CN209033785U - A kind of high boiling component distillation heater - Google Patents

A kind of high boiling component distillation heater Download PDF

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Publication number
CN209033785U
CN209033785U CN201821778008.0U CN201821778008U CN209033785U CN 209033785 U CN209033785 U CN 209033785U CN 201821778008 U CN201821778008 U CN 201821778008U CN 209033785 U CN209033785 U CN 209033785U
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China
Prior art keywords
heating
distillation
chamber
fixed bucket
heater
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CN201821778008.0U
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Inventor
王超学
王丽曼
徐文辉
刘强
梁明杰
韩吉茂
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Xinhua Pharmaceutical (shou Guang) Co Ltd
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Xinhua Pharmaceutical (shou Guang) Co Ltd
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Abstract

The utility model relates to chemical technology fields, specifically a kind of high boiling component distills heater, including heating mechanism, distill mechanism and separating mechanism, the heating mechanism includes energy-saving electromagnetic heating device and fixed bucket, the energy-saving electromagnetic heating device and fixed bucket are disposed adjacent, the outer wall of the fixed bucket is made of thermal insulation material, the inner wall of fixed bucket is made of heat-conducting pad, accommodating chamber is equipped in the side wall of the fixed bucket, heating coil is equipped in the accommodating chamber, one end of the heating coil is connect with energy-saving electromagnetic heating device, the distillation mechanism includes distillation still, the lower end of the distillation still is located in fixed bucket, the interior of distillation still is equipped with heating chamber and distillation chamber, the heating chamber is located at the lower end of distillation chamber, conduction oil is equipped in the heating chamber.The utility model has the beneficial effects that homogeneous heating temperature, easy to operate and high heating temperature distillation heater, can precise control of temperature, safety is higher.

