CN209296242U - A kind of experimental rig for the identification of non-metallic seal sealing performance - Google Patents

A kind of experimental rig for the identification of non-metallic seal sealing performance Download PDF

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Publication number
CN209296242U
CN209296242U CN201822061364.7U CN201822061364U CN209296242U CN 209296242 U CN209296242 U CN 209296242U CN 201822061364 U CN201822061364 U CN 201822061364U CN 209296242 U CN209296242 U CN 209296242U
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experimental rig
metallic seal
cavity
pressure
identification
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陆斌
郭春光
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American Drilling Deep Sea Energy Technology Research and Development Shanghai Co Ltd
MSP Drilex Shanghai Co Ltd
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American Drilling Deep Sea Energy Technology Research and Development Shanghai Co Ltd
MSP Drilex Shanghai Co Ltd
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Abstract

The utility model discloses a kind of experimental rigs for the identification of non-metallic seal sealing performance, which includes: device noumenon, and internal to have cavity, cavities open is in device noumenon bottom;Device noumenon bottom is equipped with and the close-connected bottom cover of device noumenon;It is equipped with that there are the filling members in gap with device noumenon inner wall in the cavity, the gap between described device inner body wall and the side wall of filling member is equipped with non-metallic seal to be detected;The liquid injection port communicated with the cavity is equipped at the top of device noumenon;The bottom cover is equipped with for detecting whether there is the detection hole of leakage, also comprising several pressurizations pipeline, blowdown line, heating device, temperature measuring device and device for pressure measurement for being passed through gas.The experimental rig of the utility model meets F.1.13.5.3 requirement of the standard to device experiment of ISO 10423:2009 annex, may be used in oil equipment well head and the device experiment of production tree.

Description

A kind of experimental rig for the identification of non-metallic seal sealing performance
Technical field
The utility model relates to oil equipment industry designs to confirm field, and in particular to one kind is close for non-metallic seal The experimental rig of sealing property identification.
Background technique
In oil equipment industry,Type sealing ring (S sealing) in high pressure and can have big top clearance In the case of work, be applied in the work of a variety of oil and natural gas industries.
S sealing is that the important non-metallic seal of fluid, product type specification are opened and closed in well head assembly and production tree equipment Multiplicity, security reliability is most important, once S seal failure, will cause oily (gas) well drilling well or production stops, generate huge Huge economic loss and safety accident, and will cause great environmental pollution etc..As the assembly of domestic petroleum well head and production tree set The safety of product, the requirement of reliability is continuously improved in the increase of standby demand and outlet, users at home and abroad, is to performance rate The increase in demand of 2 grades of product.Oil majors need the Performance Testing to product before product purchasing in the world at present Test performance is audited, and Performance Evaluation Test is completed to be the precondition purchased.Domestic petroleum enterprise is in the early stage of development Performance Evaluation Test is not taken much count of, but after developing to certain scale, especially when with foreign petroleum company cooperation, performance Qualification test is exactly precondition.Such as inlet channel Da Er, shell, Chevron, Kang Fei foreign oil enterprise supply chain, are being supplied Most critical one is exactly properties of product qualification test in chain audit.
The test of S sealing device is a part of non-metal sealing PR2 Performance Testing, belongs to nonmetallic fluid compatibility examination It tests, needs individually to be tested.S sealing device experimental design needs to meet ISO 10423:2009 annex and F.1.13.5.3 marks Requirement of the standard to device experiment.
At home in petroleum equipment enterprise, starting is than being the limited public affairs of beautiful diamond petroleum drilling and mining system engineering (Shanghai) earlier Department, company establish Performance Testing experiment when being prepared to enter into shell global supply chain and Dao Daer global supply chain in 2008 Room, pervious performance test in 2008 are that commission Britain mole laboratory is tested, and expense is very expensive, later in shell work With the help of Cheng Shi, the experience in British mole laboratory establishes the laboratory of oneself, starts independent innovational design oneself Properties of product testing program and program, it is less desirable always in terms of Testing Software but by offshore company's technology blockage.
