CN208990283U - It is a kind of for extracting the reaction kettle of high-purity oleic acid - Google Patents
It is a kind of for extracting the reaction kettle of high-purity oleic acid Download PDFInfo
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- CN208990283U CN208990283U CN201821613002.8U CN201821613002U CN208990283U CN 208990283 U CN208990283 U CN 208990283U CN 201821613002 U CN201821613002 U CN 201821613002U CN 208990283 U CN208990283 U CN 208990283U
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- main body
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- reaction kettle
- oleic acid
- scraping
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Abstract
The utility model discloses a kind of for extracting the reaction kettle of high-purity oleic acid, including reactor main body, the side of the reactor main body is equipped with control panel, and the other side of reactor main body is provided with refrigeration compressor, the bottom end of the reactor main body is connected with discharge port, and the front surface of reactor main body is embedded with observation window, the top of the reactor main body is connected with feed inlet, and servo motor is provided with above reactor main body, the inside of the reactor main body is equipped with cooling tube, and the front surface of the control panel is embedded with temperature indicator.The utility model is managed and scraping blender by setting cold-zone, in the inside of reactor main body, helically rotation structure arranges cooling tube, increase the contact area of cooling tube and reactor main body, scraping blender is stirred the crude oil acid solution of reactor main body simultaneously, it cools down crude oil acid oil liquid uniformly, effectively increases the cooling velocity of crude oil acid solution.
Description
Technical field
It is specially a kind of for extracting the reaction kettle of high-purity oleic acid the utility model relates to field.
Background technique
The broad understanding of reaction kettle has the container physically or chemically reacted, is designed by the structure to container and is matched with parameter
It sets, realizes the mixed function for heating, evaporation, cooling and the low high speed that technique requires.
But the crystallization process of oleic acid can not be observed, is caused for extracting the reaction kettle of high-purity oleic acid currently on the market
It can not quickly determine whether crystallization is completed, can not effectively solve the problems, such as that crude oil acid solution is attached to reactor main body inner wall, leads
The waste of crude oil acid solution is caused, the cooling velocity of crude oil acid can not be further increased, cause working efficiency that can not improve.
Utility model content
The purpose of this utility model is to provide a kind of for extracting the reaction kettle of high-purity oleic acid, to solve above-mentioned background
The problem of being proposed in technology.
To achieve the above object, the utility model provides the following technical solutions: a kind of for extracting the anti-of high-purity oleic acid
Kettle, including reactor main body are answered, the side of the reactor main body is equipped with control panel, and the other side of reactor main body is set
It is equipped with refrigeration compressor, the bottom end of the reactor main body is connected with discharge port, and the front surface of reactor main body is embedded with sight
Window is examined, the top of the reactor main body is connected with feed inlet, and servo motor is provided with above reactor main body, described anti-
Answer the inside of kettle main body that cooling tube is installed, the front surface of the control panel is embedded with temperature indicator, and control panel
Front surface is provided with control button below temperature indicator, and the top of the refrigeration compressor is fixed with connecting tube, and
Refrigeration compressor is connected with cold air efferent duct close to the side of reactor main body, and the side of the connecting tube is connected with cold air entrance
Pipe, the outer surface of the discharge port are equipped with solenoid valve, and the bottom end of the servo motor is connected close to the inside of reactor main body
There is rotation axis, the bottom end of the rotation axis is connected with scraping blender, and the two sides of rotation axis are close to the inside of scraping blender
It is provided with connecting rod, and the side of rotation axis is equipped with PT-100 temperature sensor below connecting rod.
Preferably, the outer wall of the scraping blender and the inner wall of reactor main body fit, the servo motor with scrape
Side blender is rotatablely connected by rotation axis.
Preferably, the cold air enter pipe output end and cooling tube input terminal connect, the cold air efferent duct it is defeated
The output end for entering end and cooling tube connects.The cooling tube is in the inside of reactor main body helically structural arrangement.
Preferably, the PT-100 temperature sensor and temperature indicator are electrically connected by PLC controller, and PT-100
Temperature sensor and servo motor are electrically connected by PLC controller.
