CN209307125U - A kind of muskone production waste liquor treatment equipment - Google Patents

A kind of muskone production waste liquor treatment equipment Download PDF

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Publication number
CN209307125U
CN209307125U CN201820912816.5U CN201820912816U CN209307125U CN 209307125 U CN209307125 U CN 209307125U CN 201820912816 U CN201820912816 U CN 201820912816U CN 209307125 U CN209307125 U CN 209307125U
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CN
China
Prior art keywords
tank
tube
alkali
recrystallization
neutralizing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201820912816.5U
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Chinese (zh)
Inventor
韩朝金
栾志华
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Anhui Great Nation Essential Oils Co Ltd
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Anhui Great Nation Essential Oils Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Priority to CN201820912816.5U priority Critical patent/CN209307125U/en
Application granted granted Critical
Publication of CN209307125U publication Critical patent/CN209307125U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of muskones to produce waste liquor treatment equipment, including inlet tube, the inlet tube is installed on inside recrystallization tank, water cooling tube and lower water cooling tube are provided with outside the recrystallization tank, water pump is provided in the middle part of first outlet tube, the first outlet tube right part is connected with neutralizing tank, the neutralizing tank outside top is provided with stirring motor, the stirring motor bottom is equipped with shaft, the shaft bottom is equipped with blade, acid storage tank is provided on the right side of the stirring motor, the acid storage tank bottom is equipped with out acid tube, sour electrically-controlled valve is provided with out in the middle part of the acid tube out, storage alkali tank is provided on the right side of the acid storage tank, the storage alkali pot bottom is equipped with alkali outlet pipe, alkali electrically-controlled valve is provided with out in the middle part of the alkali outlet pipe, right wall is provided with pH value detector inside the neutralizing tank, the pH value detector and it is described go out Sour electrically-controlled valve goes out the control connection of alkali electrically-controlled valve, and the neutralizing tank bottom right is provided with the second outlet tube.