Description

A kind of high boiling component distillation heater
Technical field
The utility model relates to chemical technology field, specifically a kind of high boiling component distills heater.
Background technique
China Patent No. is the distillation equipment that CN205216239U is announced, and distillation equipment is by three heating rings to distillation still Interior mixed solution is heated, and three heating rings are divided into upper, middle and lower three-layer set, is existed centainly between adjacent heating ring Distance, it is easy to cause distance heating ring into position solution temperature than distance heating ring distant positions solution temperature it is high, hold It is uneven to easily cause heating, and mixed solution is exactly so that solution is evaporated and is separated using the difference of different liquids boiling point, because This, above-mentioned patent, hence it is evident that it is uneven to will lead to solution heating.
It heats separation high boiling component to mixed solution at present mostly to heat using steam jacket, disadvantage is obvious: (1) High boiling component distillation required temperature is not achieved in vapor (steam) temperature highest 180 degree or so, and distillation rear impurity is more, and product yield is low;(2) Operate more complicated, there are security risks;(3) steam heated pressure is unstable, and temperature should not control;(4) uneven heating is even, thermal effect Rate is low.
In view of the above-mentioned problems, needing a kind of distillation heating with homogeneous heating temperature, easy to operate and high heating temperature Device.
Utility model content
The purpose of this utility model is to provide a kind of high boiling components to distill heater, to solve in above-mentioned background technique The problem of proposition.
The technical solution of the utility model is: including heating mechanism, distillation mechanism and separating mechanism, the distillation mechanism is solid Dingan County is mounted in the upper end of heating mechanism, and the separating mechanism is located at the side of distillation mechanism and the two is connected to by pipeline, described Heating mechanism includes energy-saving electromagnetic heating device and fixed bucket, and the energy-saving electromagnetic heating device and fixed bucket are disposed adjacent, described solid Surely the outer wall to struggle against is made of thermal insulation material, and the inner wall of fixed bucket is made of heat-conducting pad, is equipped with and holds in the side wall of the fixed bucket It receives chamber, heating coil is equipped in the accommodating chamber, one end of the heating coil is connect with energy-saving electromagnetic heating device, the distillation Mechanism includes distillation still, and in fixed bucket, the interior of distillation still is equipped with heating chamber and distills chamber, described for the lower end of the distillation still Heating chamber is located at the lower end of distillation chamber, is equipped with conduction oil in the heating chamber.
In one preferred embodiment of the utility model, the outside of the distillation still is equipped with fixed frame, and the fixation struggles against upper End is fixedly connected by bolt with fixed frame.
In one preferred embodiment of the utility model, the lower end of the distillation still is equipped with flowline, the flowline with plus The side wall of the connection of hot chamber, the distillation still is equipped with oil inlet pipe and feed pipe, and the oil inlet pipe is connected to heating chamber, feed pipe and Chamber connection is distilled, control valve is equipped on the flowline, oil inlet pipe and feed pipe, the upper end of the distillation still is equipped with exhaust Pipe.
In one preferred embodiment of the utility model, the separating mechanism includes first-stage condenser, secondary condenser and divides It is connected between first-stage condenser and exhaust pipe described in device by pipeline, is passed through between the secondary condenser and first-stage condenser Pipeline connection, the separator is located at the lower section of secondary condenser and is connected between the two by pipeline, under the separator End is equipped with drainage conduit.
In one preferred embodiment of the utility model, return pipe, the separation are equipped between the separator and exhaust pipe It is connected between device and exhaust pipe by return pipe.
In one preferred embodiment of the utility model, the outside of the energy-saving electromagnetic heating device is equipped with temp controlled meter, ammeter And control knob.
The utility model provides a kind of high boiling component distillation heater, compared with prior art, tool by improving herein There are following improvement and advantage:
(1) the utility model cost is relatively low and can be realized without pressure heat, it is easy to control, securely and reliably;
(2) easy to operate compared with the steam heating for needing mating steam boiler, it is controlled by control knob;
(3) easy control of temperature can be realized accurate temperature control;
(4) 300 degree of heating temperature highest or so, high boiling component distillation required temperature can be reached, distillation rear impurity is few, Product yield is high;
(5) electromagnetic heating conduction oil interlayer keeps heated liquid area in kettle big, homogeneous heating, and the thermal efficiency is high, and utilization rate is Relatively high.
Detailed description of the invention
The utility model is further explained with reference to the accompanying drawings and examples:
Fig. 1 is the schematic perspective view of the utility model;
Fig. 2 is the partial top view one of the utility model;
Fig. 3 is cross-sectional view of the Fig. 2 along A-A line;
Fig. 4 is the partial top view two of the utility model;
Fig. 5 is cross-sectional view of the Fig. 4 along B-B line;