It with the development of domestic petroleum enterprise, goes abroad successively, but properties of product qualification test is always that a bottleneck is asked Topic, although establishing the simple experiment room of oneself, is also weakened, even very much in terms of the scheme of performance test and test program Some companies directly require to be tested according to standard clause, cause to design the product testing result failure met the requirements originally. Also some domestic enterprises also use for reference the experience in beautiful diamond petroleum drilling and mining system engineering (Shanghai) Co., Ltd. laboratory, but in test side It is in terms of case and test program or not mature enough, when being prepared to enter into the audit of foreign oil enterprise supply chain, always it is found very More problems lead to not audit by supplier's chain.
For the status to current domestic petroleum enterprise, it is being familiar with the system engineering of beautiful diamond petroleum drilling and mining (Shanghai) limited public affairs In the case where taking charge of laboratory condition, S seal test device and its method are designed, enterprise can be equipped to domestic petroleum It offers reference or refers to when doing this aspect test.
Utility model content
The purpose of the utility model is to overcome the defects of the prior art, provide a kind of identification non-metallic seal, especiallyWhether the sealing performance of type sealing ring or similar product meets the experimental rig of PR2 test requirements document.
In order to achieve the above object, the utility model provides a kind of examination for the identification of non-metallic seal sealing performance Experiment device, the experimental rig includes: device noumenon, and internal to have cavity, cavities open is in device noumenon bottom;Device Body bottom portion is equipped with and the close-connected bottom cover of device noumenon;Filling out there are gap is equipped with device noumenon inner wall in the cavity Part is filled, the gap between described device inner body wall and the side wall of filling member is equipped with non-metallic seal to be detected;Device sheet The liquid injection port communicated with the cavity is equipped at the top of body, which is sealed by removable seal;The bottom cover It is equipped with for detecting whether there is the detection hole of leakage, which connect with leak detection apparatus;With non-metallic seal The cavity on top communicates, for being passed through several pressurization pipelines of gas;It is let out with what the cavity on non-metallic seal top communicated Pressure pipeline;For heating the heating device of described device ontology;It is arranged on described device ontology, for measuring described device sheet The temperature measuring device of body internal temperature;And be arranged on described device ontology, for measuring non-metallic seal upper cavity The device for pressure measurement of pressure.
Preferably, the filling member is cylindrical body, the non-metallic seal is O-ring seals.
Preferably, the bottom cover is flange.
Preferably, the heating device includes the heating watt that described device outer body is arranged in.
Preferably, the temperature measuring device includes temperature sensor, the device for pressure measurement is passed comprising pressure Sensor and pressure gauge.
Preferably, the experimental rig also includes: the test operation case outside the experimental rig is arranged in, with ventilation Equipment is connected.
Using above-mentioned experimental rig to the carry out qualification test of the sealing performance of non-metallic seal, the pressure inlet Line is the first pressurization pipeline and the second pressurization pipeline, and test method comprises the steps of:
Step 1: by liquid injection port, liquid pilot medium is injected into the cavity on non-metallic seal top;
Step 2: opening the valve on the first pressurization pipeline, pressurization gas is passed through into the cavity on non-metallic seal top Body makes it be pressurized to 300 ± 30psi, the valve being then shut off on the first pressurization pipeline;
Step 3, humid test is carried out, the humid test includes appointing for hot test, room temperature test and low-temperature test Meaning a combination of one or more;
The hot test includes:
A: device noumenon is heated, is allowed to warm to 121 DEG C to 132 DEG C;
B: the valve on the second pressurization pipeline is opened, additional mechanical supercharging gas is passed through, is pressurized to 15000psi, in pressurization In, test temperature is maintained at 121 DEG C to 132 DEG C;
C: after pressure is stablized, the dwell time is no less than 160 hours;Test temperature is maintained at 121 DEG C extremely in pressure maintaining period 132℃;Pressure drop cannot be greater than 500psi during pressure maintaining;
D: stop heating, cooling test device to room temperature;The valve on blowdown line is opened, by less than 1000psi/min Speed carry out pressure release, until pressure be 0;
The room temperature test includes:
E: experimental rig is in room temperature, opens the valve on the second pressurization pipeline, is passed through additional mechanical supercharging gas, is pressurized to 15000psi;
F: pressure starts pressure maintaining after stablizing, and the dwell time is no less than 1 hour;Pressure drop cannot be greater than during pressure maintaining 500psi;
G: opening the valve on blowdown line, carries out pressure release by the speed less than 1000psi/min, until pressure is 0;
The low-temperature test includes:
H: it is cooled to experimental rig between -18 DEG C to -29 DEG C;
I: the valve of the second pressurization pipeline is opened, additional mechanical supercharging gas is passed through, suppresses to 15000psi, in pressurization In, test temperature is maintained at -18 DEG C to -29 DEG C;
J: pressure maintaining, dwell time are no less than 1 hour;Pressure drop cannot be greater than 500psi during pressure maintaining;
K: opening the valve on blowdown line, carries out pressure release by the speed less than 1000psi/min, until pressure is 0;Make Experimental rig completes experiment after being back to room temperature.
