CN106732289A - A kind of reactor - Google Patents
A kind of reactor Download PDFInfo
- Publication number
- CN106732289A CN106732289A CN201710040111.9A CN201710040111A CN106732289A CN 106732289 A CN106732289 A CN 106732289A CN 201710040111 A CN201710040111 A CN 201710040111A CN 106732289 A CN106732289 A CN 106732289A
- Authority
- CN
- China
- Prior art keywords
- heating
- kettle
- deep fat
- jacket
- series
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F2035/99—Heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/92—Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00085—Plates; Jackets; Cylinders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00092—Tubes
Abstract
The invention discloses a kind of reactor, including kettle, the autoclave body bottom is provided with heating jacket, and the heating jacket is electrically connected with temperature controller；The kettle is provided with thermal trough in heating jacket top surface to kettle top；The thermal trough periphery is disposed with multigroup deep fat pipe；The deep fat pipe periphery is provided with insulation external jacket；The deep fat pipe input and output end enter into connection in series-parallel pipe fitting after extending insulation external jacket；The connection in series-parallel pipe fitting periphery is provided with collet；Multiple regulating valves are provided with the connection in series-parallel pipe fitting；The connection in series-parallel pipe fitting input is connected to circulating pump by electrical heating thermosistor；The present invention proposes a kind of reactor, individually autoclave body bottom is heated using the heating jacket of bottom, packet control is realized by segmented deep fat pipe simultaneously, can be to realizing that the reactant of natural layering carries out sublevel layer computer heating control, while conjuncted control can be realized.
Description
Technical field
The present invention relates to a kind of consersion unit, and in particular to a kind of reactor, belong to consersion unit technical field.
Background technology
The broad understanding of reactor has the container for physically or chemically reacting, and is matched somebody with somebody by the structure design to container and parameter
Put, realize the mixture function of heating, evaporation, cooling and the low high speed of technological requirement；Reactor be widely used in oil, chemical industry,
Rubber, agricultural chemicals, dyestuff, medical treatment, food, for completing to vulcanize, hydrogenate the pressure vessel of the technical process such as nitrification, polymerization, condensation；
Electric heating reacting kettle is the mode of heating that conduction oil is heated using electrothermal tube in kettle set, and this mode of heating is that electrothermal tube is inserted in
In kettle jacket layer, interlayer is full of conduction oil, and electrothermal tube directly heats conduction oil, and conduction oil transfers thermal energy to raw material in kettle again；
The heating system of this mode of heating have profile simple, compact conformation, it is easy to operate the characteristics of, but electric heating in process of production
Pipe directly contact heat-conducting oil heating, normal condition lower electrothermal tube pipe surface temperature is up to 500 ~ 800 degrees Celsius, and conduction oil is allowed
Maximum operating temperature it is general in 300 degrees centigrades, due to local long-time high temperature, to carbonize conduction oil rotten, conduction oil
Heat transfer efficiency constantly declines, and produces substantial amounts of sediment to concentrate on conduction oil jackets inner wall further after conduction oil charing is rotten
The thermal efficiency is reduced, more seriously the cleaning work of sediment is very difficult on jackets inner wall；Therefore, my company produces one
A kind of environmentally friendly electrical heating jacket reactor of money（Chinese Patent Application No.：201620048547.3）, including kettle and electrical heating control
Device processed, the kettle outer wall is provided with chuck, and the chuck is provided with water inlet end and water side, and the water inlet end and water side connect
Electric heating control device, the electric heating control device includes the first electric control valve, plate successively by chilled water approach axis
Formula heat exchanger, electric heater, the second electric control valve, oil circulating pump, filter, the filter are intake by pipeline with chuck
End connection, the chuck water side is connected with flow control valve, plate type heat exchanger in turn, and the plate-type heat-exchange gas is provided with chilled water
Outlet.The present invention prevents heat conduction in chuck and cooling medium precipitation or the solidification from causing heat conduction or cooling performance reduction, while carrying
For heat conduction and the mode of cooling used interchangeably, it is easy to operate；But by using, find for some specific raw material production nothings
Method temperature control well, and layering heating can not be carried out according to kettle, all layering reactants are at same temperature stratum,
In addition, when reaction mass is fewer, it is also desirable to carry out whole machine and start, energy waste is serious.
The content of the invention
To solve the above problems, the present invention proposes a kind of reactor, using the heating jacket of bottom individually to kettle bottom
Portion is heated, while packet control is realized by segmented deep fat pipe, can be to realizing that the reactant of natural layering is divided
Stratum's computer heating control, while conjuncted control can be realized.
