CN209132195U - A kind of full-automatic testing calorimeter - Google Patents
A kind of full-automatic testing calorimeter Download PDFInfo
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- CN209132195U CN209132195U CN201821606894.9U CN201821606894U CN209132195U CN 209132195 U CN209132195 U CN 209132195U CN 201821606894 U CN201821606894 U CN 201821606894U CN 209132195 U CN209132195 U CN 209132195U
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Abstract
The utility model discloses a kind of full-automatic testing calorimeters, including oxygen bomb automatic lid closing/opening closing lid device, for carrying out automatic lid closing/opening or automatic cover closing operation to oxygen bomb lid on oxygen bomb；Oxygen bomb automatic oxygenation device, for carrying out automatic oxygenation operation to oxygen bomb；Oxygen bomb automatic watering apparatus, for being automatically added to quantitative water into oxygen bomb；Oxygen bomb core, which pulls out, puts component, for extracting oxygen bomb core out of oxygen bomb ontology automatically or oxygen bomb core being put into oxygen bomb ontology；Thermal value measurement device, for carrying out thermal value measurement to the sample in the crucible in oxygen bomb；With oxygen bomb auto transferring device, for realizing the circulation of oxygen bomb between each device.The calorimeter of the utility model has many advantages, such as high degree of automation.
Description
Technical field
The utility model relates generally to sample assay technique field, refers in particular to a kind of full-automatic testing calorimeter.
Background technique
Calorimeter is the instrument for measuring the combustibles calorific value such as various solid-states, liquid, mainly by outer cylinder, inner cylinder and oxygen
The composition such as bullet, measures its calorific value by burning of the combustible in oxygen bomb.The calorimeter of Vehicles Collected from Market requires
Manual operation manually prepares oxygen bomb, and artificial oxygen supply flicks lid, manually adds water to oxygen bomb, manually puts crucible, manually ties up ignition wire,
It is manually covered to oxygen bomb, artificial oxygenation manually enters oxygen bomb in calorimeter and carries out, manual entry coal sample weight, and calorimeter is automatic
Experiment is completed, after the completion of experiment, manually oxygen bomb is filled in calorimeter and is taken out, manually exhaust gas in oxygen bomb is bled off, is manually uncapped,
Crucible is manually taken out cleaning, manual cleaning oxygen bomb.The above work is all manually to carry out, and there are problems: 1, low efficiency；2, labor
Fatigue resistance is big；3, the degree of automation is low；4, manpower intervention, it is understood that there may be the possibility of Human disturbance experimental result.
Utility model content
The technical problems to be solved in the utility model is that for technical problem of the existing technology, this is practical new
Type provides that a kind of structure is simple, full-automatic testing calorimeter of high degree of automation.
In order to solve the above technical problems, the utility model proposes technical solution are as follows:
A kind of full-automatic testing calorimeter, including
Oxygen bomb automatic lid closing/opening closing lid device, for carrying out automatic lid closing/opening or automatic cover closing operation to oxygen bomb lid on oxygen bomb；
Oxygen bomb automatic oxygenation device, for carrying out automatic oxygenation operation to oxygen bomb；
Oxygen bomb automatic watering apparatus, for being automatically added to quantitative water into oxygen bomb；
Oxygen bomb core, which pulls out, puts component, for extracting oxygen bomb core out of oxygen bomb ontology automatically or oxygen bomb core being put into oxygen bomb sheet
In vivo；
Thermal value measurement device, for carrying out thermal value measurement to the sample in the crucible in oxygen bomb；With
Oxygen bomb auto transferring device, for realizing the circulation of oxygen bomb between each device.
As a further improvement of the above technical scheme:
It further include oxygen bomb automatic air eliminator, for automatically bleeding off the gas in oxygen bomb before uncapping.
It further include oxygen bomb automatic flushing device, for being cleaned automatically to oxygen bomb ontology.
It further include oxygen bomb storing unit, for storing oxygen bomb.
It further include oxygen bomb device for aligning, for the crucible of oxygen bomb in-core to be corrected to pre-configured orientation.
Further include that crucible picks and places component, carries out pick-and-place operation for the crucible automatically to oxygen bomb in-core.
The thermal value measurement device, oxygen bomb automatic oxygenation device, oxygen bomb automatic watering apparatus, oxygen bomb automatic lid closing/opening closing lid dress
Set pulled out with oxygen bomb core put component be respectively positioned in a shell and successively linearly or annular configuration；When each device is linearly arranged,
The oxygen bomb auto transferring device is slidedly arranged on the side of each device；When each device is annularly arranged, the oxygen bomb shifts automatically
Device is slidedly arranged on the ring side of each device.
It further include crucible auto transferring device, for realizing the transfer of crucible between device each in shell and outside.
The quantity of the thermal value measurement device is multiple.
The oxygen bomb automatic air eliminator includes deflation formed punch and the first lifting assembly；The deflation formed punch is installed on described
On first lifting assembly and the oscilaltion under the driving of first lifting assembly；The bottom opening of the deflation formed punch is used
In the oxygen bomb head peripheral side covered in oxygen bomb and form all side seals；Exhaust passage and bottom end end face are equipped with inside the deflation formed punch
On be provided with thimble of the bullet core for opening the oxygen bomb to deflate.
The deflation formed punch includes deflation head and sealing fixing head, and the deflation head is installed on first lifting assembly
On, the sealing fixing head is removably mounted to the bottom of the deflation head.
The sealing fixing head includes interconnecting piece and clamping part, forms ring-shaped step between the interconnecting piece and clamping part；
It is threadedly coupled between the interconnecting piece and the deflation head, ring is installed between the bottom end end face of the ring-shaped step and deflation head
Shape sealing element forms all side seals in oxygen bomb head peripheral side to cover.