Preferably, the liquid pilot medium includes diesel oil and water;The pressurization gas includes: H2S, CO2 and CH4, the additional mechanical supercharging gas include nitrogen.
Preferably, opening the valve on the second pressurization pipeline when pressure drop is greater than 500psi during pressure maintaining, being pressurized to 15000psi。
Preferably, further include the ontology gas pressure test for detecting the experimental rig air-tightness before carrying out step 1, this Body gas pressure test method includes:
(1) into the water by experimental rig;
(2) it carries out step L: additional mechanical supercharging gas being passed through by the first pressurization pipeline and is suppressed to 15000psi;Ensure pressure After stabilization, the dwell time is no less than 15 minutes, pressure release to 0;It is primary to repeat step L;
(3) whether there is the change rate of pressure during bubble generation and pressure maintaining during test in observation water.
The utility model has the advantages that
Experimental rig provided by the utility model for the identification of non-metallic seal sealing performance, realizes nonmetallic The identification of the PR2 rank sealing performance of sealing element.The experimental rig of the utility model meets ISO 10423:2009 annex F.1.13.5.3 requirement of the standard to device experiment may be used in oil equipment well head and the device experiment of production tree.
Detailed description of the invention
Fig. 1 is the experimental rig structural schematic diagram for the identification of non-metallic seal sealing performance of the utility model.
Specific embodiment
The technical solution of the utility model is described further below in conjunction with drawings and examples.
As shown in Figure 1, the utility model provides a kind of experimental rig for the identification of non-metallic seal sealing performance, The experimental rig mainly forThe identification of the PR2 rank sealing performance of type sealing ring (S sealing) or similar products Test.The experimental rig includes: device noumenon 1, and internal to have cavity, cavities open is in the bottom of device noumenon 1;Device sheet 1 bottom of body is equipped with and the close-connected bottom cover 12 of device noumenon 1;Equipped with there are gaps with 1 inner wall of device noumenon in the cavity Filling member 13, gap between 1 inner wall of described device ontology and the side wall of filling member 13 is equipped with nonmetallic sealing to be detected Part 2;Be equipped with the liquid injection port 14 that communicates with the cavity at the top of device noumenon 1, the liquid injection port 14 by removable seal into Row sealing;The bottom cover 12 is equipped with for detecting whether there is the detection hole 121 of leakage, and detection hole 121 and leak detection fill Set connection.In some embodiments, bottom cover 12 is flange.Non-metallic seal 2 can separate the cavity inside device noumenon 1, Flow out test(ing) medium also can not can not just from detection hole 121 by non-metallic seal 2.
In the experimental rig of the utility model, filling member 13 is cylindrical body, and non-metallic seal 2 is O shape sealing ring, is fitted ForThe sealing performance qualification test of type sealing ring (S sealing).
