CN209080524U - Neodymium iron boron strip alloy sheet storage device - Google Patents

Neodymium iron boron strip alloy sheet storage device Download PDF

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Publication number
CN209080524U
CN209080524U CN201821698144.9U CN201821698144U CN209080524U CN 209080524 U CN209080524 U CN 209080524U CN 201821698144 U CN201821698144 U CN 201821698144U CN 209080524 U CN209080524 U CN 209080524U
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CN
China
Prior art keywords
cabinet
case lid
iron boron
neodymium iron
alloy sheet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201821698144.9U
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Chinese (zh)
Inventor
李蕾
高晓山
何文敬
张德文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
North Rare Earth Anhui Permanent Magnet Technology Co ltd
Original Assignee
ANHUI BAOTOU STEEL RARE EARTH PERMANENT MAGNETIC ALLOY INDUSTRY Co Ltd
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Application filed by ANHUI BAOTOU STEEL RARE EARTH PERMANENT MAGNETIC ALLOY INDUSTRY Co Ltd filed Critical ANHUI BAOTOU STEEL RARE EARTH PERMANENT MAGNETIC ALLOY INDUSTRY Co Ltd
Priority to CN201821698144.9U priority Critical patent/CN209080524U/en
Application granted granted Critical
Publication of CN209080524U publication Critical patent/CN209080524U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model relates to neodymium iron boron strip alloy sheet storage device, including the open cabinet in top, case lid, it is provided with flanging at the top of cabinet, the outside of cabinet is installed with electric hot plate;The bottom of case lid is installed with the retaining ring to match with cabinets cavity, and sealing ring is provided between case lid and flanging, is provided with multiple bolt fasteners between the edge and flanging of case lid;It is provided with the liquid feed valve being connected with inlet opening above case lid, the exhaust-valve being connected with through-hole is additionally provided with above case lid, the intake valve being connected with air inlet is additionally provided with above case lid;The outside of cabinet is provided with the tapping valve being connected with drainage hole;The outside of cabinet is provided with the exhaust valve being connected with gas vent.The neodymium iron boron strip alloy sheet storage device can store neodymium iron boron strip alloy sheet, be at oxygen-free environment, neodymium iron boron strip alloy sheet is effectively avoided to be oxidized;The neodymium iron boron strip alloy sheet storage device advantageously reduces transportation cost, highly-safe.