The oxygen bomb automatic oxygenation device includes oxygenation formed punch and the second lifting assembly；The oxygenation formed punch is installed on described
On second lifting assembly and the oscilaltion under the driving of second lifting assembly；The bottom of the oxygenation formed punch, which is equipped with, opens
Mouthful, the oxygen bomb head peripheral side in oxygen bomb is covered when for declining and forms all side seals；It is logical that inflation is equipped with inside the oxygenation formed punch
Road；The oxygenation formed punch is connected with source of oxygen by gas ducting in one end of filling channel.
Switch block and the pressure detecting part for detecting oxygen pressure are provided on the gas ducting.
It further include fixation kit and Anchor plate kit；The fixation kit is used to oxygen bomb ontology being fixed on predetermined position；Institute
Stating Anchor plate kit includes pressing plate and third lifting assembly, and the pressing plate is installed on the movable end of third lifting assembly, for pushing down
The side of crucible tray simultaneously moves down so that crucible avoids the fire rod on oxygen bomb core.
The oxygen bomb core pulls out that put component include hanging support plate and the 4th lifting assembly, and the hanging support plate is installed on described 4th liter
Come down to a lower group the movable end of part, the hanging support plate for tangle oxygen bomb head and under the driving of the 4th lifting assembly to oxygen bomb core carry out from
Dynamic pull out is put.
It includes the first translation unit, bracket and locating slot that the crucible, which picks and places component,；One end of the bracket and described the
The movable end of one translation unit is connected, and the locating slot is installed on the other end of the bracket.
Further include that oxygen bomb core holds down assembly, for before oxygen bomb core is chosen by oxygen bomb core be pressed on oxygen bomb ontology so as to
It is pulled out in oxygen bomb core and puts component and reliably tangle oxygen bomb head.
The oxygen bomb core holds down assembly including compact heap and the 5th lifting assembly, and the compact heap is installed on described 5th liter
It comes down to a lower group the movable end of part, so that oxygen bomb core is pressed on oxygen bomb for covering oxygen bomb head and pushing under the driving of the 5th lifting assembly
On ontology.
The oxygen bomb device for aligning includes correction formed punch, third rotary components and the 6th lifting assembly；The correction
The bottom opening of formed punch, the opening are equipped with the correction boss to match with the correction notch of oxygen bomb；The correction formed punch peace
Loaded on the third rotary components, and rotated under the driving of third rotary components；The third rotary components are installed on institute
It states on the 6th lifting assembly, and the oscilaltion under the driving of the 6th lifting assembly.
The oxygen bomb automatic flushing device includes fixed cell, lifting rotation component and cleaning assembly；The fixed cell,
For oxygen bomb to be fixed on cleaning positions；The cleaning assembly is installed on the lifting rotation component, and is revolved in the lifting
Under the driving for turning component, stretches in oxygen bomb and rotate to carry out washing and cleaning operation to oxygen bomb.
The cleaning assembly includes hollow brush holder support, and the side of the brush holder support is provided with bristle；The bottom of the brush holder support is sealed
It closes and top end opening, and side is provided with multiple apopores communicated with internal cavities, the opening at the top of the brush holder support is connected with
Add water assembly.
Compared with the prior art, the advantages of the utility model are:
The full-automatic testing calorimeter of the utility model by configuring the device of each automatic operating, and passes through oxygen bomb
Auto transferring device realizes the circulation of oxygen bomb between each device, realizes oxygen bomb processing automation, is automatically performed the calorific value of sample
Test, high degree of automation, high-efficient and measuring accuracy are high.
Oxygen bomb automatic air eliminator in the full-automatic testing calorimeter of the utility model is driven by the first lifting assembly
Deflation formed punch or oxygen bomb oscilaltion make sealing fixing head entangle the side of oxygen bomb head to form all side seals, gas are avoided to let out
Leakage, then opens the bullet core of oxygen bomb by thimble to deflate；Structure is simple, high degree of automation and is not easy to leak.
Oxygen bomb automatic oxygenation device in the full-automatic testing calorimeter of the utility model is driven by the second lifting assembly
It is oxygenated formed punch or oxygen bomb oscilaltion, so that sealing fixing head is entangled the side of oxygen bomb head to form all side seals, gas is avoided to let out
Whether leakage, then carry out oxygenation operation to oxygen bomb, close additionally by the cooperation of pressure detecting part and switch block to oxygenate pressure
Lattice are judged；Structure is simple, is oxygenated high degree of automation and good airproof performance.
Oxygen bomb automatic correction device in the full-automatic testing calorimeter of the utility model passes through the correction in correction formed punch
Boss is caught in correction notch, is able to drive oxygen bomb and rotates to predetermined position, so as to guarantee the oxygen bomb core taken out out of oxygen bomb
Upper bushing position is respectively positioned on same orientation, consequently facilitating other automechanisms such as manipulator carry out crucible the work such as to pick and place, mentions
High the degree of automation.
Oxygen bomb automatic flushing device in the full-automatic testing calorimeter of the utility model passes through liter when being cleaned
Drop driving of the rotary components to cleaning assembly, stretch to its decline inside oxygen bomb, then rotated again, thus to oxygen bomb into
Row washing and cleaning operation；Structure is simple, it is easy to operate, independent oxygen bomb can be cleaned, improve the degree of automation.
Oxygen bomb core in the full-automatic testing calorimeter of the utility model, which pulls out, puts device, tangles oxygen bomb by hanging support component
Head, then by the driving of lifting cylinder, pulling out automatically for oxygen bomb core can be realized and put, structure is simple, easy to operate, the degree of automation
It is high.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model.
Fig. 2 is the structural schematic diagram of oxygen bomb automatic air eliminator in the utility model.