The experimental rig also includes to communicate with the cavity on 2 top of non-metallic seal, for being passed through several increasings of gas Pressure pipeline.The cavity on 2 top of non-metallic seal is pressurized by being pressurized pipeline, can detect nonmetallic close under condition of high voltage The leakproofness of sealing 2.The experimental rig is additionally provided with the blowdown line 5 communicated with the cavity on 2 top of non-metallic seal.Pressure inlet Valve 6 is respectively arranged on line and blowdown line 5.Valve 6 is shut-off valve.In the utility model, 2 pressurization pipelines are set, point It Wei not the first pressurization pipeline 3 and the second pressurization pipeline 4.When carrying out device experiment, if 2 sealing performance of non-metallic seal is lost Effect, test(ing) medium (liquid or gas) can be leaked from detection hole 12.Leak detection apparatus using drainage to leaked gas into Row is collected and measurement.
The experimental rig also includes the heating device for heating described device ontology 1, can be used for detecting under hot environment The leakproofness of non-metallic seal 2.
In some embodiments, heating device select heating watt, the outer diameter according to device noumenon 1 is customized, guarantee effectively and Uniform heating.
The experimental rig also includes to be arranged in device noumenon 1, and the temperature for 1 internal temperature of measuring device ontology measures Device;Device for pressure measurement in device noumenon 1, for 1 internal pressure of measuring device ontology is set.
In some embodiments, the temperature measuring device is temperature sensor, and the device for pressure measurement includes Pressure sensor and pressure gauge.
It is provided with test operation case outside the experimental rig of the utility model, is connected with ventilation equipment.During test, examination Testing control box is in experimental rig in subnormal ambient, can take gas test medium away in time.
The testing program that sealing performance is identified using the experimental rig of the utility model are as follows:
A) experimental rig is simulated S seal operation environment and is designed to split type according to the principle that may be reused;
B) the standard connection flange that experimental rig selects API6A to recommend, device noumenon and flange is mating is designed;
C) bolt of device is countersunk bolt, and rule of thumb, countersunk bolt is easy installation, and tooling is small in size, light-weight;
D) temperature measurement installation standard requirements beat the hole that diameter is less than 13mm on flange, and hole is less than with a distance from inner wall 13mm;
E) temperature-adjusting heating device uses heating watt, and according to experimental rig outer diameter heating watt customized, maximum temperature will reach 140 ℃;
F) test operation case is equipped with outside experimental rig, internal exhausting forms negative pressure, and gas leakage be discharged can in time;
G) pipeline, shut-off valve and connector of test use anti-corrosion material;
H) test high pressure connection uses Autoclave button-type, it is ensured that high pressure sealing.
Test operation step has 2 parts, including ontology gas pressure test and device experiment, test operation are described as follows:
1. ontology gas pressure test
Measurement instrument needed for 1.1:
The pressure gauge (range: 0-20000psi) of a calibration;
The pressure schedule recorder of b calibration.
1.2 test(ing) mediums:
Nitrogen.
Test temperature:
Room temperature.
1.3 test procedures:
A) non-metallic seal is installed on the filling member of experimental rig, then presses Fig. 1 joint test device, and pass through row Vehicle hangs in gas pressure test pond, transfer to device bolt completely into the water, top from the water surface about 5cm, convenient for observe whether There is leakage and bubble is caused to be emerged;
B) all other shut-off valve in addition to the shut-off valve of the first pressurization pipeline is closed;
C) it is pressurized pipeline air pressure 15000psi or more the first of experimental rig, but no more than 15500psi;
D) after ensuring that pressure is stablized, the shut-off valve for closing the first pressurization pipeline starts pressure maintaining, and the dwell time is not less than 15 points Clock;
E) shut-off valve that the first pressurization pipeline is slowly opened after the completion of pressure maintaining, by the speed pressure release for being less than 1000psi/min To 0;
F) continue to be pressurized pipeline air pressure to 15000psi the first of experimental rig;
G) after ensuring that pressure is stablized, the shut-off valve for closing the first pressurization pipeline starts pressure maintaining, and the dwell time is not less than 15min;
H) shut-off valve that the first pressurization pipeline is slowly opened after the completion of pressure maintaining, by the speed pressure release for being less than 1000psi/min To 0psi;
I) after meeting acceptance criteria, experimental rig is hung out into pressure testing pond, continues to test.
