CN209039061U - The preparation facilities of melamine based porous materials - Google Patents
The preparation facilities of melamine based porous materials Download PDFInfo
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- CN209039061U CN209039061U CN201821756042.8U CN201821756042U CN209039061U CN 209039061 U CN209039061 U CN 209039061U CN 201821756042 U CN201821756042 U CN 201821756042U CN 209039061 U CN209039061 U CN 209039061U
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- conveying pipeline
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Abstract
The utility model discloses a kind of preparation facilities of melamine based porous materials, including first support, first partition is set in first support, water tank is set gradually in first partition from left to right, second support, first storage tank, back flow reaction kettle is set in second support, feed inlet is set on the kettle cover of back flow reaction kettle, condense hole, second support is located relatively at the top setting second partition of back flow reaction kettle, the through-hole being adapted with feed inlet is set on second partition, condensing tower is provided on second partition, condensing tower is internally provided with condenser pipe, the condenser pipe is connect by the first connecting tube with condensation hole, for fixing the fixation device of the first connecting tube on second partition.The utility model has the beneficial effects that: raw material good dispersion in conveying pipeline, is not easy retrogradation agglomeration, is advantageously implemented continuous production.
Description
Technical field
The utility model relates generally to the technical field of porous material, the system of specifically a kind of melamine based porous materials
Standby device.
Background technique
Melamine based porous materials are mainly using melamine as raw material in the prior art, under the action of catalyst and first
Polymerization reaction occurs for aldehyde, catalyst etc., and then calcining removal surfactant, obtains ordered mesoporous carbon, one side cost with this
It is higher, the difficult assurance difficult to control of another aspect reaction end, and resin molecular weight variation is greatly, stability is poor, easy retrogradation agglomeration, uncomfortable
Continuous production is closed, the yield of melamine based porous materials is limited, realizes the continuous metaplasia of melamine based porous materials
It produces, still needs to do a large amount of research and development.
Utility model content
To solve deficiency in the prior art, the utility model provides a kind of preparation dress of melamine based porous materials
Set, raw material good dispersion in conveying pipeline, be advantageously implemented continuous production, product percent opening up to 95% or more and arrangement of apertures it is equal
It is even, realize the enhancing to porous material comprehensive performance.
The utility model to achieve the above object, is achieved through the following technical solutions:
One aspect according to the present utility model provides a kind of preparation facilities of melamine based porous materials, including
One bracket is arranged first partition in the first support, sets gradually water tank, second in the first partition from left to right
Back flow reaction kettle is arranged in the second support for frame, the first storage tank, and feed inlet, cold is arranged on the kettle cover of the back flow reaction kettle
Solidifying hole, the second support are located relatively at the top setting second partition of back flow reaction kettle, on the second partition setting with into
Material mouth adaptable through-hole is provided with condensing tower on the second partition, and the condensing tower is internally provided with condenser pipe, described cold
Solidifying pipe is connect by the first connecting tube with condensation hole, for fixing the fixation device of the first connecting tube on the second partition；
The first support is located at the lower section setting conveying pipeline and the second storage tank of first partition, the front end of the conveying pipeline with
Back flow reaction kettle connection, the rear end of the conveying pipeline are connected to the second storage tank, and the second connecting tube, institute are arranged on second storage tank
It states and the first delivery pump is set in the second connecting tube, the other end of second connecting tube is connected to the first storage tank；
Conveyer device&apos are set in the conveying pipeline, and conveyer device&apos one end is connect with auger motor drive, outside the conveying pipeline
Portion is arranged outer tube, and several inlet tubes, outlet tube are arranged on the outer tube, and the inlet tube, outlet tube are connected to water tank,
Second delivery pump is set on the inlet tube.
Surge tank is set between the conveying pipeline and back flow reaction kettle, third storage tank is set in the first partition, it is described
Third storage tank is connected to by third connecting tube with surge tank, several baffle plates setting up and down in the surge tank, is located at bottom
Baffle plate be arranged arc conduction part.
The conveying pipeline is located relatively between the helical blade of conveyer device&apos the baffle that is staggered, so that the material in conveying pipeline
S-type flowing.
It is arranged reacting kettle jacketing outside the back flow reaction kettle, being formed between the reacting kettle jacketing and reaction kettle autoclave body can
The interlayer space of conduction oil is filled, is arranged on the reacting kettle jacketing several for assigning the nozzle of heating tube.
Several electric heating tubes of setting and temperature sensor in first storage tank
Comparison and the prior art, the utility model beneficial effect are:
1, the preparation facilities of the exemplary melamine based porous materials of the utility model, in first partition from left to right successively
Water tank, second support, the first storage tank are set, back flow reaction kettle is set in the second support, raw material good dispersion in conveying pipeline,
It is not easy retrogradation agglomeration, is advantageously implemented continuous production.