Description of symbols: heating mechanism 1, energy-saving electromagnetic heating device 1a, fixed bucket 1b, distillation mechanism 2, distillation still 2a, Heating chamber 2a1 distills chamber 2a2, and separating mechanism 3, first-stage condenser 3a, secondary condenser 3b, separator 3c, drainage conduit 3d hold Receive chamber 4, heating coil 5, fixed frame 6, flowline 7, oil inlet pipe 8, feed pipe 9, control valve 10, exhaust pipe 11, return pipe 12.
Specific embodiment
The utility model is described in detail below in conjunction with attached drawing 1 to Fig. 5, to the skill in the utility model embodiment Art scheme is clearly and completely described, it is clear that and the described embodiments are only a part of the embodiments of the utility model, and The embodiment being not all of.Based on the embodiments of the present invention, those of ordinary skill in the art are not making creativeness Every other embodiment obtained, fall within the protection scope of the utility model under the premise of labour.
The utility model provides a kind of high boiling component distillation heater by improving herein, as Figure 1-Figure 5, including Heating mechanism 1, distillation mechanism 2 and separating mechanism 3, the upper end distilled mechanism 2 and be fixedly mounted on heating mechanism 1, described point Structure 3 of disembarking is located at the side of distillation mechanism 2 and the two is connected to by pipeline, and the heating mechanism 1 includes energy-saving electromagnetic heating device 1a and fixed bucket 1b, the energy-saving electromagnetic heating device 1a and fixed bucket 1b are disposed adjacent, and the outer wall of the fixed bucket 1b is by keeping the temperature Material is made, and the inner wall of fixed bucket 1b is made of heat-conducting pad, is equipped with accommodating chamber 4, the appearance in the side wall of the fixed bucket 1b Chamber 4 of receiving is interior to be equipped with heating coil 5, and one end of the heating coil 5 is connect with energy-saving electromagnetic heating device 1a, the distillation mechanism 2 Including distillation still 2a, the lower end of the distillation still 2a is located in fixed bucket 1b, and the interior of distillation still 2a is equipped with heating chamber 2a1 and distillation Chamber 2a2, the heating chamber 2a1 are located at the lower end of distillation chamber 2a2, and the heating chamber 2a1 is interior to be equipped with conduction oil;Energy-saving electromagnetic heating Device 1a, to the heat-conducting oil heating in heating chamber 2a1, is transferred heat in distillation chamber 2a2 by heating coil 5 by conduction oil Mixed solution heated, the steam after heating is realized by separating mechanism 3 and cooling liquid and is separated, and heat-conducting pad is used In separating heating necklace and distillation still 2a, avoiding contacting between the two causes distillation still 2a to damage at high temperature.
The outside of the distillation still 2a is equipped with fixed frame 6, and the upper end of the fixed bucket 1b is fixed by bolt and fixed frame 6 Connection;Fixed bucket 1b and distillation still 2a is installed by fixed frame 6.
The lower end of the distillation still 2a is equipped with flowline 7, and the flowline 7 is connected to heating chamber 2a1, the distillation still 2a Side wall be equipped with oil inlet pipe 8 and feed pipe 9, the oil inlet pipe 8 be connected to heating chamber 2a1, feed pipe 9 with distill chamber 2a2 company It connects, control valve 10 is equipped on the flowline 7, oil inlet pipe 8 and feed pipe 9, the upper end of the distillation still 2a is equipped with exhaust pipe 11;Flowline 7 and oil inlet pipe 8 are used to replace the conduction oil in heating chamber 2a1, and feed pipe 9 is used to add into distillation still 2a mixed Close solution.
The separating mechanism 3 includes first-stage condenser 3a described in first-stage condenser 3a, secondary condenser 3b and separator 3c It is connected to, is connected between the secondary condenser 3b and first-stage condenser 3a by pipeline, institute by pipeline between exhaust pipe 11 It states separator 3c to be located at the lower section of secondary condenser 3b and be connected to by pipeline between the two, the lower end of the separator 3c is equipped with Drainage conduit 3d;By first-stage condenser 3a and secondary condenser 3b steam is sufficiently liquefied, then used separator 3c is by solution Separation.
It is equipped with return pipe 12 between the separator 3c and exhaust pipe 11, passes through between the separator 3c and exhaust pipe 11 Return pipe 12 is connected to;After separator 3c separation, part mixed solution is back in distillation still 2a by return pipe 12.
The outside of the energy-saving electromagnetic heating device 1a is equipped with temp controlled meter, ammeter and control knob;Temp controlled meter and electric current become just The working condition of heating mechanism 1 is known in user.
Working principle of the utility model is: when the utility model is used, energy-saving electromagnetic heating device 1a passes through heating coil 5 To the heat-conducting oil heating in heating chamber 2a1, added by the mixed solution that conduction oil transfers heat in distillation chamber 2a2 Heat, it is different by the boiling point of different solutions in mixed solution, certain solution is evaporated, vapor reaches separating mechanism by pipeline 3, it is cooled down and is separated by separating mechanism 3.
The foregoing description of the disclosed embodiments can be realized professional and technical personnel in the field or using originally practical new Type.Various modifications to these embodiments will be readily apparent to those skilled in the art, and determine herein The General Principle of justice can be realized in other embodiments without departing from the spirit or scope of the present utility model.Cause This, the present invention will not be limited to the embodiments shown herein, and is to fit to and principles disclosed herein The widest scope consistent with features of novelty.