Description

A kind of muskone production waste liquor treatment equipment
Technical field
The utility model relates to chemical equipment technical field, specifically a kind of muskone produces waste liquor treatment equipment.
Background technique
Muskone is the representative kind of macrocyclic musk, and muskone has sweet giving off a strong fragrance, can adjust very well with various fragrance With pharmacologically there is lean nervous centralis of putting forth energy, respiratory center and heart, promoting the effect of drought a variety of urea bodies secretion, be that one kind is controlled Treat the important drugs of mind mistake fan.
There are many synthetic method, raw material may be selected cyclohexanone, butadiene, cyclopentadecanone etc. and sets out synthesis muskone.With fourth Diene be the side of raw material fail be study at present extremely more, one of more promising method, taken by butadiene three and generate 12 Then carbon -1,5,9- triolefin hydrogenate, are oxidized to cyclododecanone, then obtain muskone through multistep reaction, yield is up to 40%.
In the prior art, muskone production waste liquor treatment equipment is usually during waste collection blending is placed in neutralizing tank And processing, it is handled using filtering, precipitating, activated carbon adsorption etc., but it is in and preceding due to having dissolved many raw materials in waste liquid Organic matter will lead to and neutralize that low efficiency, neutralization reaction product are complicated and toxicity is big, greatly increases enterprise's treatment cost of waste liquor.
Utility model content
In order to solve the problems mentioned above in the background art, the utility model is provided at a kind of muskone production waste liquid Manage equipment.
To achieve the above object, the utility model provides the following technical solutions:
A kind of muskone production waste liquor treatment equipment, including inlet tube, the inlet tube are installed on inside recrystallization tank, institute It states and is provided with water cooling tube and lower water cooling tube outside recrystallization tank, the first outlet tube is connected to the recrystallization tank, and described first Water pump is provided in the middle part of outlet tube, the first outlet tube right part is connected with neutralizing tank, first outlet tube and the neutralization Tank connection, the neutralizing tank outside top are provided with stirring motor, and the stirring motor bottom is equipped with shaft, the rotating shaft bottom Portion protrudes into inside the neutralizing tank and is equipped with blade, is provided with acid storage tank, the acid storage tank bottom on the right side of the stirring motor Acid tube is installed out, sour electrically-controlled valve is provided with out in the middle part of the acid tube out, the acid tube bottom out is located inside the neutralizing tank, Storage alkali tank is provided on the right side of the acid storage tank, the storage alkali pot bottom is equipped with alkali outlet pipe, is provided with out in the middle part of the alkali outlet pipe Alkali electrically-controlled valve, the alkali outlet pipe bottom are located inside the neutralizing tank, and right wall is provided with pH value detector inside the neutralizing tank, The pH value detector and it is described go out sour electrically-controlled valve, go out the control of alkali electrically-controlled valve and connect, the neutralizing tank bottom right is provided with the It is connected to inside two outlet tubes, second outlet tube and the neutralizing tank.
Further scheme as the utility model: the inlet tube right end is equipped with spray head.
Further scheme as the utility model: middle part is equipped with filter plate inside the recrystallization tank.
Further scheme as the utility model: the recrystallization tank interior bottom portion is provided with bottom plate.
Further scheme as the utility model: recrystallization tank interior bottom portion left end is provided with discharge port, the bottom Plate passes through the discharge port and moves left and right.
Further scheme as the utility model: the recrystallization tank interior bottom portion right end is provided with strainer, the filter Net right end is provided with first outlet tube.
Compared with prior art, the utility model has the beneficial effects that
Waste liquid is introduced into the recrystallization tank after generating, and expands the surface area of waste liquid by the spray head, with the heavy knot It is first cooling for the first time by the upper water cooling tube after the inner wall contact of brilliant tank, it falls on the filter plate, first can be carried out to waste liquid Secondary cooling, and slow down waste liquid in the recrystallization pot bottom aggregation velocity, cooling efficiency is substantially increased, while the filter plate is also The contaminant filter in waste liquid can be dropped, flows to the recrystallization pot bottom to waste liquid, the lower water cooling tube is further cooling by it, gives up Impurity in liquid starts to recrystallize, and when waste thoroughly cools down, pumps it to the neutralizing tank using the water pump, and recrystallize Impurity is taken out since the filtering of the strainer has stayed on the bottom plate, by the bottom plate by the discharge port, includes in impurity A large amount of raw material can continue to use as raw material, greatly reduce enterprise's cost of material, pass through simultaneously after elution filtering The waste liquid of recrystallization is neutralized again, more efficient, and reaction product toxicity reduces, reaction speed is accelerated, neutralize rear impurity it is less, More environmentally friendly, subsequent filter processing difficulty reduces, and for substantially reducing for enterprise's treatment cost of waste liquor, is worth of widely use.
Detailed description of the invention
Fig. 1 is the structural schematic diagram that muskone produces waste liquor treatment equipment.
Fig. 2 is that muskone produces the structural schematic diagram that tank is recrystallized in waste liquor treatment equipment.
Fig. 3 is the enlarged drawing of part A in Fig. 2.
In figure: 1- inlet tube, 101- spray head, 2- recrystallize tank, 201- filter plate, 202- bottom plate, 203- discharge port, 204- filter Net, the upper water cooling tube of 3-, water cooling tube under 4-, the first outlet tube of 5-, 6- water pump, 7- neutralizing tank, 8- stirring motor, 9- shaft, 10- leaf Piece, 11- acid storage tank, 12- go out acid tube, and 13- goes out sour electrically-controlled valve, and 14- stores up alkali tank, 15- alkali outlet pipe, and 16- goes out alkali electrically-controlled valve, 17-pH It is worth detector, the second outlet tube of 18-.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
Please refer to Fig. 1,2,3, in the utility model embodiment, a kind of muskone produces waste liquor treatment equipment, including feed liquor Pipe 1,1 right end of inlet tube are equipped with spray head 101, and the spray head 101 is installed on inside recrystallization tank 2, the recrystallization The inside of tank 2 middle part is equipped with filter plate 201, and 2 interior bottom portion of recrystallization tank is provided with bottom plate 202, inside the recrystallization tank 2 Bottom left end is provided with discharge port 203, and the bottom plate 202 passes through the discharge port 203 and moves left and right, inside the recrystallization tank 2 Bottom right end is provided with strainer 204, and 204 right end of strainer is provided with the first outlet tube 5, first outlet tube 5 with it is described It recrystallizes tank 2 to be connected to, water cooling tube 3 and lower water cooling tube 4,5 middle part of the first outlet tube is provided with outside the recrystallization tank 2 It is provided with water pump 6,5 right part of the first outlet tube is connected with neutralizing tank 7, and first outlet tube 5 connects with the neutralizing tank 7 Logical, 7 outside top of neutralizing tank is provided with stirring motor 8, and 8 bottom of stirring motor is equipped with shaft 9, the shaft 9 Bottom protrudes into 7 inside of neutralizing tank and is equipped with blade 10, and acid storage tank 11, the storage are provided on the right side of the stirring motor 8 Sour 11 bottom of tank is equipped with out acid tube 12, and sour electrically-controlled valve 13,12 bottom of acid tube out are provided with out in the middle part of the acid tube 12 out Inside the neutralizing tank 7, storage alkali tank 14 is provided on the right side of the acid storage tank 11,14 bottom of storage alkali tank is equipped with out alkali Pipe 15 is provided with out alkali electrically-controlled valve 16 in the middle part of the alkali outlet pipe 15, and 15 bottom of alkali outlet pipe is located inside the neutralizing tank 7, The 7 inside right wall of neutralizing tank is provided with pH value detector 17, the pH value detector 17 and sour out electrically-controlled valve 13, the out alkali The control connection of electrically-controlled valve 16,7 bottom right of neutralizing tank are provided with the second outlet tube 18, second outlet tube 18 with it is described It is connected to inside neutralizing tank 7.
The working principle of the utility model is: waste liquid is introduced into the recrystallization tank 2 after generating, pass through the spray head 101 The surface area for expanding waste liquid is first cooled down for the first time by the upper water cooling tube 3, is fallen in after contacting with the inner wall of the recrystallization tank 2 On the filter plate 201, first time cooling can be carried out to waste liquid, and slow down waste liquid in the 2 congregate speed of recrystallization tank, Cooling efficiency is substantially increased, while the contaminant filter in waste liquid can also drop in the filter plate 201, flows to the recrystallization to waste liquid 2 bottom of tank, the lower water cooling tube 4 is further cooling by it, and the impurity in waste liquid starts to recrystallize, and when waste thoroughly cools down, makes The neutralizing tank 7 is pumped it to the water pump 6, and the impurity recrystallized is described since the filtering of the strainer 204 has stayed in On bottom plate 202, the bottom plate 202 is taken out by the discharge port 203, includes a large amount of raw material in impurity, filtered by elution After can continue to use as raw material, greatly reduce enterprise's cost of material, while being neutralized again by the waste liquid of recrystallization, More efficient, reaction product toxicity reduces, reaction speed is accelerated, and neutralization rear impurity is less, more environmentally friendly, subsequent filter processing difficulty It reduces, for substantially reducing for enterprise's treatment cost of waste liquor, is worth of widely use.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting Related claim.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiments being understood that.

