CN209231151U - A kind of analyzer - Google Patents

A kind of analyzer Download PDF

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Publication number
CN209231151U
CN209231151U CN201822083970.9U CN201822083970U CN209231151U CN 209231151 U CN209231151 U CN 209231151U CN 201822083970 U CN201822083970 U CN 201822083970U CN 209231151 U CN209231151 U CN 209231151U
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China
Prior art keywords
specimen cup
measuring device
analyzer according
cup
temperature
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CN201822083970.9U
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Chinese (zh)
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江泽润
刘成林
李祖祥
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SHENZHEN JINSHI PETROCHEMICAL INSTRUMENT CO Ltd
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SHENZHEN JINSHI PETROCHEMICAL INSTRUMENT CO Ltd
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Abstract

The utility model relates to intermiscibility testing fields, disclose a kind of analyzer, including measuring device and specimen cup, the measuring device includes the temperature sensor being arranged in specimen cup, the measuring device further includes surrounding the semiconductor refrigerating module of specimen cup setting, the measuring device further includes metal bath, and the laser detection module for measuring cuvette sample light passing value.When measurement, by the regulation for carrying out temperature to specimen cup, the sample being placed in specimen cup is detected in real time followed by temperature sensor and laser monitoring module, by the data feedback of real-time detection at host, temperature of the host to will test and light passing value at such a temperature are recorded, then run a curve figure according to the data of record, find in the graph inflection point and by inflection point temperature and light passing value write down, obtain determination data.Have the advantages that efficiently measure solubility between refrigerant and corresponding refrigerator oil.