Claims (6)

1. a kind of high boiling component distills heater, it is characterised in that: including heating mechanism (1), distillation mechanism (2) and seperator Structure (3), distillation mechanism (2) are fixedly mounted on the upper end of heating mechanism (1), and the separating mechanism (3) is located at distillation mechanism (2) side and the two is connected to by pipeline, and the heating mechanism (1) includes energy-saving electromagnetic heating device (1a) and fixed bucket (1b), the energy-saving electromagnetic heating device (1a) and fixed bucket (1b) are disposed adjacent, and the outer wall of the fixed bucket (1b) is by thermal insulating material Material is made, and the inner wall of fixed bucket (1b) is made of heat-conducting pad, is equipped with accommodating chamber (4) in the side wall of the fixed bucket (1b), institute It states in accommodating chamber (4) and is equipped with heating coil (5), one end of the heating coil (5) is connect with energy-saving electromagnetic heating device (1a), institute Stating distillation mechanism (2) includes distillation still (2a), and the lower end of the distillation still (2a) is located in fixed bucket (1b), distillation still (2a) Interior to be equipped with heating chamber (2a1) and distillation chamber (2a2), the heating chamber (2a1) is located at the lower end of distillation chamber (2a2), the heating Conduction oil is equipped in chamber (2a1).
2. high boiling component according to claim 1 distills heater, it is characterised in that: the outside of the distillation still (2a) Equipped with fixed frame (6), the upper end of the fixed bucket (1b) is fixedly connected by bolt with fixed frame (6).
3. high boiling component according to claim 1 distills heater, it is characterised in that: the lower end of the distillation still (2a) Equipped with flowline (7), the flowline (7) is connected to heating chamber (2a1), and the side wall of the distillation still (2a) is equipped with oil inlet pipe (8) it is connected to feed pipe (9), the oil inlet pipe (8) with heating chamber (2a1), feed pipe (9) is connect with distillation chamber (2a2), described It is equipped with control valve (10) on flowline (7), oil inlet pipe (8) and feed pipe (9), the upper end of the distillation still (2a) is equipped with exhaust It manages (11).
4. high boiling component according to claim 3 distills heater, it is characterised in that: the separating mechanism (3) includes Lead between first-stage condenser (3a), secondary condenser (3b) and separator (3c) described first-stage condenser (3a) and exhaust pipe (11) Piping connection, is connected between the secondary condenser (3b) and first-stage condenser (3a) by pipeline, the separator (3c) Positioned at secondary condenser (3b) lower section and be connected between the two by pipeline, the lower end of the separator (3c) is equipped with drainage conduit (3d)。
5. high boiling component according to claim 4 distills heater, it is characterised in that: the separator (3c) and exhaust It manages and is equipped with return pipe (12) between (11), be connected between the separator (3c) and exhaust pipe (11) by return pipe (12).
6. a kind of high boiling component according to claim 1 distills heater, it is characterised in that: the energy-saving electromagnetic heating The outside of device (1a) is equipped with temp controlled meter, ammeter and control knob.
CN201821778008.0U 2018-10-30 2018-10-30 A kind of high boiling component distillation heater Active CN209033785U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821778008.0U CN209033785U (en) 2018-10-30 2018-10-30 A kind of high boiling component distillation heater

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821778008.0U CN209033785U (en) 2018-10-30 2018-10-30 A kind of high boiling component distillation heater

Publications (1)

Publication Number Publication Date
CN209033785U true CN209033785U (en) 2019-06-28

Family

ID=67040539

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821778008.0U Active CN209033785U (en) 2018-10-30 2018-10-30 A kind of high boiling component distillation heater

Country Status (1)

Country Link
CN (1) CN209033785U (en)

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