Acceptance criteria
A is generated in pond without visible bubble during pressure maintaining in gas pressure test;
Pressure is stablized during b pressure maintaining, and change rate should be maintained within 500psi per hour.
2. device experiment
Measurement instrument needed for 2.1
The pressure gauge (range: 0-20000psi) of a calibration
The pressure sensor of b calibration (connection computer shows pressure value in computer control software)
The temperature sensor (connection computer, the displays temperature value in computer control software) of c calibration
2.2 test(ing) medium
A diesel oil, water;
B pressurization gas is mixed gas (10%H2S, 80%CO2, 10%CH4);
C additional mechanical supercharging gas is nitrogen.
2.3 test temperature
Room temperature: 25 ± 5 DEG C;
Maximum temperature: 121 DEG C~132 DEG C;
Minimum temperature: -18 DEG C~-29 DEG C.
2.4 test procedures:
A) according to the size of the cavity on non-metallic seal top, calculate account for the cavity net volume 60% diesel oil amount and 5% water measures corresponding diesel oil and distilled water with suitable graduated cylinder.
B) it is injected by liquid injection hole into cavity and is ready for diesel oil, reinject distilled water.
C) Fig. 1 connection equipment is then pressed, all shut-off valves are closed, experimental rig is put into test operation case, opens ventilation Equipment makes experimental rig be in negative pressure state.
D) operator (must 2 people or more) has dressed breathing mask according to requirement of shelter, is ready for subsequent plus mixing Gas-operated.
E) the first shut-off valve for increasing pipeline is opened, is pressurized to the cavity on non-metallic seal top with mixed gas 300 ± 30psi is then shut off shut-off valve, and the mixed gas in the first pressurization pipeline is discharged, the first pressure inlet is then removed Line;
F) start-up temperature control system is slowly heated device noumenon, is warming up to 121 DEG C or more, controls at 121 DEG C To between 132 DEG C;
G) shut-off valve for opening the second pressurization pipeline, is pressurized to by the cavity that nitrogen is non-metallic seal top 15000psi, in pressurization, test temperature cannot be below 121 DEG C or higher than 132 DEG C;
H) shut-off valve of the second pressurization pipeline, nitrogen pressurization system pressure release are closed;
I) 160 hours of pressure maintaining after power is stablized test pressure drop and are not higher than 500psi, test temperature in pressure maintaining period during pressure maintaining Degree cannot be below 121 DEG C or higher than 132 DEG C.(the every 30min record of the process is primary, in the inspection of experimental rig during high temperature pressure maintaining Gaging hole is collected leaked gas with drainage, carries out recording every 4 hours primary.)
J) stop heating by temperature control system, experimental rig is made to be cooled to room temperature (25 ± 5 DEG C);
K) shut-off valve for slowly opening blowdown line carries out pressure release by the speed less than 1000psi/min, until pressure drop To 0;
L) shut-off valve for closing blowdown line opens the shut-off valve of the second pressurization pipeline, makes nonmetallic sealing by nitrogen The cavity on part top is pressurized to 15000psi;
M) pressure starts pressure maintaining after stablizing, and the dwell time is no less than 1 hour, and pressure drop is tested during pressure maintaining and is not higher than 500psi;
N) shut-off valve for slowly opening blowdown line carries out pressure release by the speed less than 1000psi/min, until pressure drop To 0;
O) heating watt on experimental rig is removed, experimental rig is put into high-low temperature test chamber;
P) high-low temperature test chamber is set as cooling mode, and segmentation cools down to experimental rig, is cooled to -18 DEG C to -29 Between DEG C;
Q) open second pressurization pipeline shut-off valve, by nitrogen be non-metallic seal top cavity suppress to 15000psi, in pressurization, test temperature cannot be below -29 DEG C or higher than -18 DEG C;
R) pressure starts pressure maintaining after stablizing, and the dwell time is no less than 1 hour, and pressure drop cannot be greater than during pressure maintaining 500psi;
S) shut-off valve for slowly opening blowdown line, by the speed pressure release for being less than 1000psi/min, until pressure is down to 0;
T) high-low temperature test chamber is opened wide, experimental rig is allowed to be back to room temperature.
