CN209130923U - A kind of calorimeter fire rod and calorimeter - Google Patents

A kind of calorimeter fire rod and calorimeter Download PDF

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Publication number
CN209130923U
CN209130923U CN201821620738.8U CN201821620738U CN209130923U CN 209130923 U CN209130923 U CN 209130923U CN 201821620738 U CN201821620738 U CN 201821620738U CN 209130923 U CN209130923 U CN 209130923U
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China
Prior art keywords
calorimeter
oxygen bomb
fire rod
electrode
rod
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CN201821620738.8U
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Chinese (zh)
Inventor
李冬军
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Hunan Sundy Science and Technology Co Ltd
Hunan Sundy Science and Technology Development Co Ltd
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Hunan Sundy Science and Technology Development Co Ltd
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Priority to CN201821620738.8U priority Critical patent/CN209130923U/en
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Abstract

The utility model discloses a kind of calorimeter fire rodes, including heating component, fixed electrode and lead electrode;The heating component includes heating rod, heater strip and two conductor pins;Two conductor pins are located in the heating rod and bottom end is connected by heater strip, and the top of two conductor pins is then connected with the fixed electrode and lead electrode respectively, and the top of two conductor pins is then connected with the fixed electrode and lead electrode respectively;The fixed electrode is located at the top of the heating rod and is removably connected with interconnecting piece, and the interconnecting piece is used to be detachably connected with the oxygen bomb core of oxygen bomb in calorimeter.The invention also discloses a kind of calorimeters, including oxygen bomb and calorimeter fire rod as described above, the fire rod to be removably mounted on the oxygen bomb core of oxygen bomb.The calorimeter of the utility model fire rod and calorimeter all have that structure is simple, the advantages that being dismounted easily.