Fig. 3 is the structural schematic diagram of oxygen bomb automatic oxygenation device in the utility model.
Fig. 4 is the structural schematic diagram of crucible automatic processing device in the utility model.
Fig. 5 is the structural schematic diagram that Anchor plate kit and crucible pick and place component in the utility model.
Fig. 6 is the structural schematic diagram of oxygen bomb device for aligning in the utility model.
Fig. 7 is the structural schematic diagram of oxygen bomb automatic flushing device in the utility model.
Fig. 8 is the test flow chart in the utility model before test and in test.
Fig. 9 is the test flow chart after testing in the utility model.
Figure label indicates: 1, thermal value measurement device；2, oxygen bomb automatic air eliminator；21, the first lifting assembly；22, it puts
Gas formed punch；2201, deflation head；22011, exhaust passage；2202, fixing head is sealed；2203, sealing element；2204, thimble；3, oxygen
Play automatic oxygenation device；31, it is oxygenated component；3101, pressure detecting part；3102, valve body；3103, switch block；3104, oxygen
Source；32, it is oxygenated formed punch；33, the second lifting assembly；4, oxygen bomb automatic watering apparatus；5, oxygen bomb automatic flushing device；51, second
Rotary components；52, lifting rotation component；5201, the first rotary components；5202, the first lifting unit；53, cleaning assembly；
5301, brush holder support；5302, bristle；5303, apopore；54, add water assembly；6, oxygen bomb device for aligning；61, formed punch is corrected；
6101, boss is corrected；62, the 6th lifting assembly；63, third rotary components；7, oxygen bomb automatic lid closing/opening closing lid device；8, crucible from
Dynamic processing unit；81, oxygen bomb core holds down assembly；8101, compact heap；8102, the 5th lifting assembly；82, oxygen bomb core, which pulls out, puts component；
8201, hanging support plate；83, Anchor plate kit；8301, pressing plate；84, crucible picks and places component；8401, bracket；8402, locating slot；8403,
First translation unit；85, component is consolidated；8501, mounting bracket；8502, positioning column；9, crucible auto transferring device；10, oxygen bomb
Auto transferring device；11, shell；12, oxygen bomb；1201, oxygen bomb ontology；1202, oxygen bomb head；1203, oxygen bomb core；1204, oxygen bomb
Lid；13, oxygen bomb storing unit.
Specific embodiment
The utility model is further described below in conjunction with Figure of description and specific embodiment.
As shown in Figure 1, the full-automatic testing calorimeter of the present embodiment, including oxygen bomb automatic lid closing/opening closing lid device 7, for pair
Oxygen bomb lid 1204 carries out automatic lid closing/opening or automatic cover closing operation on oxygen bomb 12；Oxygen bomb automatic oxygenation device 3, for oxygen bomb 12 into
Row automatic oxygenation operation；Oxygen bomb automatic watering apparatus 4, for being automatically added to quantitative water into oxygen bomb 12；Crucible automatically processes
Device 8, including oxygen bomb core pull out and put component 82, for automatically extracting out of oxygen bomb ontology 1201 oxygen bomb core 1203 or by oxygen bomb core
1203 are put into oxygen bomb ontology 1201；Thermal value measurement device 1, for carrying out thermal value measurement to the sample in crucible；And oxygen bomb
Auto transferring device 10, for realizing the circulation of oxygen bomb 12 between each device.The full-automatic testing calorimeter of the utility model,
By configuring the device of above each automatic operating, and by oxygen bomb auto transferring device 10 realize oxygen bomb 12 each device it
Between circulation, realize oxygen bomb 12 processing automation, be automatically performed the thermal value measurement of sample.
It further include oxygen bomb storing unit 13, oxygen bomb device for aligning 6 and oxygen bomb automatic flushing device 5 in the present embodiment,
Wherein oxygen bomb storing unit 13 is for storing oxygen bomb 12；Oxygen bomb device for aligning 6 is for rectifying the crucible in oxygen bomb core 1203
Just to pre-configured orientation；Oxygen bomb automatic flushing device 5, for being cleaned to oxygen bomb ontology 1201.
In the present embodiment, crucible automatic processing device 8 further includes that crucible picks and places component 84 and oxygen bomb automatic air eliminator 2；
Crucible picks and places component 84, for carrying out pick-and-place operation to the crucible in oxygen bomb core 1203 automatically；Oxygen bomb automatic air eliminator 2 is used
The gas in oxygen bomb 12 is bled off automatically in front of uncapping, guarantees that oxygen bomb 12 is in deflation status before uncapping, guarantees test
The safety of work.
In the present embodiment, thermal value measurement device 1, oxygen bomb storing unit 13, oxygen bomb automatic air eliminator 2, oxygen bomb fill automatically
Oxygen device 3, oxygen bomb automatic watering apparatus 4, oxygen bomb automatic flushing device 5, oxygen bomb device for aligning 6, oxygen bomb automatic lid closing/opening close
Lid arrangement 7 and crucible automatic processing device 8 are respectively positioned in a shell 11 and successively linearly or annular configuration, wherein thermal value measurement
The quantity of device 1 is four；When each device is linearly arranged, oxygen bomb auto transferring device 10 is slidedly arranged on the side of each device；
When each device is annularly arranged, oxygen bomb auto transferring device 10 is slidedly arranged on the ring side of each device.It is set between inside and outside the shell 11
Be equipped with crucible auto transferring device 9, for realizing in shell 11 between each device and outside crucible transfer.In addition, other
In embodiment, the other shapes such as at L-shaped are also can be set in each device.