Acceptance criteria
A. during entire rated pressure pressure maintaining, test pressure drop should be less than 500psi, can when pressure drop is greater than 500psi 15000psi is pressurized to from the second pressurization pipeline with nitrogen;
B. during hot test, highest test temperature cannot be below 121 DEG C or higher than 132 DEG C;
C. during low-temperature test, minimum test temperature cannot be below -29 DEG C or higher than -18 DEG C;
D. after hot test in 160 hours, the leakage rate that leak detection apparatus detects should be less than 100cm3, do not hold Continuous visible bubble in bubble (20cm3/ h or more);
E. after room temperature and low-temperature test, the leakage rate that leak detection apparatus detects should be less than 20cm3, persistently may not be used See bubble (20cm3/ h or more).
In conclusion being filled using the test provided by the utility model for the identification of non-metallic seal sealing performance It sets, realizes the device experiment of the PR2 rank sealing performance identification of non-metallic seal.The experimental rig of the utility model meets F.1.13.5.3 requirement of the standard to device experiment of ISO 10423:2009 annex, may be used on oil equipment well head and production tree Device experiment in.
It is discussed in detail although the content of the utility model has passed through above preferred embodiment, but it should be appreciated that on The description stated is not considered as limitations of the present invention.After those skilled in the art have read above content, for A variety of modifications and substitutions of the utility model all will be apparent.Therefore, the protection scope of the utility model should be by appended Claim limit.

Claims (6)

1. a kind of experimental rig for the identification of non-metallic seal sealing performance, which is characterized in that the experimental rig packet Contain:
Device noumenon, internal to have cavity, cavities open is in device noumenon bottom;Device noumenon bottom is equipped with and device noumenon Close-connected bottom cover;Equipped with there are the filling member in gap, described device inner body walls with device noumenon inner wall in the cavity Gap between the side wall of filling member is equipped with non-metallic seal to be detected;It is equipped with and the cavity phase at the top of device noumenon Logical liquid injection port, the liquid injection port are sealed by removable seal;The bottom cover be equipped with for detecting whether in the presence of The detection hole of leakage, the detection hole are connect with leak detection apparatus;
It is communicated with the cavity on non-metallic seal top, for being passed through several pressurization pipelines of gas;
The blowdown line communicated with the cavity on non-metallic seal top;
For heating the heating device of described device ontology;
It is arranged on described device ontology, for measuring the temperature measuring device of described device body interior temperature;And
It is arranged on described device ontology, for measuring the device for pressure measurement of non-metallic seal upper cavity pressure.
2. the experimental rig for the identification of non-metallic seal sealing performance as described in claim 1, which is characterized in that described Filling member be cylindrical body, the non-metallic seal be O-ring seals.
3. the experimental rig for the identification of non-metallic seal sealing performance as described in claim 1, which is characterized in that described Bottom cover be flange.
4. the experimental rig for the identification of non-metallic seal sealing performance as described in claim 1, which is characterized in that described Heating device include that the heating watt of described device outer body is set.
5. the experimental rig for the identification of non-metallic seal sealing performance as described in claim 1, which is characterized in that described Temperature measuring device include temperature sensor, the device for pressure measurement include pressure sensor and pressure gauge.
6. the experimental rig for the identification of non-metallic seal sealing performance as described in claim 1, which is characterized in that described Experimental rig also include: the test operation case outside the experimental rig is set, is connected with ventilation equipment.
CN201822061364.7U 2018-12-10 2018-12-10 A kind of experimental rig for the identification of non-metallic seal sealing performance Active CN209296242U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109387336A (en) * 2018-12-10 2019-02-26 美钻深海能源科技研发(上海)有限公司 A kind of experimental rig and method for the identification of non-metallic seal sealing performance

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109387336A (en) * 2018-12-10 2019-02-26 美钻深海能源科技研发(上海)有限公司 A kind of experimental rig and method for the identification of non-metallic seal sealing performance

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