Description

Neodymium iron boron strip alloy sheet storage device
Technical field
The utility model relates to neodymium iron boron strip alloy sheet storage devices, belong to rare earth material processing technique field.
Background technique
Rare earth permanent-magnetic material neodymium iron boron is a kind of important magnetic material, is referred to as " magnetic with excellent magnetic property King " is widely used in modern industry and electronic technology.In the neodymium iron boron manufacturing, first it is dilute that neodymium iron boron is made in smelting Native alloy fragment, then NdFeB rear-earth alloy fragment is processed into powder, finally NdFeB rear-earth alloy powder is gathered into Then type is sintered, be finally cut into required size again and complete.
In the manufacturing process of NdFeB rear-earth alloy fragment, usually first each raw material are smelted into liquid alloy liquid, then Large stretch of alloy sheet is formed by refining, cooling, then alloy sheet is carried out brokenly by two mutually matched breaker rolls It is broken to obtain the NdFeB rear-earth alloy fragment of chunky shape.And sintered NdFeB product is before sintering blank into, due to easy oxygen The characteristic of change, if product is aoxidized before sintering process, will generate very performance so that product storage becomes particularly important Big negative effect, it is serious it also occur that spontaneous combustion, causes safety accident.
Currently, neodymium iron boron strip alloy sheet after being ground into neodymium iron boron alloy powder, is stored and is poured usually using polybag Inert gas carrys out starvation storage.And storage of the neodymium iron boron strip alloy sheet before not being ground into neodymium iron boron alloy powder, If made in such a way that polybag stores and pours inert gas due to neodymium iron boron strip alloy sheet easy damaged polybag It is revealed at inert gas, is also just unable to reach the purpose of starvation.Thus it is common to use seal box stores, by neodymium Iron boron strip alloy sheet is put into inside seal box, is then 300~500Pa by being evacuated to vacuum degree, then to sealing Argon gas is filled with inside case to protect;The oxygen inside seal box can not be thoroughly removed when in this process, due to vacuumizing, because This, still has micro oxygen inside seal box, the partial oxidation is micro- to the oxidation of neodymium iron boron strip alloy sheet since content is few Its is micro-, thus the storage method is suitable for the production process of most of sintered NdFeB product.But for artificial satellite, In the specials such as radar, aerospace equipment, nuclear magnetic resonance equipment, therefore, to assure that storage condition is oxygen-free environment, to reach Oxygen-free environment, generallys use ethyl alcohol, hexane, acetone and other organic solvent to replace inert gas to carry out starvation, to leakproofness Inside is filled with organic solvent and easily its internal air can be discharged, and ethyl alcohol, hexane, acetone and other organic solvent will not It is physically or chemically reacted with the generation of neodymium iron boron strip alloy sheet, therefore, can satisfy storage request;But this method there is also , a large amount of uses of organic solvent following defect: 1), the gross mass of seal box is caused to significantly improve, this can improve subsequent transport Cost;2), ethyl alcohol, hexane, acetone and other organic solvent are combustibles, and storage condition and transportation environment require height, if operation It is improper, Yi Fasheng safety accident.
Utility model content
The utility model is in view of the deficienciess of the prior art, provide neodymium iron boron strip alloy sheet storage device, specifically Technical solution is as follows:
Neodymium iron boron strip alloy sheet storage device, including the open cabinet in top, case lid are provided at the top of the cabinet The outside of flanging, the cabinet is installed with electric hot plate;The bottom of the case lid is installed with the retaining ring to match with cabinets cavity, Be provided with sealing ring between the case lid and flanging, the sealing ring is set in the outside of retaining ring, the edge of the case lid with Multiple bolt fasteners are provided between flanging;The capping of the case lid is provided with inlet opening, the top setting of the case lid Have the liquid feed valve being connected with inlet opening, the capping of the case lid is additionally provided with through-hole, be additionally provided with above the case lid with The exhaust-valve that through-hole is connected, the capping of the case lid are additionally provided with air inlet, are additionally provided with above the case lid and air inlet The intake valve that hole is connected;The side wall of the cabinet is provided with drainage hole, and the outside of the cabinet is provided with to be connected with drainage hole Logical tapping valve;The side wall of the cabinet is provided with gas vent, and the outside of the cabinet is provided with the row being connected with gas vent Air valve.
As an improvement of the above technical solution, the bolt fastener includes the nut that bolt and bolt match, described The edge of flanging is provided with the first mounting hole of the bar portion disengaging for bolt, and the edge of the case lid is provided with the bar for bolt Second mounting hole of portion's disengaging, the bolts and nuts are threadedly coupled.
As an improvement of the above technical solution, handle is installed with above the bolt head.
As an improvement of the above technical solution, the pressure for measuring box house air pressure is additionally provided with above the case lid Power vacuum meter.