As shown in Fig. 2, oxygen bomb automatic air eliminator 2 includes deflation formed punch 22 and the first lifting assembly 21；Deflation formed punch 22
Including deflation head 2201 and sealing fixing head 2202, sealing fixing head 2202 is removably mounted to the bottom of deflation head 2201, uses
In 1202 peripheral side of oxygen bomb head covered in oxygen bomb 12 and form all side seals；Upper and lower perforative exhaust is equipped with inside deflation head 2201
Thimble 2204 is provided on channel 22011 and bottom end end face, the first lifting assembly 21 is connected with deflation formed punch 22 or oxygen bomb 12,
For driving deflation formed punch 22 or oxygen bomb 12 to move up and down；When being deflated, deflation head 2201 and sealing fixing head 2202
Entire lowering makes sealing fixing head 2202 entangle the side of oxygen bomb head 1202 to form all side seals, then passes through thimble 2204
The bullet core of oxygen bomb 12 is opened to deflate, the gas of releasing is expelled to collection box (or other fingers through exhaust passage 22011 again
Determine device) it is handled；Structure is simple, high degree of automation and is not easy to leak.Certainly, in other embodiments, can also lead to
It crosses lifting cylinder and is gone up and down lifting to replace deflation formed punch 22 to oxygen bomb 12.
In the present embodiment, sealing fixing head 2202 includes interconnecting piece and clamping part, and ring is formed between interconnecting piece and clamping part
Shape step；Wherein interconnecting piece and deflation head 2201 (specially set axis) are detachably connected and (such as are threadedly coupled), ring-shaped step and
Lip ring 2203 is equipped between the bottom end end face of deflation head 2201, it is close in 1202 peripheral side of oxygen bomb head formation side to cover
Envelope.In addition, the tapered shape of the inner opening of clamping part or arc shape, convenient for the alignment with oxygen bomb head 1202；Deflation head 2201
Connector is arranged in top, and connector then connects one end of atmospheric pipe 206, and the other end of atmospheric pipe is connected with collection box.
As shown in figure 3, oxygen bomb automatic oxygenation device 3 includes oxygenation formed punch 32 and the second lifting assembly 33；It is oxygenated formed punch 32
Including oxygenation head and sealing fixing head 2202 (identical as the sealing fixing head 2202 of oxygen bomb automatic air eliminator 2), the second lifting
Component 33 is connected with oxygenation formed punch 32 or oxygen bomb 12, driving oxygenation formed punch 32 or 12 oscilaltion of oxygen bomb；Seal fixing head
2202 are removably mounted to the bottom of oxygenation head, and 1202 peripheral side of oxygen bomb head in oxygen bomb 12 is covered when for declining and forms side
Sealing；It is oxygenated inside head and is equipped with upper and lower perforative filling channel；Head is oxygenated to connect in one end of filling channel by gas ducting
There is oxygenation component 31, specifically includes source of oxygen 3104, switch block 3103 and pressure detecting part 3101, switch block 3103 and use
It is arranged on gas ducting in the pressure detecting part 3101 of detection oxygen pressure, specifically, pressure detecting part 3101 passes through valve body
3102 are mounted on gas ducting, and source of oxygen 3104 is then connected with one end of gas ducting.When carrying out oxygenation operation, it is oxygenated head
With sealing 2202 entire lowering of fixing head, sealing fixing head 2202 is made to entangle the side of oxygen bomb head 1202 and form all side seals,
Then source of oxygen 3104 enters in oxygen bomb 12 through gas ducting, oxygenation head, oxygen bomb head 1202 and bullet core；In oxygenation a period of time
Afterwards, switch block 3103 disconnects, and is no longer oxygenated, and pressure detecting part 3101 detects the oxygen in oxygen bomb 12- gas ducting circuit at this time
Atmospheric pressure, if circuit pressure value is maintained within a predetermined range within a certain period of time, then oxygenation terminates.Pass through the second lifting assembly 33
Oxygenation 32 oscilaltion of formed punch is driven, so that sealing fixing head 2202 is entangled the side of oxygen bomb head 1202 to form all side seals, keeps away
Exempt from gas leakage, oxygenation operation then is carried out to oxygen bomb 12, additionally by matching for pressure detecting part 3101 and switch block 3103
Close whether qualification judges to oxygenate pressure；Structure is simple, high degree of automation and good airproof performance.
As shown in Figure 4 and Figure 5, crucible automatic processing device 8 pulls out including fixation kit, oxygen bomb core and puts component 82, pressing plate group
Part 83 and crucible pick and place component 84；Fixation kit (puts oxygen bomb core for pulling out for oxygen bomb ontology 1201 to be fixed on predetermined position
1203 position)；Oxygen bomb core, which pulls out, puts the top that component 82 is installed on predetermined position, for tangling oxygen bomb head 1202 and oscilaltion
Pull out putting to oxygen bomb core 1203, hanging support plate 8201 and lifting cylinder are specifically included, hanging support plate 8201 is installed on lifting cylinder
Movable end, hanging support plate 8201 is for tangling oxygen bomb head 1202 and carry out automatically under the driving of lifting cylinder to oxygen bomb core 1203
It pulls out and puts；Anchor plate kit 83 includes pressing plate 8301 and lifting cylinder, and pressing plate 8301 is installed on the movable end of lifting cylinder, for pushing down
The side of crucible tray simultaneously moves down so that crucible avoids the fire rod on oxygen bomb core 1203；Crucible picks and places component 84 and is used under
Crucible on the crucible tray of shifting carries out pick-and-place operation.It is pulled out by oxygen bomb core and puts the realization of component 82 pulling out automatically to oxygen bomb core 1203
It puts, then crucible tray is moved to by suitable position by Anchor plate kit 83, crucible picks and places component 84 and then carries out to crucible on crucible tray
Operation is picked and placed, it includes the first translation unit 8403, bracket 8401 and locating slot 8402 that wherein crucible, which picks and places component 84,；Bracket 8401
One end be connected with the movable end of the first translation unit 8403, locating slot 8402 is installed on the other end of bracket 8401, structure letter
It is single, easy to operate；Overall structure is simple, easy to operate and high degree of automation.
