CN209077369U - A kind of reaction kettle convenient for cleaning - Google Patents
A kind of reaction kettle convenient for cleaning Download PDFInfo
- Publication number
- CN209077369U CN209077369U CN201821752608.XU CN201821752608U CN209077369U CN 209077369 U CN209077369 U CN 209077369U CN 201821752608 U CN201821752608 U CN 201821752608U CN 209077369 U CN209077369 U CN 209077369U
- Authority
- CN
- China
- Prior art keywords
- shaft
- reaction kettle
- cleaning
- rotating shaft
- outer tube
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 53
- 238000004140 cleaning Methods 0.000 title claims abstract description 45
- 230000007246 mechanism Effects 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 230000009467 reduction Effects 0.000 claims description 15
- 238000010438 heat treatment Methods 0.000 claims description 8
- 230000008450 motivation Effects 0.000 claims 2
- 239000000463 material Substances 0.000 abstract description 7
- 239000007788 liquid Substances 0.000 abstract description 5
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 29
- 238000000034 method Methods 0.000 description 10
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 6
- 230000008569 process Effects 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 229910021529 ammonia Inorganic materials 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000004440 column chromatography Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
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- Accessories For Mixers (AREA)
Abstract
The utility model relates to a kind of reaction kettles convenient for cleaning, including autoclave body, mixing component and the first driving mechanism, the mixing component includes first rotating shaft and agitating paddle, outer tube is equipped on the outside of first rotating shaft, outer tube wall is the hollow structure of lower end closure and top is communicated with water inlet line, outer tube is communicated with the periphery of one group of cleaning sprayer, the second shaft is equipped with below autoclave body, second shaft is rotatablely connected through autoclave body lower surface and with first rotating shaft, second shaft is connected with the clean plate to match with inner wall of kettle shape, clean plate is connected with cleaning brush, when needing to clear up reaction kettle after reaction, opening liquid reserve tank valve makes in outer tube wall full of water, it is sprayed by cleaning sprayer to inner wall of kettle surrounding, starting the second driving mechanism simultaneously makes the second shaft drive clean plate rotation, reaction kettle inner wall is cleaned to realize, this setting Reaction kettle inner wall can be cleared up automatically after reaction in reaction kettle materials inside, improve the efficiency and quality of cleaning reaction kettle.
Description
Technical field
The utility model relates to field of chemical equipment more particularly to a kind of reaction kettles convenient for cleaning.
Background technique
Acetonitrile also known as methyl cyanide, colourless liquid, highly volatile have the special odor similar to ether, can dissolve it is a variety of it is organic,
Inorganic and gaseous matter is the organic solvent of function admirable and the important source material of fine chemistry industry, and acetonitrile is also as mobile phase point
From molecule, it is usually used in column chromatography and more modern high performance liquid chromatography.Industrially, there are many method for synthesizing acetonitrile, have acetic acid with
The side of the direct synthesis techniques such as ammonia reacts, propane is reacted with ammonia, ethyl alcohol is reacted with ammonia and synthesis of acrylonitrile while by-product acetonitrile
Method, the agitating device of various materials being combined by reaction kettle is realized in existing acetonitrile reaction kettle, makes object by heating
Material sufficiently reaction synthesis acetonitrile, obtains the acetonitrile of higher purity using processes such as filter, rectifying, acetonitrile is synthesized in reaction kettle
Afterwards, it since the reaction time continues longer, is gone on smoothly to guarantee that next round synthesizes acetonitrile reaction, therefore operator needs pair
Reaction kettle is cleaned, and reaction kettle is usually all integral structure, and the method for conventional clean reaction kettle injects water in reaction kettle, so
The method for removing shock residue by stirring paddle stirring water flow afterwards, cleaning efficiency is low, and often occurs cleaning sordid problem.
Utility model content
Technical problem to be solved in the utility model is to overcome the deficiencies in the prior art, is provided a kind of convenient for clear
The reaction kettle washed.