2, several baffle plates setting up and down in the utility model surge tank, the baffle plate setting arc positioned at bottom drain
Portion mixes raw material before entering conveying pipeline, and mixture is heated to 65-135 DEG C, and controls the time of delivery of product
It is 8-18 minutes, mixture is sufficiently stirred, is conducive to carry out polycondensation reaction in conveying pipeline.
3, the utility model conveying pipeline is located relatively between the helical blade of conveyer device&apos the baffle that is staggered, so that conveying pipeline
The S-type flowing of interior material, is conducive to raw material and sufficiently flows in conveying pipeline, increases the uniformity of raw material, when being conducive to pyrolysis
Hole is evenly distributed.
Detailed description of the invention
Attached drawing 1 is the structural schematic diagram of the preparation facilities of melamine based porous materials；
Attached drawing 2 is the structural schematic diagram of back flow reaction kettle；
Attached drawing 3 is the structural schematic diagram of conveying pipeline；
Attached drawing 4 is the structural schematic diagram of surge tank；
Attached drawing 5 is the cross-sectional view of the first storage tank.
Label shown in attached drawing: 1, first support；11, first partition；12, second support；13, second partition；2, water tank；
3, back flow reaction kettle；31, condensing tower；32, condenser pipe；33, feed inlet；34, the first connecting tube；4, the first storage tank；41, electric heating
Pipe；42, temperature sensor；5, the second storage tank；51, the second connecting tube；52, the first delivery pump；6, conveying pipeline；61, conveying twists
Dragon；62, auger motor；63, outer tube；64, inlet tube；65, outlet tube；66, the second delivery pump；67, baffle；7, surge tank；
71, baffle plate；72, arc conduction part；8, third storage tank；9, reacting kettle jacketing；91, nozzle.
Specific embodiment
With reference to the drawings and specific embodiments, the utility model is described in further detail.It should be understood that these embodiments are only used for
Illustrate the utility model rather than limitation the scope of the utility model.In addition, it should also be understood that, having read the utility model instruction
Content after, those skilled in the art can make various changes or modifications the utility model, and such equivalent forms are equally fallen
In the scope of the appended claims of the present application.
Embodiment 1:
The present embodiment provides a kind of preparation facilities of melamine based porous materials, including first support 1, described first
First partition 11 is set on frame 1, sets gradually water tank 2, second support 12, the first storage tank from left to right in the first partition 11
4, water tank 2 is interior to be arranged heating system, heats water to set temperature；Back flow reaction kettle 3 is set in the second support 12, it is described
Several electric heating tubes 41 of setting and temperature sensor 42 in first storage tank 4.
Feed inlet 33, condensation hole are set on the kettle cover of the back flow reaction kettle 3, and the second support 12 is located relatively at reflux
Second partition 13 is arranged in the top of reaction kettle 3, and the through-hole that setting is adapted with feed inlet 33 on the second partition 13 is described
It is provided with condensing tower 31 on second partition 13, the condensing tower 31 is internally provided with condenser pipe 32, and the condenser pipe 32 passes through the
One connecting tube 34 is connect with condensation hole, for fixing the fixation device of the first connecting tube 34 on the second partition 13.
The first support 1 is located at the lower section setting conveying pipeline 6 and the second storage tank 5 of first partition 11, the conveying pipeline 6
Front end is connected to back flow reaction kettle 3, and the rear end of the conveying pipeline 6 is connected to the second storage tank 5, and is arranged on second storage tank 5
The first delivery pump 52, the other end and first of second connecting tube 51 is arranged in second connecting tube 51 in two connecting tubes 51
Storage tank 4 is connected to；
Conveyer device&apos 61 are set in the conveying pipeline 6, and 61 one end of conveyer device&apos and auger motor 62 are sequentially connected, described defeated
It is arranged outer tube 63 outside expects pipe 6, several inlet tubes 64, outlet tube 65 are set on the outer tube 63, the inlet tube 64 goes out
Liquid pipe 65 is connected to water tank 2, and the second delivery pump 66 is arranged on the inlet tube 64.
Embodiment 2:
The present embodiment feature same as Example 1 repeats no more, and the present embodiment is different from embodiment 1 to be characterized in that:
Surge tank 7 is set between the conveying pipeline 6 and back flow reaction kettle 3, holds toluene part, n-butanol in surge tank 7；Make
Used time is added in surge tank 7 according to set ratio uniform, and third storage tank 8, the third storage tank 8 are arranged in the first partition 11
It is connected to by third connecting tube with surge tank 7,2-6 baffle plate 71 setting up and down in the surge tank 7, positioned at the folding of bottom
Arc conduction part 72 is arranged in flowing plate 71, and each raw material is mixed into conveying pipeline 6.