Description

A kind of calorimeter fire rod and calorimeter
Technical field
The utility model relates generally to sample assay technique field, refers in particular to a kind of calorimeter fire rod and calorimeter.
Background technique
Calorimeter is the instrument for measuring the combustibles calorific value such as various solid-states, liquid, mainly by outer cylinder, inner cylinder and oxygen The composition such as bullet, measures its calorific value by burning of the combustible in oxygen bomb.But current used fire rod Structure is complicated, dismounting is inconvenient.
Utility model content
The technical problems to be solved in the utility model is that for technical problem of the existing technology, this is practical new Type provides the calorimeter fire rod that a kind of structure is simple, is dismounted easily.
In order to solve the above technical problems, the utility model proposes technical solution are as follows:
A kind of calorimeter fire rod, including heating component, fixed electrode and lead electrode;The heating component includes adding Hot pin, heater strip and two conductor pins;Two conductor pins are located in the heating rod and bottom end is connected by heater strip, and two The top of root conductor pin is then connected with the fixed electrode and lead electrode respectively;The fixed electrode is located at the heating rod Top and it is removably connected with interconnecting piece, the interconnecting piece is used to be detachably connected with the oxygen bomb core of oxygen bomb in calorimeter.
As a further improvement of the above technical scheme:
The heating rod is silicon nitride ceramics stick.
The bottom of the heating rod is in arcuation.
The middle part of the heating rod is interspersed to be equipped with fireguard.
The conductor pin is connected by metalization layer with fixed electrode and lead electrode.
The upper end of the fixed electrode is equipped with threaded hole, and one end of the interconnecting piece is threadedly coupled with the threaded hole.
The other end of the interconnecting piece is equipped with external screw thread, for being threadedly coupled with the threaded hole on oxygen bomb core.
The fixed electrode and lead electrode are the electrode of corrosion-resistant material.
The lead electrode is connected with non-rigid conducting wire.
It is described the invention also discloses a kind of calorimeter, including oxygen bomb and calorimeter fire rod as described above Fire rod is removably mounted on the oxygen bomb core of oxygen bomb.
Compared with the prior art, the advantages of the utility model are:
The calorimeter fire rod of the utility model, by being detachably connected (specially spiral shell between interconnecting piece and oxygen bomb core Line connection), it is dismounted easily;The overall structure of heating component is simple, and structure reliable with the connection of fixed electrode and lead electrode Simply;By the way of heating fire rod igniting, numerous technical problems of Fuse Type igniting are prevented, heating fire rod is repeatable It uses, without replacing ignition wire after each test again, reduces labor intensity and use cost, substantially increase work operations Efficiency reduces experimental implementation difficulty;Special heating fire rod igniting form is taken, there is no ignition wire remnants, make The point that must be tested every time is intimately consistent, and the high-precision and operational safety of coal sample experiment has been effectively ensured.
The calorimeter fire rod of the utility model, the bottom of heating rod are in arc-shaped, reduce connecing for heating rod and crucible Contacting surface product, and can be avoided the sample in mycrodyne crucible (such as coal sample), so that the coal sample of heating rod bottom is burnt sufficiently, and can also Heat is enough reduced to be transferred on crucible from heating rod.
The calorimeter of the utility model equally has the advantages that described in fire rod as above.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model.
Fig. 2 is the structural schematic diagram of utility model calorimeter.
Figure label indicates: 1, heating component;101, heating rod;102, conductor pin;103, heater strip;104, it metallizes Layer;2, fixed electrode;3, lead electrode;301, conducting wire;4, fireguard;5, interconnecting piece;501, external screw thread;6, oxygen bomb;601, oxygen Play ontology;602, oxygen bomb core;603, oxygen bomb lid;7, crucible.
Specific embodiment
The utility model is further described below in conjunction with Figure of description and specific embodiment.
As depicted in figs. 1 and 2, the calorimeter fire rod of the present embodiment, including heating component 1, fixed electrode 2 and conducting wire Electrode 3;Heating component 1 includes heating rod 101, heater strip 103 and two conductor pins 102;Two conductor pins 102 are installed on heating The inside and bottom end of stick 101 by heater strip 103 connection (heater strip 103 also is located in heating rod 101, in addition conductor pin 102 with Heater strip 103 is filled in heating rod 101 by silicon nitride filler), the top of two conductor pins 102 then respectively with fixation Electrode 2 is connected with lead electrode 3;Electrode 2 is wherein fixed to be installed on the top of heating rod 101 and be removably connected with interconnecting piece 5, Interconnecting piece 5 is used to be detachably connected with the oxygen bomb core 602 of oxygen bomb 6 in calorimeter, i.e., fire rod is installed on oxygen by interconnecting piece 5 In bullet core 602.The calorimeter fire rod of the utility model is torn open by being detachably connected between interconnecting piece 5 and oxygen bomb core 602 Dress is easy;The overall structure of heating component 1 is simple, reliable with the connection of fixed electrode 2 and lead electrode 3 and structure is simple;It adopts With the mode of heating fire rod igniting, numerous technical problems of Fuse Type igniting are prevented, heating fire rod is reusable, no With ignition wire is replaced after each test again, labor intensity and use cost are reduced, work operations efficiency is substantially increased, is dropped Low experimental implementation difficulty;Special heating fire rod igniting form is taken, there is no ignition wire remnants, so that examination every time The point tested is intimately consistent, and the high-precision and operational safety of coal sample experiment has been effectively ensured.
In the present embodiment, heating rod 101 is silicon nitride ceramics stick;The bottom of heating rod 101 is in arc-shaped, reduces heating rod 101 with the contact area of crucible 7, and can be avoided the sample (such as coal sample) in mycrodyne crucible 7, make the coal of 101 bottom of heating rod Sample burning sufficiently, but also can reduce heat and be transferred on crucible 7 from heating rod 101.
In the present embodiment, the middle part of heating rod 101 is interspersed to be equipped with fireguard 4, and specifically, fireguard 4 is stainless steel material Or other high temperature resistants, corrosion resistant material;Fireguard 4 avoids 7 combustion flame of crucible from directly burning electricity for protecting each electrode Pole extends the service life of electrode.
In the present embodiment, conductor pin 102 is connected by metalization layer 104 with fixed electrode 2 and lead electrode 3, is easy to real It is existing;It wherein fixes electrode 2 and lead electrode 3 is stainless steel material or other high temperature resistants, corrosion-resistant material, improve and use the longevity Life.
In the present embodiment, the upper end of fixed electrode 2 is equipped with threaded hole, and one end of interconnecting piece 5 is cylindrical, with threaded hole spiral shell Line connection.The other end of interconnecting piece 5 is then equipped with external screw thread 501, for being threadedly coupled with the threaded hole on oxygen bomb core 602.That is point Lighted torch is threadedly coupled with oxygen bomb core 602, is dismounted easily.
As shown in Fig. 2, the invention also discloses a kind of calorimeter, including oxygen bomb and calorimeter point as described above Lighted torch, fire rod are removably mounted on the oxygen bomb core of oxygen bomb.Specifically, oxygen bomb 6 includes oxygen bomb ontology 601,602 and of oxygen bomb core Oxygen bomb lid 603, oxygen bomb core 602 are placed in oxygen bomb ontology 601, and oxygen bomb lid 603 then seals between oxygen bomb ontology 601 and screw thread connects It connects;Interconnecting piece 5 at the top of fire rod is then threadedly coupled with the threaded hole of oxygen bomb core 602, and the bottom of fire rod is then placed in crucible 7 Interior, lead electrode 3 is then connected with non-rigid conducting wire 301, and non-rigid conducting wire 301 is then fixed on a fixed position of oxygen bomb core 602. When dismantling fire rod, crucible 7 is taken down, conducting wire 301 of dismantling, unclamps fixed electrode 2.
Although the utility model has been disclosed with preferred embodiment as above, it is not intended to limit the utility model.It is any Those skilled in the art, in the case where not departing from technical solutions of the utility model range, all using the disclosure above Technology contents many possible changes and modifications are made to technical solutions of the utility model, or be revised as the equivalent of equivalent variations Embodiment.Therefore, all contents without departing from technical solutions of the utility model, according to the utility model technical spirit to the above reality Any simple modifications, equivalents, and modifications that example is done are applied, should all be fallen in the range of technical solutions of the utility model protection.