The utility model is to be achieved by the following technical programs:
A kind of reaction kettle convenient for cleaning, including autoclave body, mixing component and the first driving mechanism, the mixing component packet
It includes the first rotating shaft being connected with the first driving mechanism and is fixed in the agitating paddle of first rotating shaft lower part, the autoclave body upper surface
Equipped with upper capping, the first rotating shaft is rotatablely connected through upper capping and with upper capping, which is characterized in that outside the first rotating shaft
Side is equipped with outer tube, and the outer tube wall is the hollow structure of lower end closure and top is communicated with water inlet line, outer tube upper end with it is upper
Cover affixed, the outer tube is communicated with the periphery of one group of cleaning sprayer, it is equipped with the second driving mechanism below the autoclave body, described second
Driving mechanism is communicated with the second shaft, and second shaft is rotatablely connected through autoclave body lower surface and with first rotating shaft, and second turn
Axis connection has the clean plate to match with inner wall of kettle shape, and the clean plate is connected with cleaning brush, the cleaning brush and autoclave body
Inner wall fits closely.
According to the above technical scheme, it is preferable that the water inlet line is equipped with heating device.
According to the above technical scheme, it is preferable that be connected between the clean plate and the second shaft by support plate.
According to the above technical scheme, it is preferable that be connected with securing plate between the clean plate and the second shaft.
According to the above technical scheme, it is preferable that there are four clean plates for the second shaft surrounding connection.
According to the above technical scheme, it is preferable that first driving mechanism include first motor and with first motor phase
The first reduction gearbox even, first reduction gearbox are connected with first rotating shaft, second driving mechanism include the second motor and
The second reduction gearbox being connected with the second motor, second reduction gearbox are connected with the second shaft.
According to the above technical scheme, it is preferable that second shaft upper surface is provided with groove, and the first rotating shaft lower end is set
It is rotatablely connected in groove and with groove lower surface by ball.
The beneficial effects of the utility model are:
When needing to clear up reaction kettle after reaction, opening the liquid reserve tank valve being connected to water inlet line makes to fill in outer tube wall
Full water is sprayed by one group of cleaning sprayer that outer tube surrounding is connected to inner wall of kettle surrounding, while the second driving mechanism of starting makes
Second shaft drives clean plate rotation, to be cleaned by cleaning brush to reaction kettle inner wall, this setting can be in reaction kettle
Automatically reaction kettle inner wall is cleared up after portion's material reaction, improves the efficiency and quality of cleaning reaction kettle.
Detailed description of the invention
Fig. 1 is the schematic view of the front view of the utility model.
Fig. 2 is the present invention looks up structural representation of the utility model.
In figure: 1. first motors, 2. first reduction gearboxes, 3. autoclave bodies, 4. heating mantles, 5. clean plates, 6. support plates, 7. rollings
Pearl, 8. securing plates, 9. second driving mechanisms, 10. second shafts, 11. cleaning brush, 12. heating devices, 13. outer tubes, 14. cleanings
Spray head, 15. first rotating shafts.
Specific embodiment
In order to make those skilled in the art more fully understand the technical solution of the utility model, with reference to the accompanying drawing
The utility model is described in further detail with most preferred embodiment.
As shown, the utility model includes autoclave body 3, mixing component and the first driving mechanism, the mixing component packet
Include the first rotating shaft 15 being connected with the first driving mechanism and the agitating paddle for being fixed in 15 lower part of first rotating shaft, the autoclave body 3
Upper surface is equipped with upper capping, the first rotating shaft 15 through upper capping and with upper capping rotation connection, which is characterized in that described the
Outer tube 13 is equipped on the outside of one shaft 15,13 tube wall of outer tube is the hollow structure of lower end closure and top is communicated with water inlet pipe
Road, 13 upper end of outer tube and upper capping are affixed, and the outer tube 13 is communicated with the periphery of one group of cleaning sprayer 14, sets below the autoclave body 3
There is the second driving mechanism 9, second driving mechanism 9 is communicated with the second shaft 10, and second shaft 10 runs through 3 following table of autoclave body
Face is simultaneously rotatablely connected with first rotating shaft 15, and the second shaft 10 is connected with the clean plate 5 to match with 3 inner wall shape of autoclave body, described
Clean plate 5 is connected with cleaning brush 11, and the cleaning brush 11 is fitted closely with 3 inner wall of autoclave body, is enclosed with heating outside the autoclave body 3
Set 4, autoclave body 3 are equipped with inlet port and outlet port, the cover board for sealing it are equipped on the outside of the inlet port and outlet port, when anti-
Should after when needing to clear up reaction kettle, opening liquid reserve tank valve be connected to water inlet line makes 13 tube wall of outer tube is interior to be full of water, passes through
One group of cleaning sprayer 14 of 13 surrounding of outer tube connection is sprayed to 3 inner wall surrounding of autoclave body, while the second driving mechanism 9 of starting makes second
Shaft 10 drives clean plate 5 to rotate, to be cleaned by cleaning brush 11 to reaction kettle inner wall, this setting can be in reaction kettle
Automatically reaction kettle inner wall is cleared up after portion's material reaction, improves the efficiency and quality of cleaning reaction kettle.