Preferably, the control button and solenoid valve are electrically connected, and the servo motor and reactor main body pass through fixation
Bar connection.
Preferably, it is connected on the inside of the outside of the connecting rod and scraping blender, and the quantity of connecting rod is two.
Compared with prior art, the utility model has the beneficial effects that the utility model improves setting visual window, work people
The permeable visual window of member, observes the crystallization process of oleic acid, solves the problems, such as not determining whether crystallization is completed, raising is set
Set scraping blender, just the outside of blender fits closely official with reactor main body inner wall, scraping blender while rotating,
The crude oil acid solution for being attached to reaction kettle inner wall can be scraped, solve the problems, such as wastage of material, managed by setting cold-zone
With scraping blender, in the inside of reactor main body, helically rotation structure arranges cooling tube, increases cooling tube and reaction kettle master
The contact area of body, while scraping blender is stirred the crude oil acid solution of reactor main body, keeps crude oil acid oil liquid equal
Even cooling effectively increases the cooling velocity of crude oil acid solution.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is the schematic diagram of internal structure of the utility model reactor main body.
In figure: 1, reactor main body；2, control button；3, temperature indicator；4, control panel；5, cold air enters pipe；6,
Servo motor；7, feed inlet；8, connecting tube；9, refrigeration compressor；10, cold air efferent duct；11, observation window；12, solenoid valve；13,
Discharge port；14, rotation axis；15, cooling tube；16, scraping blender；17, PT-100 temperature sensor；18, connecting rod.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
It is provided by the utility model a kind of for extracting the reaction kettle embodiment of high-purity oleic acid referring to FIG. 1-2: a kind of
For extracting the reaction kettle of high-purity oleic acid, including reactor main body 1, the side of reactor main body 1 is equipped with control panel 4,
And the other side of reactor main body 1 is provided with refrigeration compressor 9, the bottom end of reactor main body 1 is connected with discharge port 13, and reacts
The front surface of kettle main body 1 is embedded with observation window 11, and the top of reactor main body 1 is connected with feed inlet 7, and reactor main body 1
Top is provided with servo motor 6, and the inside of reactor main body 1 is equipped with cooling tube 15, and the front surface of control panel 4 is embedded with temperature
Display 3 is spent, and the front surface of control panel 4 is provided with control button 2, refrigeration compressor 9 close to the lower section of temperature indicator 3
Top be fixed with connecting tube 8, and refrigeration compressor 9 is connected with cold air efferent duct 10 close to the side of reactor main body 1, connection
The side of pipe 8 is connected with cold air and enters pipe 5, and the outer surface of discharge port 13 is equipped with solenoid valve 12, and the bottom end of servo motor 6 is close
Reactor main body 1 is internally connected with rotation axis 14, and the bottom end of rotation axis 14 is connected with scraping blender 16, and rotation axis 14
Two sides are provided with connecting rod 18 close to the inside of scraping blender 16, and the side of rotation axis 14 is pacified close to the lower section of connecting rod 18
Equipped with PT-100 temperature sensor 17.
This is used to extract the reaction kettle of high-purity oleic acid: when using device purification oleic acid, first leading to crude oil acid solution
It crosses feed inlet 7 to pour into device, then feed inlet 7 is sealed, control refrigeration compressor 9 is run, and refrigeration compressor 9 compresses air
And cold air is inputted by connecting tube 8 after cooling down and is entered in pipe 5, cold air enters pipe 5 and cooling compressed air is inputted cooling tube again
In 15, cooling air takes away the temperature of the crude oil acid solution inside reactor main body 1 after cooling tube 15, then defeated by cold air
Outlet pipe 10 returns in refrigeration compressor 9, and cold compression air enters cooling tube 15 with this repeatedly, makes the temperature inside reactor main body 1
Degree quickly reduces, and while temperature reduces in reactor main body 1, control servo motor 6 is run, and servo motor 6 passes through rotation
Axis 14 drives scraping blender 16 and connecting rod 18 to rotate, and makes the crude oil acid solution uniform decrease in temperature in reactor main body 1, at this time
The temperature signal of crude oil acid solution is switched to electric signal and is delivered in PLC controller by PT-100 temperature sensor 17, PLC controller
After receiving electric signal, switched to digital signal, and is delivered on temperature indicator 3, it can intuitive observing response kettle master
Temperature inside body 1, after the temperature in reactor main body 1 reaches the fusing point of oleic acid, PT-100 temperature sensor 17 passes through PLC
Controller control servo motor 6 is out of service, and the oleic acid in crude oil acid solution starts to crystallize at this time, and control refrigeration compressor 9 is protected
Hold the temperature inside reactor main body 1.