Claims (10)

1. a kind of calorimeter fire rod, which is characterized in that including heating component (1), fixed electrode (2) and lead electrode (3); The heating component (1) includes heating rod (101), heater strip (103) He Lianggen conductor pin (102);Two conductor pins (102) it is located in the heating rod (101) and bottom end to connect by heater strip (103), the top of two conductor pins (102) is then divided It is not connected with the fixed electrode (2) and lead electrode (3);The fixed electrode (2) is located at the top of the heating rod (101) And interconnecting piece (5) are removably connected with, the interconnecting piece (5) is used for detachable with the oxygen bomb core (602) of oxygen bomb in calorimeter (6) Connection.
2. calorimeter fire rod according to claim 1, which is characterized in that the heating rod (101) is silicon nitride pottery Porcelain stick.
3. calorimeter fire rod according to claim 1, which is characterized in that the bottom of the heating rod (101) is in arc Shape.
4. calorimeter fire rod according to claim 1 or 2 or 3, which is characterized in that in the heating rod (101) Portion is interspersed to be equipped with fireguard (4).
5. calorimeter fire rod according to claim 1 or 2 or 3, which is characterized in that the conductor pin (102) passes through Metalization layer (104) is connected with fixed electrode (2) and lead electrode (3).
6. calorimeter fire rod according to claim 1 or 2 or 3, which is characterized in that the fixed electrode (2) it is upper End is equipped with threaded hole, and one end of the interconnecting piece (5) is threadedly coupled with the threaded hole.
7. calorimeter fire rod according to claim 6, which is characterized in that the other end of the interconnecting piece (5) is equipped with External screw thread (501), for being threadedly coupled with the threaded hole on oxygen bomb core (602).
8. calorimeter fire rod according to claim 1 or 2 or 3, which is characterized in that the fixed electrode (2) and lead Line electrode (3) is the electrode of corrosion-resistant material.
9. calorimeter fire rod according to claim 1 or 2 or 3, which is characterized in that lead electrode (3) connection There are non-rigid conducting wire (301).
10. a kind of calorimeter, including oxygen bomb (6), which is characterized in that further include as in one of claimed in any of claims 1 to 9 Calorimeter fire rod, the fire rod are removably mounted on the oxygen bomb core (602) of oxygen bomb (6).
CN201821620738.8U 2018-09-29 2018-09-29 A kind of calorimeter fire rod and calorimeter Active CN209130923U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821620738.8U CN209130923U (en) 2018-09-29 2018-09-29 A kind of calorimeter fire rod and calorimeter

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821620738.8U CN209130923U (en) 2018-09-29 2018-09-29 A kind of calorimeter fire rod and calorimeter

Publications (1)

Publication Number Publication Date
CN209130923U true CN209130923U (en) 2019-07-19

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110988021A (en) * 2019-11-19 2020-04-10 中国农业科学院农产品加工研究所 Heat value detection sample loading device and food self-heating bag detection method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110988021A (en) * 2019-11-19 2020-04-10 中国农业科学院农产品加工研究所 Heat value detection sample loading device and food self-heating bag detection method
CN110988021B (en) * 2019-11-19 2022-07-08 中国农业科学院农产品加工研究所 Heat value detection sample loading device and food self-heating bag detection method

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