According to above-described embodiment, it is preferable that the water inlet line is equipped with heating device 12, to the cleaning in water inlet line
Water, which carries out heating, can be improved the temperature of ejected wash water, softens the residuals in reaction kettle after reaction suitably, is conducive to
Cleaning effect.
According to above-described embodiment, it is preferable that it is connected between the clean plate 5 and the second shaft 10 by support plate 6, the
Clean plate 5 is driven by support plate 6 when two shafts 10 rotate, so that cleaning brush 11 is bonded the movement of 3 inner wall of autoclave body and completes cleaning.
According to above-described embodiment, it is preferable that be connected with securing plate 8, securing plate between the clean plate 5 and the second shaft 10
8 setting strengthens bonding strength so that connect even closer between clean plate 5 and the second shaft 10.
According to above-described embodiment, it is preferable that there are four clean plates 5 for 10 surrounding of the second shaft connection, suitably increase
With the contact area of 3 inner wall of autoclave body, cleaning efficiency is improved.
According to above-described embodiment, it is preferable that first driving mechanism include first motor 1 and with 1 phase of first motor
The first reduction gearbox 2 even, first reduction gearbox 2 are connected with first rotating shaft 15, and first motor 1 is driven by the first reduction gearbox 2
First rotating shaft 15 drives agitating paddle rotation to complete the stirring operation in reaction process, and second driving mechanism 9 includes the second electricity
Machine and the second reduction gearbox being connected with the second motor, second reduction gearbox are connected with the second shaft 10, and the second motor passes through
The cleaning operation that second reduction gearbox drives the second shaft 10 that the rotation of clean plate 5 is driven to complete 3 inner wall of team's autoclave body.
According to above-described embodiment, it is preferable that 10 upper surface of the second shaft is provided with groove, 15 lower end of first rotating shaft
It is placed in groove and is rotatablely connected with groove lower surface by ball 7,15 lower end of first rotating shaft and groove lower surface are equal in this example
Equipped with the arc groove matched with ball 7, make to be rotatablely connected and the two between first rotating shaft 15 and the second shaft 10 by ball 7
Rotation process is not interfere with each other, this setting reaction whipping process can be separately controlled with cleaning process, can both be carried out simultaneously,
Stirrings can be waited to carry out prune job again after the completion.
When needing to clear up reaction kettle after reaction, opening the liquid reserve tank valve being connected to water inlet line makes in 13 tube wall of outer tube
It full of water, is sprayed by one group of cleaning sprayer 14 that 13 surrounding of outer tube is connected to 3 inner wall surrounding of autoclave body, while starting the second driving
Mechanism 9 makes the second shaft 10 that clean plate 5 be driven to rotate, to be cleaned by cleaning brush 11 to reaction kettle inner wall, this setting
Reaction kettle inner wall can be cleared up automatically after reaction in reaction kettle materials inside, improve the efficiency and quality of cleaning reaction kettle.
The above is only the preferred embodiment of the utility model, it is noted that for the common skill of the art
For art personnel, without departing from the principle of this utility model, several improvements and modifications can also be made, these improve and
Retouching also should be regarded as the protection scope of the utility model.