Description

A kind of analyzer
Technical field
The utility model relates to intermiscibility testing field more particularly to a kind of analyzers.
Background technique
The dissolution characteristics of refrigerant and corresponding refrigerator oil are constantly subjected to widely pay close attention to.Refrigeration system generally requires to freeze Machine oil and refrigerant have certain intermiscibility.If the intermiscibility of the two is good, refrigerant meltage in refrigerator oil can accordingly increase Greatly, then the oil return rate of system can be greatly speeded up.
Currently on the market, lack the instrument for carrying out solubility measurement to refrigerant and corresponding refrigerator oil, be badly in need of a kind of high The solubility measuring instrument of effect.
Utility model content
In view of the deficienciess of the prior art, having efficiently the purpose of this utility model is to provide a kind of analyzer The advantages of measuring solubility between refrigerant and corresponding refrigerator oil.
To achieve the above object, the utility model can be achieved by the following technical programs:
A kind of analyzer, including measuring device and specimen cup, the measuring device include the temperature being arranged in specimen cup Sensor is spent, the measuring device further includes surrounding the semiconductor refrigerating module of specimen cup setting, and the measuring device further includes Metal bath, and the laser detection module for measuring cuvette sample light passing value.
It further, further include measurement body, the measurement is provided with solid thermal insulation medium in vivo, and the measuring device is set It sets at the middle part of thermal insulation medium.
Setting in this way, thermal insulation medium play the role of heat preservation to the inside of measurement body.
Further, the specimen cup includes test tube and the copper sheathing that is set in outside test tube, and the copper sheathing and measurement body are sliding The bottom of copper sheathing is arranged in dynamic connection, the metal bath.
Setting in this way, if cracking occurs for test tube, glass fragment broken at this time will not spluttering, avoid pair The case where operator damages improves the safety in utilization of specimen cup.
Further, the specimen cup further includes cup lid, is provided with locking member on the cup lid.
Setting in this way, in test, cup lid and locking member can be sealed processing to specimen cup, avoid outer The case where boundary's factor impacts specimen cup plays the effect of isolation to sample.
Further, it is provided with quick coupling on the cup lid, driving quick coupling is additionally provided on the cup lid and is carried out Close the electrically operated valve closed.
Setting in this way, can be added sample amount carry out stable control, whole setting so that specimen cup more Has practicability.
It further, further include host, the measurement body and host are rotatablely connected, and driving measurement is provided on the host The driving motor that body is rocked.
Setting in this way when driving motor works, can drive measurement body integrally to be rocked, such setting can rise To artificial hand effect is replaced, enable sample mixability more uniform.
Further, rubber mat, the bottom connection touching of the rubber mat and test tube are fixed in the copper sheathing.
Setting in this way, rubber mat play the role of protection to test tube.
Further, the quick coupling is connected with filling module.
Setting in this way, when filling sample into specimen cup by quick coupling using filling module, sample adds Dosage can obtain accurate numerical value, so that final testing result is more accurate.
Further, the filling module includes gas circuit switching station and peristaltic pump, and the gas circuit switching station is provided with defeated Air intake, output port and manipulation port, the input port is provided with gas source tank, manipulation port is connected with vacuum pump, institute It states peristaltic pump and is also provided with feed end and conveying end, the feed end is connected with storage tank.
Further, it is connected with flowmeter between the gas source tank and input terminal, connects between the vacuum pump and manipulation section It is connected to vacuum meter.
Utility model has the advantages that leading to when being measured using intermiscibility of the analyzer to lubricating oil and freon The regulation that semiconductor refrigeration module and metal bath carry out temperature to specimen cup is crossed, is supervised followed by temperature sensor and laser It surveys module to detect the sample being placed in specimen cup in real time, and by the data feedback of real-time detection at host, it is main Temperature of the machine to will test and light passing value at such a temperature are recorded, and are then run a curve according to the data of record Figure, find in the graph inflection point and by inflection point temperature and light passing value write down, to obtain determination data.It is high with energy The advantages of measuring solubility between refrigerant and corresponding refrigerator oil to effect.
Detailed description of the invention
Fig. 1 is the concrete structure diagram of the utility model;
Fig. 2 is the concrete structure diagram that module is filled in the utility model.
Appended drawing reference: 1, quick coupling;2, electrically operated valve;3, locking member;4, temperature sensor;5, test tube;6, copper sheathing;7, Thermal insulation medium;8, semiconductor refrigerating module;9, laser detection module;10, metal bath;11, rubber mat;12, safety exhaust;13, Display module;14, driving motor;15, rack;16, gas circuit switching station;17, peristaltic pump;18, vacuum pump;19, vacuum meter;20, Flowmeter;21, gas source tank;22, storage tank;23, balance.
Specific embodiment
The utility model is further described below in conjunction with attached drawing and specific embodiment:
A kind of analyzer, as shown in Figure 1 and Figure 2, including measurement body and host.Wherein measurement body includes measuring device And specimen cup.Analyzer in the present embodiment is used to measure the intermiscibility of lubricating oil and freon.Wherein, specimen cup includes examination Pipe 5 and the copper sheathing 6 being set in outside test tube 5 are provided with cup lid at the top of copper sheathing 6, while being provided on cup lid by copper sheathing 6 The locking member 3 of inner sealing.In addition quick coupling 1 is fixed at the top of cup lid, it, can be by fast when test tube 5 is sealed by cup lid Quick coupling 1 adds sample into test tube 5, while being equipped with driving quick coupling 1 on cup lid and carrying out closing the electrically operated valve 2 closed, borrows When helping quick coupling 1 that sample is added into test tube 5, closed by the conjunction that manipulation electrically operated valve 2 is controllable quick coupling 1, in this way 1 setting can be added sample amount carry out stable control, whole setting is so that specimen cup has more practicability.
More preferably, safety exhaust 12 is additionally provided on cup lid, safety exhaust 12 is by included digital pressure gauge control A pressure value, when the pressure value in copper sheathing 6 reaches preset level, safety exhaust is arranged when beginning to use in system in advance 12 can automatically open exhaust, and the pressure that the setting of safety exhaust 12 avoids in copper sheathing 6 is excessive, itself cause to damage to copper sheathing 6 It is bad, directly play the role of protection to specimen cup.
The inside for measuring body is filled with the thermal insulation medium 7 being arranged in solid-state, and the setting of thermal insulation medium 7 is to the inside for measuring body Play the role of heat preservation, in the present embodiment, thermal insulation medium 7 is foamed glue.It is equipped at the middle part of thermal insulation medium 7 and is put for copper sheathing 6 The cavity entered, while the aperture being embedded into thermal insulation medium 7 for 6 one end of copper sheathing is offered on measurement body, copper sheathing 6 passes through aperture It is slidably connected with measurement body.The setting being slidably connected enable the taking-up of specimen cup and be installed into it is more convenient, and in the process of measurement In, test tube 5 will do it the pressure change of a series of temperature change and inside, and the setting of copper sheathing 6 avoids teat glass 5 Fly the case where hurting sb.'s feelings outside fragment in cracking, the work for shielding and then playing to operator protection is played to test tube 5 With so that the use of equipment has more safety.
Measuring device includes temperature sensor 4 and laser detection module 9, wherein temperature sensor 4 is set with cup lid fixation It sets, and the measurement end of temperature sensor 4 extends into the bottom of test tube 5, data output end is in prominent cup lid setting.In thermal insulation medium The semiconductor refrigerating module 8 being arranged around copper sheathing 6 is fixed in 7, measuring device further includes the metal bath for being set in 6 bottom of copper sheathing 10, and metal bath 10 is equally fixedly connected with thermal insulation medium 7.Laser detection module 9 and thermal insulation medium 7 are in fixed setting, laser Detection module 9 is located at the top of metal bath 10, the bottom of copper sheathing 6 is arranged in.
When being measured using intermiscibility of the analyzer to lubricating oil and freon, by semiconductor refrigerating module 8 and Metal bath 10 carries out the regulation of temperature to specimen cup, followed by temperature sensor 4 and laser monitoring module to being placed on sample Sample in product cup is detected in real time, and by the data feedback of real-time detection at host, and host is to will test Temperature and light passing value at such a temperature are recorded, and are then run a curve figure according to the data of record, are looked in the graph To inflection point and by inflection point temperature and light passing value write down,
More preferably, the display module 13 of displays temperature measured value and laser measurement values is equipped on host.In addition in master Driving motor 14 is fixed on machine, symmetrical expression is fixed with shaft on measurement body two sides, and measurement body is rotated by shaft and host Connection, meanwhile, wherein a shaft and the output shaft of driving motor 14 are fixed to each other.When driving motor 14 works, survey can be driven Amount body is integrally rocked, and such setting, which can be played, replaces artificial hand effect, and enables sample mixability more equal It is even.
More preferably, filling module is connected in quick coupling 1.Filling module includes rack 15, fixed in rack 15 There are gas circuit switching station 16 and peristaltic pump 17.Wherein, gas circuit switching station 16 is equipped with input port, output port and manipulation gas Mouthful, input port is connected with gas source tank 21, manipulation port is connected with vacuum pump 18.In addition, peristaltic pump 17 also be equipped with feed end with And conveying end, storage tank 22 is connected on feed end.For the ease of real-time monitoring, connected between gas source tank 21 and input terminal There is flowmeter 20, while being connected with vacuum meter 19 between vacuum pump 18 and manipulation section.Filling module further includes balance 23, balance 23 setting enables the sample introduction more transparence of a whole filling process, enables staff that sample can be added in real time Amount is controlled.
Specific work process: when being measured, quantitative lubricating oil is added into specimen cup for manipulation peristaltic pump 17, covers cup Lid is sealed specimen cup, and subsequent staff vacuumizes specimen cup.At this time by the output on gas circuit switching station 16 Port is connected with quick coupling 1, quantitative freon is added into specimen cup by being manipulated to electrically operated valve 2, at this time sample The filling process of product terminates.
After filling, start driving motor 14, driving motor 14 drives measurement body integrally to be rocked, makes by shaft The sample obtained in test tube 5 is uniformly mixed.Then operation metal bath 10 and semiconductor refrigerating module 8, to the temperature in test tube 5 Degree is regulated and controled, and the temperature sensor 4 being now in test tube 5 will monitor in real time the temperature in test tube 5, simultaneously will The temperature detected passes through display module 13 in real time and shows.When carrying out laser detection to the sample in test tube 5, laser passes through Different light passing values is had after mixing sample, host records the light passing value under different temperatures at this time, to run a curve Figure then finds inflection point by curve graph and records corresponding temperature.
For those skilled in the art, it can be made various other equivalent according to above technical scheme and design Change and deforms, and all these change and modification all should belong within the protection scope of the utility model claims.

Claims (10)

1. a kind of analyzer, including measuring device and specimen cup, it is characterized in that: the measuring device include temperature sensor with And semiconductor refrigerating module, the temperature sensor are arranged in specimen cup, the semiconductor refrigerating module is set around specimen cup It sets, the measuring device further includes metal bath, and the laser detection module for measuring cuvette sample light passing value.
2. a kind of analyzer according to claim 1, it is characterized in that: further including measurement body, the measurement is provided in vivo The middle part of thermal insulation medium is arranged in solid thermal insulation medium, the measuring device.
3. a kind of analyzer according to claim 2, it is characterized in that: the specimen cup includes test tube and is set in test tube Outer copper sheathing, the copper sheathing are slidably connected with measurement body, and the bottom of copper sheathing is arranged in the metal bath.
4. a kind of analyzer according to claim 3, it is characterized in that: the specimen cup further includes cup lid, on the cup lid It is provided with locking member.
5. a kind of analyzer according to claim 4, it is characterized in that: quick coupling is provided on the cup lid, the cup Covering to be additionally provided with drives quick coupling to carry out closing the electrically operated valve closed.
6. a kind of analyzer according to claim 5, it is characterized in that: further including host, the measurement body and host are rotated It connects, the driving motor that driving measurement body is rocked is provided on the host.
7. a kind of analyzer according to claim 3, it is characterized in that: be fixed with rubber mat in the copper sheathing, the rubber mat with The bottom connection of test tube touches.
8. a kind of analyzer according to claim 5, it is characterized in that: the quick coupling is connected with filling module.
9. a kind of analyzer according to claim 8, it is characterized in that: the filling module includes gas circuit switching station and compacted Dynamic pump, the gas circuit switching station are provided with input port, output port and manipulation port, the input port and are provided with gas source Tank, manipulation port are connected with vacuum pump, and the peristaltic pump is also provided with feed end and conveying end, and the feed end is connected with Storage tank.
10. a kind of analyzer according to claim 9, it is characterized in that: being connected with stream between the gas source tank and input terminal Scale is connected with vacuum meter between the vacuum pump and manipulation section.
CN201822083970.9U 2018-12-12 2018-12-12 A kind of analyzer Active CN209231151U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201822083970.9U CN209231151U (en) 2018-12-12 2018-12-12 A kind of analyzer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201822083970.9U CN209231151U (en) 2018-12-12 2018-12-12 A kind of analyzer

Publications (1)

Publication Number Publication Date
CN209231151U true CN209231151U (en) 2019-08-09

Family

ID=67507326

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201822083970.9U Active CN209231151U (en) 2018-12-12 2018-12-12 A kind of analyzer

Country Status (1)

Country Link
CN (1) CN209231151U (en)

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