is mounted on drive by belt transmission connection driving disc spacing pressing, the driving disc spacing pressing
On the transmission shaft of dynamic motor.
7. the fast sampling reaction kettle as described in claims 1 or 2 or 3 or 4 or 5, which is characterized in that the sampling pipe end and
Extension spring is housed, the extension spring drives probe tube to balance pipe for providing between the balance pipe far from probe tube side
The elastic force of contraction.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821892679.XU CN209362480U (en) | 2018-11-16 | 2018-11-16 | Fast sampling reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821892679.XU CN209362480U (en) | 2018-11-16 | 2018-11-16 | Fast sampling reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209362480U true CN209362480U (en) | 2019-09-10 |
Family
ID=67836998
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821892679.XU Active CN209362480U (en) | 2018-11-16 | 2018-11-16 | Fast sampling reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209362480U (en) |
-
2018
- 2018-11-16 CN CN201821892679.XU patent/CN209362480U/en active Active
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