As an improvement of the above technical solution, lifting lug is installed with above the case lid.
As an improvement of the above technical solution, the bottom of the cabinet is provided with multiple universal wheels, the universal wheel setting In the lower section of cabinet.
As an improvement of the above technical solution, the inner wall of the cabinet is installed with the first filter for being completely covered by drainage hole Net, the inner wall of the cabinet are installed with the second strainer for being completely covered by gas vent.
It as an improvement of the above technical solution, is clearance fit between the outer ring of the retaining ring and the inner wall of cabinet.
It as an improvement of the above technical solution, is interference fit between the inner ring of the sealing ring and the outer ring of retaining ring.
Neodymium iron boron strip alloy sheet storage device described in the utility model can store neodymium iron boron strip alloy sheet, and make It is in oxygen-free environment, and neodymium iron boron strip alloy sheet can effectively be avoided to be oxidized;Relative to directly adopt organic solvent come every Absolutely at oxygen-free environment for, the neodymium iron boron strip alloy sheet storage device does protection gas using argon gas, and the neodymium iron boron is thin Gross mass with alloy sheet storage device is lower, advantageously reduces transportation cost, while highly-safe.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of neodymium iron boron strip alloy sheet storage device described in the utility model;
Fig. 2 is the structural schematic diagram of cabinet described in the utility model;
Fig. 3 is the structural schematic diagram of case lid described in the utility model.
Specific embodiment
In order to make the purpose of the utility model, technical solutions and advantages more clearly understood, below in conjunction with attached drawing and implementation Example, the present invention will be further described in detail.It should be appreciated that specific embodiment described herein is only used to explain The utility model is not used to limit the utility model.
As shown in Figures 1 to 3, the neodymium iron boron strip alloy sheet storage device, including the open cabinet 10 in top, case lid 20, the top of the cabinet 10 is provided with the flanging 15 turned down to the outside of cabinet 10, and the outside of the cabinet 10 is installed with electricity Hot plate 40;The bottom of the case lid 20 is installed with the retaining ring 25 to match with 10 inner cavity of cabinet, the case lid 20 and flanging 15 Between be provided with sealing ring 30, the sealing ring 30 is set in the outside of retaining ring 25, the edge and flanging 15 of the case lid 20 Between be provided with multiple bolt fasteners, be fastened by bolts that part is fixed to be connected between the edge and flanging 15 of the case lid 20 It connects;The capping of the case lid 20 is provided with inlet opening 201, and the top of the case lid 20 is provided with to be connected with inlet opening 201 Liquid feed valve 21, the capping of the case lid 20 are additionally provided with through-hole 202, and the top of the case lid 20 is additionally provided with and 202 phase of through-hole The exhaust-valve 22 of connection, the capping of the case lid 20 are additionally provided with air inlet 203, the top of the case lid 20 be additionally provided with into The intake valve 23 that stomata 203 is connected;The side wall of the cabinet 10 is provided with drainage hole 11, and the outside of the cabinet 10 is provided with The tapping valve 12 being connected with drainage hole 11;The side wall of the cabinet 10 is provided with gas vent 13, and the outside of the cabinet 10 is set It is equipped with the exhaust valve 14 being connected with gas vent 13.
The metal that the cabinet 10 and case lid 20 are all made of high mechanical strength is made.It opens bolt fastener and makes cabinet 10 It is separated with case lid 20, is then packed into neodymium iron boron strip alloy sheet to the inside of cabinet 10, then covers case lid 20.Utilize diaphragm pump Organic solvent is transported to the inside of cabinet 10 by liquid feed valve 21, is such as connected to the output end of diaphragm pump with liquid feed valve 21, every The input terminal of membrane pump is connected to the storage barrel equipped with organic solvent, liquid feed valve 21 and exhaust-valve 22 is opened, in the driving of diaphragm pump Under, organic solvent is transported to the inside of cabinet 10, when the output end of exhaust-valve 22 overflows organic solvent outward, illustrates cabinet By organic solvent to being full of, the inner air of cabinet 10 is discharged completely for 10 inside, be then shut off exhaust-valve 22 and into Liquid valve 21 closes diaphragm pump.Wherein, the organic solvent is one of ethyl alcohol, hexane, acetone;It is described to have in the present embodiment Solvent is preferably the acetone of low boiling point.Air pump is set between intake valve 23 and argon bottle, opens intake valve 23 and tapping valve 12, while booster air pump, argon gas can be transported to the inside of cabinet 10 by air pump, so that the acetone inside cabinet 10 can Row outwardly, when the output end of tapping valve 12 is not then exhausted from acetone, closes tapping valve 12, closes intake valve from tapping valve 12 23 and air pump;Exhaust valve 14 is connected to vacuum pump, is then powered to electric hot plate 40, electric hot plate 40, which is powered, generates heat to give Cabinet 10 heats, so that the temperature inside cabinet 10 is 58~60 DEG C, at such a temperature, acetone is evaporated into gas, at this time