Further include that oxygen bomb core holds down assembly 81 in the present embodiment, for before oxygen bomb core 1203 is chosen by oxygen bomb core
1203 are pressed on oxygen bomb ontology 1201 and put component 82 in order to which oxygen bomb core pulls out and reliably tangle oxygen bomb head 1202.Specifically, oxygen bomb
It 81 includes the compact heap 8101 to match with oxygen bomb head 1202 and the 5th lifting assembly 8102 (such as lifting cylinder) that core, which holds down assembly,
Compact heap 8101 is installed on the movable end of the 5th lifting assembly 8102, for covering oxygen bomb head 1202 and in the 5th lifting assembly
It pushes under 8102 driving and is pressed on oxygen bomb core 1203 on oxygen bomb ontology 1201, make the annular groove of 1202 side of oxygen bomb head
It is pulled out with subsequent oxygen bomb core and puts 82 flush of component, consequently facilitating the hanging support to oxygen bomb head 1202, structure is simple, improves subsequent oxygen
The reliability of 1202 hanging support of bullet.
In the present embodiment, due to oxygen bomb core 1203 pull out put or shift during, it may appear that the case where rocking, because
This is additionally provided with the firm component 85 for keeping horizontal stability during hanging support of oxygen bomb core 1203.Specifically, component is consolidated
85 include lifting cylinder, mounting bracket 8501 and multiple positioning columns 8502；Mounting bracket 8501 is installed on third lifting unit
One end of movable end, multiple positioning columns 8502 is installed in mounting bracket 8501, the other end then with the cover board phase of oxygen bomb head 1202
It supports, so as to limit rocking for oxygen bomb core 1203, improves reliability.
As shown in fig. 7, oxygen bomb automatic flushing device 5 includes lifting rotation component 52 and cleaning assembly 53；Cleaning assembly 53,
It is installed on lifting rotation component 52, and under the driving of lifting rotation component 52, stretches in oxygen bomb 12 and rotates to oxygen
Bullet 12 carries out washing and cleaning operation.When being cleaned, driving by lifting rotation component 52 to cleaning assembly 53 stretches its decline
Enter to oxygen bomb 12, then rotated again, to carry out washing and cleaning operation to oxygen bomb 12；Structure is simple, it is easy to operate, can
Independent oxygen bomb 12 is cleaned, the degree of automation is improved.
In the present embodiment, oxygen bomb automatic watering apparatus 4, which can choose, is independent priming apparatus, can choose with oxygen bomb certainly
Dynamic cleaning device 5 is integrated；Specifically: cleaning assembly 53 includes cleaning brush, specifically includes brush holder support 5301 and bristle 5302, bristle
5302 are distributed in the side of brush holder support 5301.Wherein it is multiple with internal cavities phase to be that hollow brush holder support and side are provided with for brush holder support 5301
Logical apopore 5303 (or effluent trough etc.), in addition the bottom end closure of brush holder support 5301, the top end opening of brush holder support 5301, opening then connect
It is connected to and adds water assembly 54.Adding water assembly 54 includes filler pipe, make-up water pump and water source；One end of filler pipe is connected with make-up water pump, adds
The other end of water pipe is connected by being oriented to connector with brush holder support 5301, and water source is connected with make-up water pump.Inside cleaning brush is to oxygen bomb 12
While cleaning, water source passes sequentially through make-up water pump, filler pipe, brush holder support 5301 and enters in oxygen bomb 12, and realization automatically adds water,
Improve cleaning efficiency and effect；It is integrated in same device with water is added due to that will clean, integrated level is high, it is automatic to further improve
Change degree.
In the present embodiment, lifting rotation component 52 includes the first lifting unit 5202 and the first rotary components 5201；Cleaning
Component 53 is installed on the first rotary components 5201, and the first rotary components 5201 are installed on the first lifting unit 5202.Wherein
First lifting unit 5202 is lifting cylinder, and the first rotary components 5201 are rotary cylinder etc.；Specifically, the first lifting unit
5202 include lifting cylinder and lifting support, and lifting cylinder drives lifting support oscilaltion, and wherein brush holder support 5301 passes through first
Lifting support is stretched out again after rotary components 5201, is connected by guiding connector with filler pipe.In addition, second rotation of the installation of oxygen bomb 12
On component 51, after cleaning, drives oxygen bomb 12 to rotate by the second rotary components 51, the sewage in oxygen bomb 12 is poured out.
As shown in fig. 6, oxygen bomb device for aligning 6 includes correction formed punch 61, third rotary components 63 and the 6th lifting group
Part 62；The bottom opening of formed punch 61 is wherein corrected, opening is equipped with the correction boss to match with the correction notch of oxygen bomb 12
6101；Correction formed punch 61 is installed on third rotary components 63, and is rotated under the driving of third rotary components 63；Third rotation
Component 63 is installed on the 6th lifting assembly 62, and the oscilaltion under the driving of the 6th lifting assembly 62.When in use, pass through
6th lifting assembly 62 drives correction formed punch 61 to decline, and makes opening sleeve on oxygen bomb head 1202, then passes through third rotary components
63 rotational correction formed punches 61 make correction boss 6101 be caught in correction notch, thus band so that correction formed punch 61 is pushed in rotation
Dynamic oxygen bomb 12 is rotated to predetermined position.It is caught in correction notch by the correction boss 6101 in correction formed punch 61, is able to drive oxygen
Bullet 12 is rotated to predetermined position, so as to guarantee that bushing position is respectively positioned on same side on the bullet core taken out out of oxygen bomb 12
Position, consequently facilitating other automechanisms such as manipulator carry out crucible the work such as to pick and place.
In the present embodiment, crucible auto transferring device 9 and oxygen bomb auto transferring device 10 can use manipulator or defeated
Band etc. is sent, oxygen bomb automatic lid closing/opening closing lid device 7 and thermal value measurement device 1 belong to conventional structure, and details are not described herein.
As shown in Figure 8 and Figure 9, the utility model further correspondingly discloses a kind of based on full-automatic testing calorimetric as described above
The test method of instrument, comprising the following steps:
S01, oxygen bomb 12 are uncapped: oxygen bomb is moved on oxygen bomb automatic lid closing/opening closing lid device 7 by oxygen bomb auto transferring device 10,
Oxygen bomb lid 1204 is opened by oxygen bomb automatic lid closing/opening closing lid device 7；
S02, pull out oxygen bomb core 1203: the oxygen bomb uncapped is moved to oxygen bomb core and pulls out by oxygen bomb auto transferring device 10 puts component
82, it is pulled out by oxygen bomb core and puts component 82 and extract oxygen bomb core 1203 out of oxygen bomb ontology 1201；
S03, it places crucible: the crucible for holding sample being placed on the crucible tray of oxygen bomb core 1203；Oxygen bomb is automatic simultaneously
Oxygen bomb ontology 1201 is moved to oxygen bomb automatic watering apparatus 4 by transfer device 10, by oxygen bomb automatic watering apparatus 4 to oxygen bomb sheet
Quantitative water is added in body 1201；
S04, put oxygen bomb core 1203: oxygen bomb auto transferring device 10 is by oxygen bomb core 1203 and the oxygen bomb ontology 1201 of water is added to move
It moves to oxygen bomb core to pull out and puts component 82, pulled out by oxygen bomb core and put component 82 oxygen bomb core 1203 is placed in oxygen bomb ontology 1201；
S05,12 closing lid of oxygen bomb: oxygen bomb 12 is moved to oxygen bomb automatic lid closing/opening closing lid device 7 by oxygen bomb auto transferring device 10
The lid of oxygen bomb lid 1204 is closed on oxygen bomb ontology 1201 by oxygen bomb automatic lid closing/opening closing lid device 7；
S06, test: oxygen bomb 12 is moved in thermal value measurement device 1 and carries out thermal value measurement by oxygen bomb auto transferring device 10.
In the present embodiment, before step S01, oxygen bomb 12 is moved to deflation station to oxygen by oxygen bomb auto transferring device 10
Bullet 12 carries out deflation operation, guarantees that oxygen bomb 12 is in deflation status before uncapping, guarantees the safety of test job.
In the present embodiment, between step S02 and step S03, oxygen bomb auto transferring device 10 moves oxygen bomb ontology 1201
It moves to washing station and carries out washing and cleaning operation, guarantee the cleanliness of oxygen bomb ontology 1201.
In the present embodiment, between step S01 and step S02, oxygen bomb 12 is moved to strong by oxygen bomb auto transferring device 10
Positive station rotates oxygen bomb 12 to preset bearing, so as to guarantee crucible position on the oxygen bomb core 1203 taken out out of oxygen bomb 12
It sets and is respectively positioned on same orientation, consequently facilitating other automechanisms such as manipulator carry out crucible the work such as to pick and place, improve automation
Degree.
Specifically, it elaborates below with reference to test method of the specific embodiment to the utility model:
Firstly, oxygen bomb auto transferring device 10 (such as manipulator) takes out oxygen bomb 12 from oxygen bomb storing unit 13；
The oxygen bomb of taking-up 12 is put into oxygen bomb automatic air eliminator 2 again, oxygen bomb automatic air eliminator 2 is in oxygen bomb 12
Gas is bled off；
Oxygen bomb 12 is transferred to oxygen bomb automatic lid closing/opening closing lid device 7 by manipulator, passes through oxygen bomb automatic lid closing/opening closing lid 7, device
Oxygen bomb lid 1204 is opened；
Oxygen bomb 12 oxygen bomb device for aligning 6 is sent into again by manipulator, by oxygen bomb device for aligning 6 by oxygen bomb 12
Aligning；
Oxygen bomb 12 is transferred to crucible automatic processing device 8 by manipulator, and the oxygen bomb core in crucible automatic processing device 8 compresses
Oxygen bomb core 1203 is pressed on oxygen bomb ontology 1201 by component 81；
Oxygen bomb 12 is transferred to oxygen bomb core and pulls out by manipulator puts component 82, extracts oxygen bomb core 1203；
Oxygen bomb ontology 1201 is sent into oxygen bomb automatic flushing device 5 by manipulator, and oxygen bomb automatic flushing device 5 is oxygen bomb ontology
1201 clean up；
The oxygen bomb ontology 1201 cleaned up is sent into oxygen bomb automatic watering apparatus 4 by manipulator, is automatically added water by oxygen bomb
Device 4 is to oxygen bomb ontology 1201 plus 10ml water；
Manipulator sends oxygen bomb ontology 1201 in crucible automatic processing device 8 back to；
During oxygen bomb ontology 1201 carries out cleaning plus water, crucible is put into crucible auto transferring device by operator
9, crucible is transferred to by crucible by crucible auto transferring device 9 and is picked and placed on component 84, then component 84 is picked and placed for earthenware by crucible
Crucible is placed on the crucible tray in oxygen bomb core 1203；
Oxygen bomb core, which pulls out, to be put component 82 oxygen bomb core 1203 is put into oxygen bomb ontology 1201；
Oxygen bomb 12 is put into oxygen bomb automatic lid closing/opening closing lid device 7 by manipulator, by oxygen bomb automatic lid closing/opening closing lid device 7 by oxygen
The lid of bullet lid 1204 closes on oxygen bomb ontology 1201；
Oxygen bomb 12 is sent into oxygen bomb automatic oxygenation device 3 by manipulator, to being filled with 3mpa oxygen in oxygen bomb 12；
Oxygen bomb 12 is transferred to thermal value measurement device 1 and carries out thermal value measurement by manipulator；
After completing 12 thermal value measurement of oxygen bomb；
Manipulator takes out oxygen bomb 12 out of thermal value measurement device 1, then the oxygen bomb 12 of taking-up is put into oxygen bomb automatic deflation
In device 2, gas in oxygen bomb 12 is bled off；
Oxygen bomb 12 is transferred to oxygen bomb automatic lid closing/opening closing lid device 7 by manipulator, and oxygen bomb lid 1204 is opened；
Oxygen bomb is sent into oxygen bomb device for aligning 6 by manipulator, 12 aligning of oxygen bomb；
Manipulator, which pulls out the oxygen bomb core that oxygen bomb 12 is transferred in crucible automatic processing device 8, puts component 82, extracts oxygen bomb core
1203；
Oxygen bomb ontology 1201 is sent into oxygen bomb automatic flushing device 5 by manipulator, and oxygen bomb automatic flushing device 5 is oxygen bomb ontology
1201 clean up；
Oxygen bomb ontology 1201 is sent back to crucible automatic processing device 8 by manipulator；
During oxygen bomb ontology 1201 carries out cleaning plus water, crucible picks and places component 84 and will be placed in oxygen bomb core 1203
Crucible tray on crucible take out, transfer to crucible auto transferring device 9, then earthenware is transferred to by crucible auto transferring device 9
Crucible picks and places mouth；
Oxygen bomb core, which pulls out, to be put component 82 oxygen bomb core 1203 is put into oxygen bomb ontology 1201；
Oxygen bomb 12 is put into oxygen bomb automatic lid closing/opening closing lid device 7 by manipulator, by oxygen bomb automatic lid closing/opening closing lid device 7 by oxygen
The lid of bullet lid 1204 closes on oxygen bomb ontology 1201；
Manipulator is returned to oxygen bomb 12 storage area of oxygen bomb storing unit 13.
Above are merely preferred embodiments of the utility model, the protection scope of the utility model is not limited merely to above-mentioned
Embodiment, technical solution belonging to the idea of the present invention belong to the protection scope of the utility model.It should be pointed out that pair
For those skilled in the art, several improvements and modifications without departing from the principle of the utility model,
It should be regarded as the protection scope of the utility model.
Claims (22)
1. a kind of full-automatic testing calorimeter, which is characterized in that including
Oxygen bomb automatic lid closing/opening closing lid device (7), for carrying out automatic lid closing/opening to oxygen bomb lid (1204) on oxygen bomb (12) or from dynamic circuit connector
Lid operation；
Oxygen bomb automatic oxygenation device (3), for carrying out automatic oxygenation operation to oxygen bomb (12)；
Oxygen bomb automatic watering apparatus (4), for being automatically added to quantitative water into oxygen bomb (12)；
Oxygen bomb core, which pulls out, puts component (82), for automatically extracting oxygen bomb core (1203) out of oxygen bomb ontology (1201) or by oxygen bomb core
(1203) it is put into oxygen bomb ontology (1201)；
Thermal value measurement device (1), for carrying out thermal value measurement to the sample in the crucible in oxygen bomb (12)；With
Oxygen bomb auto transferring device (10), for realizing the circulation of oxygen bomb (12) between each device.
2. full-automatic testing calorimeter according to claim 1, which is characterized in that further include oxygen bomb automatic air eliminator
(2), for automatically bleeding off the gas in oxygen bomb (12) before uncapping.
3. full-automatic testing calorimeter according to claim 1, which is characterized in that further include oxygen bomb automatic flushing device
(5), for being cleaned automatically to oxygen bomb ontology (1201).
4. full-automatic testing calorimeter according to claim 1, which is characterized in that it further include oxygen bomb storing unit (13),
For storing oxygen bomb (12).
5. full-automatic testing calorimeter according to claim 1, which is characterized in that further include oxygen bomb device for aligning
(6), for the crucible in oxygen bomb core (1203) to be corrected to pre-configured orientation.
6. full-automatic testing calorimeter according to claim 1, which is characterized in that it further include that crucible picks and places component (84),
For carrying out pick-and-place operation to the crucible in oxygen bomb core (1203) automatically.
7. full-automatic testing calorimeter as claimed in any of claims 1 to 6, which is characterized in that the calorific value is surveyed
(1), oxygen bomb automatic oxygenation device (3), oxygen bomb automatic watering apparatus (4), oxygen bomb automatic lid closing/opening closing lid device (7) and oxygen are set in trial assembly
Bullet core, which is pulled out, puts component (82) and is respectively positioned in a shell (11) and successively linearly or annular configuration；When each device is linearly arranged
When, the oxygen bomb auto transferring device (10) is slidedly arranged on the side of each device；When each device is annularly arranged, the oxygen bomb is certainly
Turn moving device (10) is slidedly arranged on the ring side of each device.
8. full-automatic testing calorimeter according to claim 7, which is characterized in that further include crucible auto transferring device
(9), for realizing in shell (11) between each device and outside crucible transfer.
9. full-automatic testing calorimeter as claimed in any of claims 1 to 6, which is characterized in that the calorific value is surveyed
The quantity that (1) is set in trial assembly is multiple.