Embodiment 3:
The present embodiment feature same as Example 1 repeats no more, and the present embodiment is different from embodiment 1 to be characterized in that:
The conveying pipeline 6 is located relatively between the helical blade of conveyer device&apos 61 baffle 67 that is staggered, so that in conveying pipeline 6
The S-type flowing of material, be conducive to raw material and sufficiently flowed in conveying pipeline 6, increase the uniformity of raw material, be conducive to pyrolysis when hole
Gap is evenly distributed.
Embodiment 4:
The present embodiment feature same as Example 1 repeats no more, and the present embodiment is different from embodiment 1 to be characterized in that:
It is arranged reacting kettle jacketing 9 outside the back flow reaction kettle 3, is formed between the reacting kettle jacketing 9 and reaction kettle autoclave body
Have the interlayer space that can fill conduction oil, be arranged on the reacting kettle jacketing 9 it is several for assigning the nozzles 91 of heating tube, using adding
Heat pipe is heated to set temperature when carrying out back flow reaction, by the material in back flow reaction kettle 3.
Above description is only the preferred embodiment of the application and the explanation to institute's application technology principle.Those skilled in the art
Member is it should be appreciated that utility model range involved in the application, however it is not limited to made of the specific combination of above-mentioned technical characteristic
Technical solution, at the same should also cover do not depart from the utility model design in the case where, by above-mentioned technical characteristic or its be equal
Feature carries out any combination and other technical solutions for being formed.Such as features described above and (but being not limited to) disclosed herein have
There are similar functions.
Claims (5)
1. a kind of preparation facilities of melamine based porous materials, which is characterized in that including first support, in the first support
First partition is set, sets gradually water tank, second support, the first storage tank in the first partition from left to right, described second
Back flow reaction kettle is set on frame, feed inlet, condensation hole are set on the kettle cover of the back flow reaction kettle, and the second support is with respect to position
In the top of back flow reaction kettle, second partition is set, the through-hole that setting is adapted with feed inlet on the second partition, described the
Be provided with condensing tower on two partitions, the condensing tower is internally provided with condenser pipe, the condenser pipe by the first connecting tube with it is cold
Solidifying hole connects, for fixing the fixation device of the first connecting tube on the second partition；
The first support is located at lower section setting conveying pipeline and the second storage tank, the front end of the conveying pipeline and the reflux of first partition
Reaction kettle connection, the rear end of the conveying pipeline is connected to the second storage tank, is arranged the second connecting tube on second storage tank, and described the
First delivery pump is set in two connecting tubes, and the other end of second connecting tube is connected to the first storage tank；
Conveyer device&apos are set in the conveying pipeline, and conveyer device&apos one end is connect with auger motor drive, the conveying pipeline outer cover
If outer tube, several inlet tubes, outlet tube are set, and the inlet tube, outlet tube are connected to water tank, described on the outer tube
Second delivery pump is set on inlet tube.
2. the preparation facilities of melamine based porous materials according to claim 1, which is characterized in that the conveying pipeline with
Surge tank is set between back flow reaction kettle, third storage tank is set in the first partition, the third storage tank is connected by third
Pipe is connected to surge tank, several baffle plates setting up and down in the surge tank, and the baffle plate setting arc positioned at bottom drains
Portion.
3. the preparation facilities of melamine based porous materials according to claim 1, which is characterized in that the conveying pipeline phase
Between the baffle that is staggered the helical blade for being located at conveyer device&apos, so that the S-type flowing of material in conveying pipeline.
4. the preparation facilities of melamine based porous materials according to claim 1, which is characterized in that the back flow reaction
It is arranged reacting kettle jacketing outside kettle, the interlayer space that can fill conduction oil is formed between the reacting kettle jacketing and reaction kettle autoclave body,
It is arranged on the reacting kettle jacketing several for assigning the nozzle of heating tube.
5. the preparation facilities of melamine based porous materials according to claim 1, which is characterized in that first storage tank
It is interior that several electric heating tubes and temperature sensor are set.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821756042.8U CN209039061U (en) | 2018-10-16 | 2018-10-16 | The preparation facilities of melamine based porous materials |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821756042.8U CN209039061U (en) | 2018-10-16 | 2018-10-16 | The preparation facilities of melamine based porous materials |
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| Publication Number | Publication Date |
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| CN209039061U true CN209039061U (en) | 2019-06-28 |
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| CN201821756042.8U Active CN209039061U (en) | 2018-10-16 | 2018-10-16 | The preparation facilities of melamine based porous materials |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109264694A (en) * | 2018-10-16 | 2019-01-25 | 蚌埠学院 | The preparation method and device of melamine based porous materials |
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2018
- 2018-10-16 CN CN201821756042.8U patent/CN209039061U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109264694A (en) * | 2018-10-16 | 2019-01-25 | 蚌埠学院 | The preparation method and device of melamine based porous materials |
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