case Gas inside body 10 is the gaseous mixture of gaseous state acetone and argon gas;Then exhaust valve 14 is opened, vacuum pump is opened, to cabinet 10 Inside carries out being evacuated to vacuum degree being 300~500Pa, closes vacuum pump, exhaust valve 14, powers off to electric hot plate 40;By adopting Take the means vacuumized so that the gaseous state content of acetone inside cabinet 10 significantly reduces, even if between the inside of cabinet 10 restore To room temperature, gaseous state acetone is liquefied as aqueous acetone again, and the content of the aqueous acetone is less than ten a ten thousandths, the liquid third The content of ketone is the ratio of the gross mass and the gross mass of the cabinet 10 equipped with neodymium iron boron strip alloy sheet of aqueous acetone, Er Qiebing Ketone will not react with neodymium iron boron strip alloy sheet, therefore to will not influence neodymium iron boron thin for the aqueous acetone of 10 internal residual of cabinet Storage with alloy sheet.Finally, opening intake valve 23 and air pump, continue to be filled with argon gas to the inside of cabinet 10, until cabinet 10 Internal air pressure reaches 120~150kPa, closes intake valve 23 and air pump.In above process, due to organic molten using inputting The mode of agent exhausts the air inside cabinet 10, to avoid the inside of subsequent cabinet 10 from containing oxygen, then by cabinet 10 Internal organic solvent is discharged and is removed the organic solvent inside cabinet 10 to greatest extent by the way of heating evaporation, finally Argon gas is poured into carry out isolated protection to the neodymium iron boron strip alloy sheet inside cabinet 10 to the inside of cabinet 10 again;Finally, case Neodymium iron boron strip alloy sheet inside body 10 is in oxygen-free environment, simultaneously as there is no a large amount of organic for the inside of cabinet 10 Solvent pours into the lighter weight of the cabinet 10 of argon gas, after this is advantageously reduced for the cabinet 10 for filling organic solvent Continuous transportation cost;Meanwhile the flammable organic solvent contained inside cabinet 10 is negligible, and therefore, the storage rings of cabinet 10 Border and transportation environment are of less demanding, are not susceptible to safety accident.Wherein, the presence of sealing ring 30, so that cabinet 10 and case lid 20 are able to maintain sealing, the preferable rubber ring of the sealing ring 30 after fixation.The presence of retaining ring 25 has the function of positioning, So that case lid 20 is easily closed with the top cover of cabinet 10.Further, resistance, the outer ring of the retaining ring 25 and cabinet are installed to reduce It is clearance fit between 10 inner wall.Further, match between the inner ring of the sealing ring 30 and the outer ring of retaining ring 25 for interference It closes, this is not only advantageous to further increase sealing effect, but also facilitates installation sealing ring 30.
Further, for convenience of open, closure case lid 20, the bolt fastener include bolt 51, with 51 phase of bolt The nut 52 matched, the edge of the flanging 15 are provided with the first mounting hole 151 of the bar portion disengaging for bolt 51, the case lid 20 edge is provided with the second mounting hole 204 of the bar portion disengaging for bolt 51, successively the second installation of the bar portion of the bolt 51 Hole 204,151 rear bolt 51 of the first mounting hole bar portion be threadedly coupled with nut 52.
Further, the bolt 51 is rotated for convenience, is installed with handle 53 above 51 head of bolt.
Further, for convenience of in time understand cabinet 10 inside air pressure, the top of the case lid 20 be additionally provided with for Measure the pressure vacuum meter 24 of 10 air pressure inside of cabinet.The pressure vacuum meter 24 is a kind of can both to measure greater than atmospheric pressure Positive pressure can measure the instrument of the negative pressure less than atmospheric pressure again.
Further, for convenience of case lid 20 is sling, the top of the case lid 20 is installed with lifting lug 26.
Further, for convenience of the mobile cabinet 10, the bottom of the cabinet 10 is provided with multiple universal wheels 18, described The lower section of cabinet 10 is arranged in universal wheel 18.
Further, the inner wall of the cabinet 10 is installed with the first strainer 16 for being completely covered by drainage hole 11, the case The inner wall of body 10 is installed with the second strainer 17 for being completely covered by gas vent 13.The presence of first strainer 16, avoids cabinet Neodymium iron boron strip alloy sheet inside 10 enters drainage hole 11;Similarly, the presence of the second strainer 17, avoids inside cabinet 10 Neodymium iron boron strip alloy sheet enters gas vent 13.
In the above-described embodiments, the neodymium iron boron strip alloy sheet storage device can store neodymium iron boron strip alloy sheet, And it is at oxygen-free environment, neodymium iron boron strip alloy sheet can effectively be avoided to be oxidized;It is organic molten relative to directlying adopt Agent completely cuts off into for oxygen-free environment, and the neodymium iron boron strip alloy sheet storage device does protection gas, the neodymium using argon gas The gross mass of iron boron strip alloy sheet storage device is lower, advantageously reduces transportation cost, while highly-safe.
The above is only the preferred embodiment of the utility model only, is not intended to limit the utility model, all at this Made any modifications, equivalent replacements, and improvements etc., should be included in the utility model within the spirit and principle of utility model Protection scope within.