10. full-automatic testing calorimeter according to claim 2, which is characterized in that the oxygen bomb automatic air eliminator (2)
Including deflation formed punch (22) and the first lifting assembly (21)；The deflation formed punch (22) is installed on first lifting assembly (21)
The upper and oscilaltion under the driving of first lifting assembly (21)；The bottom opening of the deflation formed punch (22), for covering
Oxygen bomb (12) oxygen bomb head (1202) peripheral side and form all side seals；Exhaust passage is equipped with inside the deflation formed punch (22)
(22011) and on the end face of bottom end the thimble (2204) for being provided with the bullet core for opening the oxygen bomb (12) to deflate.
11. full-automatic testing calorimeter according to claim 10, which is characterized in that the deflation formed punch (22) includes putting
Gas head (2201) and sealing fixing head (2202), the deflation head (2201) are installed on first lifting assembly (21), institute
State the bottom that sealing fixing head (2202) is removably mounted to the deflation head (2201).
12. full-automatic testing calorimeter according to claim 11, which is characterized in that sealing fixing head (2202) packet
Interconnecting piece and clamping part are included, forms ring-shaped step between the interconnecting piece and clamping part；The interconnecting piece and the deflation head
(2201) it is threadedly coupled between, lip ring is installed between the ring-shaped step and the bottom end end face of deflation head (2201)
(2203), all side seals are formed in oxygen bomb head (1202) peripheral side to cover.
13. full-automatic testing calorimeter as claimed in any of claims 1 to 6, which is characterized in that the oxygen bomb is certainly
Dynamic oxygenate apparatus (3) include oxygenation formed punch (32) and the second lifting assembly (33)；The oxygenation formed punch (32) is installed on described
On two lifting assemblies (33) and the oscilaltion under the driving of second lifting assembly (33)；The bottom of oxygenation formed punch (32)
Portion is equipped with opening, and oxygen bomb head (1202) peripheral side in oxygen bomb (12) is covered when for declining and forms all side seals；The oxygenation
Filling channel is equipped with inside formed punch (32)；The oxygenation formed punch (32) is connected in one end of filling channel by gas ducting aerobic
Gas source (3104).
14. full-automatic testing calorimeter according to claim 13, which is characterized in that be provided with out on the gas ducting
Close component (3103) and the pressure detecting part (3101) for detecting oxygen pressure.
15. full-automatic testing calorimeter as claimed in any of claims 1 to 6, which is characterized in that further include fixing
Component and Anchor plate kit (83)；The fixation kit is used to oxygen bomb ontology (1201) being fixed on predetermined position；The pressing plate group
Part (83) includes pressing plate (8301) and third lifting assembly, and the pressing plate (8301) is installed on the movable end of third lifting assembly,
For pushing down the side of crucible tray and moving down so that crucible avoids the fire rod on oxygen bomb core (1203).
16. full-automatic testing calorimeter as claimed in any of claims 1 to 6, which is characterized in that the oxygen bomb core
Pull out that put component (82) include hanging support plate (8302) and the 4th lifting assembly, the hanging support plate (8302) is installed on the 4th lifting
The movable end of component, the hanging support plate (8302) is for tangling oxygen bomb head (1202) and under the driving of the 4th lifting assembly to oxygen
Bullet core (1203) pull out automatically and is put.
17. full-automatic testing calorimeter according to claim 6, which is characterized in that the crucible picks and places component (84) packet
Include the first translation unit (8403), bracket (8401) and locating slot (8402)；One end and described first of the bracket (8401)
The movable end of translation unit (8403) is connected, and the locating slot (8402) is installed on the other end of the bracket (8401).
18. full-automatic testing calorimeter as claimed in any of claims 1 to 6, which is characterized in that further include oxygen bomb
Core holds down assembly (81), for oxygen bomb core (1203) to be pressed on oxygen bomb ontology (1201) before oxygen bomb core (1203) is chosen
It puts component (82) in order to which oxygen bomb core pulls out and reliably tangles oxygen bomb head (1202).
19. full-automatic testing calorimeter according to claim 18, which is characterized in that the oxygen bomb core holds down assembly (81)
Including compact heap (8101) and the 5th lifting assembly (8102), the compact heap (8101) is installed on the 5th lifting assembly
(8102) movable end makes oxygen bomb for covering oxygen bomb head (1202) and pushing under the driving of the 5th lifting assembly (8102)
Core (1203) is pressed on oxygen bomb ontology (1201).
20. full-automatic testing calorimeter according to claim 5, which is characterized in that the oxygen bomb device for aligning (6)
Including correction formed punch (61), third rotary components (63) and the 6th lifting assembly (62)；It opens the bottom of correction formed punch (61)
Mouthful, the opening is equipped with the correction boss (6101) to match with the correction notch of oxygen bomb (12)；The correction formed punch (61)
It is installed on the third rotary components (63), and is rotated under the driving of third rotary components (63)；The third rotation group
Part (63) is installed on the 6th lifting assembly (62), and the oscilaltion under the driving of the 6th lifting assembly (62).
21. full-automatic testing calorimeter according to claim 3, which is characterized in that the oxygen bomb automatic flushing device (5)
Including fixed cell, lifting rotation component (52) and cleaning assembly (53)；The fixed cell, for oxygen bomb (12) to be fixed on
Cleaning positions；The cleaning assembly (53) is installed on the lifting rotation component (52), and in the lifting rotation component
(52) it under driving, stretches in oxygen bomb (12) and rotates to carry out washing and cleaning operation to oxygen bomb (12).
22. full-automatic testing calorimeter according to claim 21, which is characterized in that during the cleaning assembly (53) includes
Empty brush holder support (5301), the side of the brush holder support (5301) is provided with bristle (5302)；It closes the bottom of the brush holder support (5301)
And top end opening, and side is provided with multiple apopores (5303) communicated with internal cavities, at the top of the brush holder support (5301)
Opening is connected with plus water assembly (54).
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