Claims (6)

1. a kind of muskone produces waste liquor treatment equipment, including inlet tube (1), it is characterised in that: the inlet tube (1) is installed on Tank (2) inside is recrystallized, is provided with water cooling tube (3) and lower water cooling tube (4), the first outlet tube outside the recrystallization tank (2) (5) it is connected to, is provided with water pump (6) in the middle part of first outlet tube (5), first outlet tube (5) with the recrystallization tank (2) Right part is connected with neutralizing tank (7), and first outlet tube (5) is connected to the neutralizing tank (7), top on the outside of the neutralizing tank (7) Portion is provided with stirring motor (8), and stirring motor (8) bottom is equipped with shaft (9), and shaft (9) bottom is protruded into described Neutralizing tank (7) is internal and is equipped with blade (10), is provided with acid storage tank (11), the acid storage tank on the right side of the stirring motor (8) (11) bottom is equipped with out acid tube (12), and sour electrically-controlled valve (13), the acid tube out are provided with out in the middle part of described acid tube (12) out (12) bottom is located at the neutralizing tank (7) inside, is provided with storage alkali tank (14), the storage alkali tank on the right side of the acid storage tank (11) (14) bottom is equipped with alkali outlet pipe (15), is provided with out alkali electrically-controlled valve (16), the alkali outlet pipe in the middle part of the alkali outlet pipe (15) (15) bottom is located at the neutralizing tank (7) inside, and the internal right wall of the neutralizing tank (7) is provided with pH value detector (17), described PH value detector (17) and the electrically-controlled valve (13) sour out, alkali electrically-controlled valve (16) control connects out, neutralizing tank (7) bottom, right Side is provided with the second outlet tube (18), is connected to inside second outlet tube (18) and the neutralizing tank (7).
2. a kind of muskone according to claim 1 produces waste liquor treatment equipment, it is characterised in that: the inlet tube (1) Right end is equipped with spray head (101).
3. a kind of muskone according to claim 1 produces waste liquor treatment equipment, it is characterised in that: the recrystallization tank (2) internal middle part is equipped with filter plate (201).
4. a kind of muskone according to claim 1 produces waste liquor treatment equipment, it is characterised in that: the recrystallization tank (2) interior bottom portion is provided with bottom plate (202).
5. a kind of muskone according to claim 4 produces waste liquor treatment equipment, it is characterised in that: the recrystallization tank (2) interior bottom portion left end is provided with discharge port (203), and the bottom plate (202) passes through the discharge port (203) and moves left and right.
6. a kind of muskone according to claim 1 produces waste liquor treatment equipment, it is characterised in that: the recrystallization tank (2) interior bottom portion right end is provided with strainer (204), and strainer (204) right end is provided with first outlet tube (5).
CN201820912816.5U 2018-06-13 2018-06-13 A kind of muskone production waste liquor treatment equipment Expired - Fee Related CN209307125U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820912816.5U CN209307125U (en) 2018-06-13 2018-06-13 A kind of muskone production waste liquor treatment equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820912816.5U CN209307125U (en) 2018-06-13 2018-06-13 A kind of muskone production waste liquor treatment equipment

Publications (1)

Publication Number Publication Date
CN209307125U true CN209307125U (en) 2019-08-27

Family

ID=67668329

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820912816.5U Expired - Fee Related CN209307125U (en) 2018-06-13 2018-06-13 A kind of muskone production waste liquor treatment equipment

Country Status (1)

Country Link
CN (1) CN209307125U (en)

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190827

CF01 Termination of patent right due to non-payment of annual fee