Claims (9)

1. neodymium iron boron strip alloy sheet storage device, it is characterised in that: including the open cabinet in top (10), case lid (20), institute It states and is provided at the top of cabinet (10) flanging (15), the outside of the cabinet (10) is installed with electric hot plate (40);The case lid (20) bottom is installed with the retaining ring (25) to match with cabinet (10) inner cavity, sets between the case lid (20) and flanging (15) It is equipped with sealing ring (30), the sealing ring (30) is set in the outside of retaining ring (25), the edge and flanging of the case lid (20) (15) multiple bolt fasteners are provided between;The capping of the case lid (20) is provided with inlet opening (201), the case lid (20) Top be provided with the liquid feed valve (21) being connected with inlet opening (201), the capping of the case lid (20) is additionally provided with through-hole (202), the exhaust-valve (22) being connected with through-hole (202) is additionally provided with above the case lid (20), the case lid (20) Capping is additionally provided with air inlet (203), is additionally provided with the intake valve being connected with air inlet (203) above the case lid (20) (23);The side wall of the cabinet (10) is provided with drainage hole (11), and the outside of the cabinet (10) is provided with and drainage hole (11) The tapping valve (12) being connected;The side wall of the cabinet (10) is provided with gas vent (13), the external setting of the cabinet (10) There is the exhaust valve (14) being connected with gas vent (13).
2. neodymium iron boron strip alloy sheet storage device according to claim 1, it is characterised in that: the bolt fastener packet The nut (52) for including bolt (51), matching with bolt (51), the edge of the flanging (15) is provided with for bolt (51) The first mounting hole (151) of bar portion disengaging, the edge of the case lid (20) are provided with second of the bar portion disengaging for bolt (51) Mounting hole (204), the bolt (51) are threadedly coupled with nut (52).
3. neodymium iron boron strip alloy sheet storage device according to claim 2, it is characterised in that: bolt (51) head Top be installed with handle (53).
4. neodymium iron boron strip alloy sheet storage device according to claim 1, it is characterised in that: the case lid (20) it is upper Side is additionally provided with the pressure vacuum meter (24) for measuring cabinet (10) air pressure inside.
5. neodymium iron boron strip alloy sheet storage device according to claim 1, it is characterised in that: the case lid (20) it is upper Side is installed with lifting lug (26).
6. neodymium iron boron strip alloy sheet storage device according to claim 1, it is characterised in that: the bottom of the cabinet (10) Portion is provided with multiple universal wheels (18), lower section of universal wheel (18) setting in cabinet (10).
7. neodymium iron boron strip alloy sheet storage device according to claim 1, it is characterised in that: the cabinet (10) it is interior Wall is installed with the first strainer (16) for being completely covered by drainage hole (11), and the inner wall of the cabinet (10) is installed with gas vent (13) the second strainer (17) being completely covered by.
8. neodymium iron boron strip alloy sheet storage device according to claim 1, it is characterised in that: outside the retaining ring (25) It is clearance fit between circle and the inner wall of cabinet (10).
9. neodymium iron boron strip alloy sheet storage device according to claim 1, it is characterised in that: the sealing ring (30) It is interference fit between inner ring and the outer ring of retaining ring (25).
CN201821698144.9U 2018-10-12 2018-10-12 Neodymium iron boron strip alloy sheet storage device Expired - Fee Related CN209080524U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821698144.9U CN209080524U (en) 2018-10-12 2018-10-12 Neodymium iron boron strip alloy sheet storage device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821698144.9U CN209080524U (en) 2018-10-12 2018-10-12 Neodymium iron boron strip alloy sheet storage device

Publications (1)

Publication Number Publication Date
CN209080524U true CN209080524U (en) 2019-07-09

Family

ID=67119871

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821698144.9U Expired - Fee Related CN209080524U (en) 2018-10-12 2018-10-12 Neodymium iron boron strip alloy sheet storage device

Country Status (1)

Country Link
CN (1) CN209080524U (en)

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GR01 Patent grant
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CP01 Change in the name or title of a patent holder
CP01 Change in the name or title of a patent holder

Address after: 230000 north side of Juner Road, Wanshan Town, Lujiang County, Hefei City, Anhui Province

Patentee after: North rare earth (Anhui) permanent magnet Technology Co.,Ltd.

Address before: 230000 north side of Juner Road, Wanshan Town, Lujiang County, Hefei City, Anhui Province

Patentee before: ANHUI BAO TOU STEEL RARE EARTH PERMANENT MAGNETIC ALLOY INDUSTRY Co.,Ltd.

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190709