Reactor of the invention, including kettle, the autoclave body bottom are provided with heating jacket, the heating jacket electrical connection
There is temperature controller；The kettle is provided with thermal trough in heating jacket top surface to kettle top；The thermal trough periphery is successively
It is provided with multigroup deep fat pipe；The deep fat pipe periphery is provided with insulation external jacket；The deep fat pipe input and output end extend
Connection in series-parallel pipe fitting is entered into after going out to be incubated external jacket；The connection in series-parallel pipe fitting periphery is provided with collet；The connection in series-parallel pipe fitting
On be provided with multiple regulating valves；The connection in series-parallel pipe fitting input is connected to circulating pump by electrical heating thermosistor；The circulation
Pump input is connected to heat exchanger output end；The heat exchanger input is connected to heat-conducting oil heating pot；The kettle top sets
It is equipped with lid；Lead column is provided with outside the kettle；Slide plate is movably installed with the lead column；Install the slide plate bottom surface
There is big pressure telescoping cylinder；The big pressure telescoping cylinder is fixed in lead column；Stirring power mechanism is provided with the lid；Institute
Stirring power mechanism is stated to be installed with the puddler on the inside of kettle.
Further, the heating jacket includes jacket body, and is installed on the heating tube on the inside of jacket body；The heating tube
It is connected to temperature controller.
Further, the connection in series-parallel pipe fitting includes and deep fat pipe input and the tandem tube of output end two；Described in upper one group
The tandem tube of deep fat pipe output end is provided with parallel transistor with the tandem tube of deep fat pipe input described in next group；It is described
Regulating valve is provided with parallel transistor.
Yet further, it is socketed with collet outside the tandem tube and parallel transistor.
Further, the electrical heating thermosistor includes independent heating storehouse；Having heaters is installed in the independent heating storehouse
And temperature sensing device；The heater and temperature sensing device are connected respectively to temperature controller.
Further, the collet includes heat-insulated body, and is installed on the door-plate on front side of heat-insulated body；The door-plate leads to
Bolt is crossed to be fixed with heat-insulated body.
Used as preferred embodiment, deep fat pipe described in every group is constituted by the coil pipe enclosed at least about kettle two；Upper the following group
The coil pipe is close to.
As preferred embodiment, heat-conducting layer is provided between the kettle and thermal trough.
Used as preferred embodiment, the lid inner side is provided with inner seal ring.
Compared with prior art, reactor of the invention is independent to kettle bottom using the heating jacket of bottom for the present invention
Portion is heated, while packet control is realized by segmented deep fat pipe, can be to realizing that the reactant of natural layering is divided
Stratum's computer heating control, while conjuncted control can be realized；When ordinary material is processed, bottom-heated chuck is started, and set temperature
Degree, realizes the heating response of material, and when overall heating is needed, regulating valve of outwarding winding is worked, soon together by all of circulating pump
Speed carries out heat cycles to conduction oil, and realization is rapidly heated and is incubated well；When needing to carry out temperature setting according to stratum,
Regulating valve is closed, and realizes that current line temperature is gathered by electrical heating thermosistor, and realize that the road temperature sets by temperature controller
Fixed and control, completes independent pipeline control.
Brief description of the drawings
Fig. 1 is overall structure diagram of the invention.
Specific embodiment
Embodiment 1：
As shown in figure 1, reactor of the invention, including kettle 1, the bottom of the kettle 1 is provided with heating jacket 2, the heating
Chuck 2 is electrically connected with temperature controller 3；The kettle 1 is provided with thermal trough 4 in the top surface of heating jacket 2 to kettle top；It is described
The periphery of thermal trough 4 is disposed with multigroup deep fat pipe 5；The periphery of deep fat pipe 5 is provided with insulation external jacket 6；The deep fat pipe 5
Input and output end enter into connection in series-parallel pipe fitting 7 after extending insulation external jacket 6；The periphery of connection in series-parallel pipe fitting 7 is provided with
Collet 8；Multiple regulating valves 9 are provided with the connection in series-parallel pipe fitting 7；The input of connection in series-parallel pipe fitting 8 is adjusted by electrical heating
Warm device 10 is connected to circulating pump 11；The input of the circulating pump 11 is connected to the output end of heat exchanger 12；The heat exchanger 12 is input into
End is connected to heat-conducting oil heating pot 13；The top of the kettle 1 is provided with lid 14；Lead column 15 is provided with outside the kettle 1；
Slide plate 16 is movably installed with the lead column 15；The bottom surface of the slide plate 16 is provided with big pressure telescoping cylinder 17；The big pressure
Telescoping cylinder 17 is fixed in lead column 15；Stirring power mechanism 18 is provided with the lid 14；The stirring power mechanism 18
Puddler with the inner side of kettle 1 is installed.
Embodiment 2：
Reactor of the invention, the heating jacket 2 includes jacket body 2a, and is installed on the heating tube 2b on the inside of jacket body；Institute
State heating tube 2b and be connected to temperature controller 3.
Embodiment 3：
Reactor of the invention, the connection in series-parallel pipe fitting 7 includes and deep fat pipe input and the tandem tube 7a of output end two；Upper one group
The tandem tube 7a of the output end of deep fat pipe 5 is provided with simultaneously with the tandem tube of the input of deep fat pipe 5 described in next group
Union 7b；The regulating valve 9 is provided with parallel transistor 7b；Collet is socketed with outside the tandem tube 7a and parallel transistor 7b.
Embodiment 4：
Reactor of the invention, the electrical heating thermosistor 10 includes independent heating storehouse 10a；Peace in the independent heating storehouse 10a
Equipped with heater 10b and temperature sensing device 10c；The heater 10b and temperature sensing device 10c are connected respectively to temperature control
Device.
Wherein, the collet 8 includes heat-insulated body 8a, and is installed on the door-plate 8b on front side of heat-insulated body；The door-plate
8b is fixed by bolt with heat-insulated body 8a.Deep fat pipe 5 described in every group is constituted by the coil pipe enclosed at least about kettle two；Upper the following group
The coil pipe is close to.Heat-conducting layer 19 is provided between the kettle 1 and thermal trough 4.The inner side of the lid 14 is provided with interior sealing
Ring.
Reactor of the invention, is individually heated using the heating jacket of bottom to autoclave body bottom, while by segmentation
Formula deep fat pipe realizes packet control, can be to realizing that the reactant of natural layering carries out sublevel layer computer heating control, while can be real
Existing conjuncted control；When ordinary material is processed, bottom-heated chuck is started, and set temperature, realize the heating response of material, when
When needing overall heating, regulating valve of outwarding winding is worked together by all of circulating pump, quickly carries out heat cycles to conduction oil,
Realization is rapidly heated and is incubated well；When needing to carry out temperature setting according to stratum, regulating valve is closed, and by electrical heating
Thermosistor realizes current line temperature collection, and realizes that the road temperature sets and control by temperature controller, completes independent pipeline control
System.
With above-mentioned according to desirable embodiment of the invention as enlightenment, by above-mentioned description, relevant staff is complete
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property scope is not limited to the content on specification, it is necessary to its technical scope is determined according to right.
Claims (9)
1. a kind of reactor, it is characterised in that：Including kettle, the autoclave body bottom is provided with heating jacket, the heating jacket
It is electrically connected with temperature controller；The kettle is provided with thermal trough in heating jacket top surface to kettle top；Outside the thermal trough
Enclose and be disposed with multigroup deep fat pipe；The deep fat pipe periphery is provided with insulation external jacket；The deep fat pipe input and output
End enters into connection in series-parallel pipe fitting after extending insulation external jacket；The connection in series-parallel pipe fitting periphery is provided with collet；The string is simultaneously
Multiple regulating valves are provided with union part；The connection in series-parallel pipe fitting input is connected to circulating pump by electrical heating thermosistor；Institute
State circulating pump input and be connected to heat exchanger output end；The heat exchanger input is connected to heat-conducting oil heating pot；The kettle
Top is provided with lid；Lead column is provided with outside the kettle；Slide plate is movably installed with the lead column；The slide plate bottom
Face is provided with big pressure telescoping cylinder；The big pressure telescoping cylinder is fixed in lead column；Stirring power is provided with the lid
Mechanism；The stirring power mechanism installs with the puddler on the inside of kettle.
2. reactor according to claim 1, it is characterised in that：The heating jacket includes jacket body, and is installed on folder
Heating tube on the inside of body；The heating tube is connected to temperature controller.
3. reactor according to claim 1, it is characterised in that：The connection in series-parallel pipe fitting include with deep fat pipe input and
The tandem tube of output end two；The institute of the tandem tube of deep fat pipe output end described in upper a group and deep fat pipe input described in next group
State tandem tube and be provided with parallel transistor；The regulating valve is provided with parallel transistor.
4. reactor according to claim 3, it is characterised in that：It is socketed with outside the tandem tube and parallel transistor heat-insulated
Set.
5. reactor according to claim 1, it is characterised in that：The electrical heating thermosistor includes independent heating storehouse；Institute
State installation having heaters and temperature sensing device in independent heating storehouse；The heater and temperature sensing device are connected respectively to temperature
Control device.
6. reactor according to claim 1, it is characterised in that：The collet include heat-insulated body, and be installed on every
Door-plate on front side of hot jacket body；The door-plate is fixed by bolt with heat-insulated body.
7. reactor according to claim 1, it is characterised in that：Deep fat pipe described in every group is by enclosing at least about kettle two
Coil pipe is constituted；Coil pipe described in upper the following group is close to.
8. reactor according to claim 1, it is characterised in that：Heat-conducting layer is provided between the kettle and thermal trough.
9. reactor according to claim 1, it is characterised in that：The lid inner side is provided with inner seal ring.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710040111.9A CN106732289A (en) | 2017-01-20 | 2017-01-20 | A kind of reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710040111.9A CN106732289A (en) | 2017-01-20 | 2017-01-20 | A kind of reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106732289A true CN106732289A (en) | 2017-05-31 |
Family
ID=58944567
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710040111.9A Pending CN106732289A (en) | 2017-01-20 | 2017-01-20 | A kind of reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106732289A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107261887A (en) * | 2017-07-28 | 2017-10-20 | 朱明� | A kind of lubricating oil blending tank |
| CN111389330A (en) * | 2020-03-25 | 2020-07-10 | 河南神马尼龙化工有限责任公司 | Reaction temperature stability maintaining system of adipic acid production system by nitric acid oxidation method |
| CN113840650A (en) * | 2019-09-26 | 2021-12-24 | 株式会社Lg化学 | Esterification reaction apparatus and esterification reaction method |
| CN114904470A (en) * | 2022-04-18 | 2022-08-16 | 安徽省谱诺药化设备有限公司 | Inner cavity uniform heating type stainless steel reaction kettle |
| CN116212770A (en) * | 2023-03-13 | 2023-06-06 | 南通太洋高新材料科技有限公司 | Fluoride reation kettle temperature control system and temperature control device |
| CN117427527A (en) * | 2023-12-20 | 2024-01-23 | 宿迁鑫凯隆新材料科技有限公司 | Mixing equipment is used in production of environmental protection type surface treatment agent |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1843612A (en) * | 2006-03-13 | 2006-10-11 | 江南大学 | Multifunctional post-extraction tank for extracting biological reaction product |
| US8721982B2 (en) * | 2009-08-04 | 2014-05-13 | Taiyo Nippon Sanso Corporation | Reaction device |
| CN103933919A (en) * | 2014-04-08 | 2014-07-23 | 中国华能集团清洁能源技术研究院有限公司 | Reaction kettle type heating system for heat transfer reaction of material in chemical industry |
| CN204247206U (en) * | 2014-11-19 | 2015-04-08 | 铁岭德士捷化工有限公司 | A kind of crystallizing kettle producing molecular sieve |
-
2017
- 2017-01-20 CN CN201710040111.9A patent/CN106732289A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1843612A (en) * | 2006-03-13 | 2006-10-11 | 江南大学 | Multifunctional post-extraction tank for extracting biological reaction product |
| US8721982B2 (en) * | 2009-08-04 | 2014-05-13 | Taiyo Nippon Sanso Corporation | Reaction device |
| CN103933919A (en) * | 2014-04-08 | 2014-07-23 | 中国华能集团清洁能源技术研究院有限公司 | Reaction kettle type heating system for heat transfer reaction of material in chemical industry |
| CN204247206U (en) * | 2014-11-19 | 2015-04-08 | 铁岭德士捷化工有限公司 | A kind of crystallizing kettle producing molecular sieve |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107261887A (en) * | 2017-07-28 | 2017-10-20 | 朱明� | A kind of lubricating oil blending tank |
| CN113840650A (en) * | 2019-09-26 | 2021-12-24 | 株式会社Lg化学 | Esterification reaction apparatus and esterification reaction method |
| CN111389330A (en) * | 2020-03-25 | 2020-07-10 | 河南神马尼龙化工有限责任公司 | Reaction temperature stability maintaining system of adipic acid production system by nitric acid oxidation method |
| CN114904470A (en) * | 2022-04-18 | 2022-08-16 | 安徽省谱诺药化设备有限公司 | Inner cavity uniform heating type stainless steel reaction kettle |
| CN116212770A (en) * | 2023-03-13 | 2023-06-06 | 南通太洋高新材料科技有限公司 | Fluoride reation kettle temperature control system and temperature control device |
| CN116212770B (en) * | 2023-03-13 | 2023-10-27 | 南通太洋高新材料科技有限公司 | Fluoride reation kettle temperature control system and temperature control device |
| CN117427527A (en) * | 2023-12-20 | 2024-01-23 | 宿迁鑫凯隆新材料科技有限公司 | Mixing equipment is used in production of environmental protection type surface treatment agent |
| CN117427527B (en) * | 2023-12-20 | 2024-03-05 | 宿迁鑫凯隆新材料科技有限公司 | Mixing equipment is used in production of environmental protection type surface treatment agent |
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Application publication date: 20170531 |