Claims (7)
1. a kind of reaction kettle convenient for cleaning, including autoclave body, mixing component and the first driving mechanism, the mixing component include
The first rotating shaft that is connected with the first driving mechanism and the agitating paddle for being fixed in first rotating shaft lower part, the autoclave body upper surface is set
There is upper capping, the first rotating shaft is rotatablely connected through upper capping and with upper capping, which is characterized in that on the outside of the first rotating shaft
Equipped with outer tube, the outer tube wall is the hollow structure of lower end closure and top is communicated with water inlet line, outer tube upper end and upper envelope
Cover affixed, the outer tube is communicated with the periphery of one group of cleaning sprayer, and the second driving mechanism is equipped with below the autoclave body, and described second drives
Motivation structure is communicated with the second shaft, and second shaft is rotatablely connected through autoclave body lower surface and with first rotating shaft, the second shaft
It is connected with the clean plate to match with inner wall of kettle shape, the clean plate is connected with cleaning brush, in the cleaning brush and autoclave body
Wall fits closely.
2. a kind of reaction kettle convenient for cleaning according to claim 1, which is characterized in that the water inlet line is equipped with heating
Device.
3. a kind of reaction kettle convenient for cleaning according to claim 1, which is characterized in that the clean plate and the second shaft it
Between be connected by support plate.
4. a kind of reaction kettle convenient for cleaning according to claim 3, which is characterized in that the clean plate and the second shaft it
Between be connected with securing plate.
5. a kind of reaction kettle convenient for cleaning according to claim 4, which is characterized in that the second shaft surrounding is connected with
Four clean plates.
6. a kind of reaction kettle convenient for cleaning according to claim 1, which is characterized in that first driving mechanism includes the
One motor and the first reduction gearbox being connected with first motor, first reduction gearbox are connected with first rotating shaft, and described second drives
Motivation structure includes the second motor and the second reduction gearbox for being connected with the second motor, and second reduction gearbox is connected with second turn
Axis.
7. according to claim 1 to any one of 6 a kind of reaction kettle convenient for cleaning, which is characterized in that described
Two shaft upper surfaces are provided with groove, and the first rotating shaft lower end, which is placed in groove and is rotated with groove lower surface by ball, to be connected
It connects.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821752608.XU CN209077369U (en) | 2018-10-26 | 2018-10-26 | A kind of reaction kettle convenient for cleaning |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821752608.XU CN209077369U (en) | 2018-10-26 | 2018-10-26 | A kind of reaction kettle convenient for cleaning |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209077369U true CN209077369U (en) | 2019-07-09 |
Family
ID=67121040
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821752608.XU Expired - Fee Related CN209077369U (en) | 2018-10-26 | 2018-10-26 | A kind of reaction kettle convenient for cleaning |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209077369U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110918031A (en) * | 2019-11-26 | 2020-03-27 | 湖南力泓新材料科技股份有限公司 | Zinc sulfate production is with reation kettle convenient to wash |
| CN110975787A (en) * | 2019-12-06 | 2020-04-10 | 浙江理工大学 | Phase change functional additive mixing arrangement |
| CN112569892A (en) * | 2020-12-31 | 2021-03-30 | 驻马店恒瑞高温节能材料有限公司 | Energy-conserving material raw materials reation kettle of high temperature convenient to wash |
| CN113799271A (en) * | 2021-10-09 | 2021-12-17 | 江昌启 | Tangent plane adsorbent cleaning system for special ceramic processing |
-
2018
- 2018-10-26 CN CN201821752608.XU patent/CN209077369U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110918031A (en) * | 2019-11-26 | 2020-03-27 | 湖南力泓新材料科技股份有限公司 | Zinc sulfate production is with reation kettle convenient to wash |
| CN110975787A (en) * | 2019-12-06 | 2020-04-10 | 浙江理工大学 | Phase change functional additive mixing arrangement |
| CN112569892A (en) * | 2020-12-31 | 2021-03-30 | 驻马店恒瑞高温节能材料有限公司 | Energy-conserving material raw materials reation kettle of high temperature convenient to wash |
| CN113799271A (en) * | 2021-10-09 | 2021-12-17 | 江昌启 | Tangent plane adsorbent cleaning system for special ceramic processing |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190709 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |