CN209188279U - A kind of sulfentrazone centrifugal dehydration system - Google Patents

A kind of sulfentrazone centrifugal dehydration system Download PDF

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Publication number
CN209188279U
CN209188279U CN201821546283.XU CN201821546283U CN209188279U CN 209188279 U CN209188279 U CN 209188279U CN 201821546283 U CN201821546283 U CN 201821546283U CN 209188279 U CN209188279 U CN 209188279U
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China
Prior art keywords
filter screen
sulfentrazone
connecting shaft
kettle cover
autoclave body
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Application number
CN201821546283.XU
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Chinese (zh)
Inventor
许小祥
徐慧
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Jiangsu Baozhong Baoda Pharmaceutical Co ltd
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JIANGSU BAOZONG BAODA PHARMACEUTICAL CO Ltd
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Priority to CN201821546283.XU priority Critical patent/CN209188279U/en
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Abstract

The utility model relates to a kind of sulfentrazone centrifugal dehydration systems, it is characterised in that: including autoclave body, kettle cover, connecting shaft, agitating shaft, agitating paddle, heating layer, stirring motor, centrifugation motor and filter screen;After mother liquor enters the interior paddle stirring by stirring of filter screen in the utility model, centrifugal pan is centrifuged, and the liquid across filter screen is flowed out by discharge port, then carries out heating, drying;It rethinks and solvent is added in filter screen, so that sulfentrazone dissolution is flowed out by liquid pumping hole negative pressure extraction exudation filter screen from liquid pumping hole in a solvent;Separation, drying and solvent dissolution in the elementary production steps of sulfentrazone are completed in the same apparatus, are not needed to carry out transfer exposure in air, have both been improved the production efficiency of sulfentrazone product, and in turn avoided environmental pollution.

Description

A kind of sulfentrazone centrifugal dehydration system
Technical field
The utility model relates to sulfentrazone manufacture field more particularly to a kind of sulfentrazone centrifugal dehydration systems.
Background technique
It include the separation of sulfentrazone in the production technology of sulfentrazone, drying, solvent dissolves these three steps, and one As need sulfentrazone after being separated in main ring object, need from separator to take out sulfentrazone then It is transferred in drying equipment and is dried, then carry out being displaced through DMF solvent and be dissolved;Multiple equipment is needed to carry out so each The volatilization that the operation of sample and sulfentrazone are often exposed to some powder in air is easy to cause air pollution.
Utility model content
The technical problem to be solved by the present invention is to provide a kind of sulfentrazone centrifugal dehydration system, can be realized general Sulfentrazone production in separation, dry and be dissolved in different equipment that carry out process redundancy complicated and have and largely wave The problem of hair causes air pollution in air.
In order to solve the above technical problems, the technical solution of the utility model are as follows: a kind of sulfentrazone centrifugal dehydration system, Innovative point is: including autoclave body, kettle cover, connecting shaft, agitating shaft, agitating paddle, heating layer, stirring motor, centrifugation motor and filtering Net;
The bottom face of the kettle cover is connected to the upper surface of autoclave body;Stepped connecting shaft mounting hole is provided on kettle cover; The upper surface of kettle cover is equipped with fixed stirring motor along vertical direction, and the output end of stirring motor protrudes into the connection in kettle cover In shaft mounting hole;The connecting shaft is mounted in the connecting shaft mounting hole of kettle cover, the upper end of connecting shaft and the output of stirring motor End is connected;The top of agitating shaft is connected with the bottom end of connecting shaft by flange;Connecting shaft drives under the driving of stirring motor and stirs Mix axis rotation;The agitating paddle is vertically connected on agitating shaft;Mother liquor import and solvent inlet are provided on the kettle cover;It is described Discharge port is set on the bottom face of autoclave body;
The autoclave body includes outer housing and inner housing, is formed between a receiving heating layer between the outer housing and inner housing Gap, the heating layer are arranged between outer housing and the gap of inner housing;Liquid pumping hole is provided on the side of the autoclave body;
The filter screen is in cylinder-shaped structure, and the outside of agitating paddle is arranged in filter screen, and the bottom end of filter screen is connected with one Centrifugal pan, the centrifugal pan extend the bottom end of autoclave body by a rotary shaft;The output end and rotary shaft phase of the centrifugation motor Even, rotary shaft drives centrifugation disc spins, to realize centrifugation.
Further, the heating layer is that several heating module units are formed by connecting.
Further, phase is cooperated by single-revolution axis and connection sheet between the top of the filter screen and the inner wall of inner housing Even.
Further, the mother liquor import and solvent inlet are respectively positioned on the inside front of filter screen.
Utility model has the advantages that
1) after mother liquor enters the interior paddle stirring by stirring of filter screen in the utility model, centrifugal pan is centrifuged, and is passed through The liquid of strainer is flowed out by discharge port, then carries out heating, drying;It rethinks and solvent is added in filter screen, so that sulfentrazone is molten Solution passes through liquid pumping hole negative pressure extraction exudation filter screen in a solvent and flows out from liquid pumping hole;In the elementary production steps of sulfentrazone Separation, drying and solvent dissolution are completed in the same apparatus, are not needed to carry out transfer exposure in air, are both improved methylsulphur The production efficiency of careless amine product, in turn avoids environmental pollution.
Detailed description of the invention
Utility model will be further described in detail below with reference to the attached drawings and specific embodiments.
Fig. 1 is a kind of structural schematic diagram of sulfentrazone centrifugal dehydration system of the utility model.
Specific embodiment
The following examples can make professional and technical personnel that the utility model be more fully understood, but therefore will not The utility model is limited among the embodiment described range.
A kind of sulfentrazone centrifugal dehydration system as shown in Figure 1, including autoclave body 1, kettle cover 2, connecting shaft 3, agitating shaft 4, Agitating paddle 5, heating layer 6, stirring motor 7, centrifugation motor 8 and filter screen 9.
The bottom face of kettle cover 2 is connected to the upper surface of autoclave body 1;Stepped 3 mounting hole of connecting shaft is provided on kettle cover 2; The upper surface of kettle cover 2 is equipped with fixed stirring motor 7 along vertical direction, and the output end of stirring motor 5 is protruded into kettle cover 2 In 3 mounting hole of connecting shaft;The connecting shaft 3 is mounted in 3 mounting hole of connecting shaft of kettle cover 2, the upper end of connecting shaft 3 and stirring electricity The output end of machine 7 is connected;The top of agitating shaft 4 is connected with the bottom end of connecting shaft 3 by flange;Connecting shaft 3 is in stirring motor 7 Driving is lower to drive agitating shaft 4 to rotate;The agitating paddle 5 is vertically connected on agitating shaft 4;Be provided on the kettle cover 2 mother liquor into Mouth and solvent inlet;Discharge port 13 is set on the bottom face of the autoclave body 1.
Autoclave body 1 includes outer housing 11 and inner housing 12, forms one between the outer housing 11 and inner housing 12 and accommodates heating The gap of layer 6, the heating layer 6 are arranged between outer housing 11 and the gap of inner housing 12;It is arranged on the side of the autoclave body 1 There is liquid pumping hole 14.
Filter screen 9 is in cylinder-shaped structure, and the outside of agitating paddle 5 is arranged in filter screen 9, and the bottom end of filter screen 9 is connected with one Centrifugal pan 81, the centrifugal pan 81 extend the bottom end of autoclave body 1 by a rotary shaft;The output end of the centrifugation motor 8 and rotation Shaft is connected, and rotary shaft drives centrifugal pan 81 to rotate, to realize centrifugation.
Heating layer 6 is that several heating module units are formed by connecting.
It is connected between the top of filter screen 9 and the inner wall of inner housing by single-revolution axis and connection sheet cooperation.
Mother liquor import and solvent inlet are respectively positioned on the inside front of filter screen 9.
It should be understood by those skilled in the art that the present utility model is not limited to the above embodiments, above-described embodiment and Only illustrate the principles of the present invention described in specification, on the premise of not departing from the spirit and scope of the utility model, The utility model also has various changes and improvements, these changes and improvements both fall within the scope of the claimed invention It is interior.The protection scope of the present invention is defined by the appended claims and their equivalents.

Claims (4)

1. a kind of sulfentrazone centrifugal dehydration system, it is characterised in that: including autoclave body, kettle cover, connecting shaft, agitating shaft, agitating paddle, Heating layer, stirring motor, centrifugation motor and filter screen;
The bottom face of the kettle cover is connected to the upper surface of autoclave body;Stepped connecting shaft mounting hole is provided on kettle cover;Kettle cover Upper surface fixed stirring motor is installed along vertical direction, the output end of stirring motor protrudes into the connecting shaft peace in kettle cover It fills in hole;The connecting shaft is mounted in the connecting shaft mounting hole of kettle cover, the upper end of connecting shaft and the output end phase of stirring motor Even;The top of agitating shaft is connected with the bottom end of connecting shaft by flange;Connecting shaft drives agitating shaft under the driving of stirring motor Rotation;The agitating paddle is vertically connected on agitating shaft;Mother liquor import and solvent inlet are provided on the kettle cover;The autoclave body Bottom face on discharge port is set;
The autoclave body includes outer housing and inner housing, and a gap for accommodating heating layer is formed between the outer housing and inner housing, The heating layer is arranged between outer housing and the gap of inner housing;Liquid pumping hole is provided on the side of the autoclave body;
The filter screen is in cylinder-shaped structure, and the outside of agitating paddle is arranged in filter screen, and the bottom end of filter screen is connected with a centrifugation Disk, the centrifugal pan extend the bottom end of autoclave body by a rotary shaft;The output end of the centrifugation motor is connected with rotary shaft, revolves Shaft drives centrifugation disc spins, to realize centrifugation.
2. a kind of sulfentrazone centrifugal dehydration system according to claim 1, it is characterised in that: the heating layer is several Heating module unit is formed by connecting.
3. a kind of sulfentrazone centrifugal dehydration system according to claim 1, it is characterised in that: the top of the filter screen It is connected between the inner wall of inner housing by single-revolution axis and connection sheet cooperation.
4. a kind of sulfentrazone centrifugal dehydration system according to claim 1, it is characterised in that: the mother liquor import and molten Agent import is respectively positioned on the inside front of filter screen.
CN201821546283.XU 2018-09-21 2018-09-21 A kind of sulfentrazone centrifugal dehydration system Active CN209188279U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821546283.XU CN209188279U (en) 2018-09-21 2018-09-21 A kind of sulfentrazone centrifugal dehydration system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821546283.XU CN209188279U (en) 2018-09-21 2018-09-21 A kind of sulfentrazone centrifugal dehydration system

Publications (1)

Publication Number Publication Date
CN209188279U true CN209188279U (en) 2019-08-02

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CN201821546283.XU Active CN209188279U (en) 2018-09-21 2018-09-21 A kind of sulfentrazone centrifugal dehydration system

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111871049A (en) * 2020-08-24 2020-11-03 江西智联塑化科技有限公司 Wasabramide behenate purification device
CN115388628A (en) * 2022-08-01 2022-11-25 贵州海福农业发展有限公司 Dewatering device for preparing konjac glucomannan

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111871049A (en) * 2020-08-24 2020-11-03 江西智联塑化科技有限公司 Wasabramide behenate purification device
CN111871049B (en) * 2020-08-24 2023-08-08 江西智联新材料有限公司 Wasabia acid amide purification device
CN115388628A (en) * 2022-08-01 2022-11-25 贵州海福农业发展有限公司 Dewatering device for preparing konjac glucomannan
CN115388628B (en) * 2022-08-01 2024-02-09 贵州海福农业发展有限公司 Dewatering device for preparing konjak gum

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Address after: 226500 No.10, Yuejiang Road, Changjiang Town, Rugao City, Nantong City, Jiangsu Province

Patentee after: Jiangsu Baozhong Baoda Pharmaceutical Co.,Ltd.

Address before: 226500 No.10, Yuejiang Road, Changjiang Town, Rugao City, Nantong City, Jiangsu Province

Patentee before: JIANGSU BAOZONG & BAODA PHARMACHEM Co.,Ltd.