Please emphatically refering to fig. 1, control button 2 and solenoid valve 12 are electrically connected, convenient for controlling solenoid valve by control button 2
12 open or close, and servo motor 6 is connect with reactor main body 1 by fixed link, are fixed on reaction kettle master convenient for servo motor 6
The top of body 1.
It please be stirred emphatically referring to Fig.2, the outer wall of scraping blender 16 and the inner wall of reactor main body 1 fit convenient for scraping
It mixes device 16 to scrape the grease being attached in reactor main body 1, servo motor 6 is rotated with scraping blender 16 by rotation axis 14
Connection leads to rotation axis 14 convenient for servo motor 6 and scraping blender 16 is driven to rotate；The outside of connecting rod 18 and scraping blender 16
Inside be connected, and the quantity of connecting rod 18 is two, convenient for connecting rod 18 increase scraping blender 16 and rotation axis 14 it
Between attachment force.
Please be emphatically refering to fig. 1 with Fig. 2, the output end that cold air enters pipe 5 is connect with the input terminal of cooling tube 15, is convenient for cold air
It will utter a sound and be inputted in cooling tube 15 into pipe 5, the input terminal of cold air efferent duct 10 is connect with the output end of cooling tube 15, convenient for cold
Gas efferent duct 10 exports the cold air in cooling tube 15.Cooling tube 15 is in the inside of reactor main body 1 helically structural arrangement, just
Contact area between honest cooling tube 15 and reactor main body 1, accelerates the cooling velocity of device；PT-100 temperature sensor
17 are electrically connected with temperature indicator 3 by PLC controller, will be warm convenient for PT-100 temperature sensor 17 by PLC controller
Degree is presented in digital form on temperature indicator 3, and PT-100 temperature sensor 17 and servo motor 6 are controlled by PLC
Device is electrically connected, and it is out of service to control servo motor 6 convenient for PT-100 temperature sensor 17.
Working principle: firstly, when using device purification oleic acid, crude oil acid solution is first poured into dress by feed inlet 7
In setting, then feed inlet 7 is sealed, control refrigeration compressor 9 is run, and refrigeration compressor 9 passes through company after air is compressed and cooled down
Adapter tube 8 inputs cold air and enters in pipe 5, and cold air enters pipe 5 again in cooling compressed air input cooling tube 15, and cooling air passes through
The temperature of the crude oil acid solution inside reactor main body 1 is taken away after supercooling pipe 15, then refrigeration is returned to by cold air efferent duct 10
In compressor 9, cold compression air enters cooling tube 15 with this repeatedly, reduces the temperature inside reactor main body 1 quickly；So
Afterwards, while temperature reduces in reactor main body 1, control servo motor 6 is run, and servo motor 6 is driven by rotation axis 14
Scraping blender 16 and connecting rod 18 rotate, and make the crude oil acid solution uniform decrease in temperature in reactor main body 1, at this time PT-100 temperature
The temperature signal of crude oil acid solution is switched to electric signal and is delivered in PLC controller by sensor 17, and PLC controller receives telecommunications
After number, switched to digital signal, and is delivered on temperature indicator 3, it can temperature inside intuitive observing response kettle main body 1
Degree, after the temperature in reactor main body 1 reaches the fusing point of oleic acid, PT-100 temperature sensor 17 is controlled by PLC controller
Servo motor 6 is out of service, and the oleic acid in crude oil acid solution starts to crystallize at this time, and control refrigeration compressor 9 keeps reaction kettle master
Temperature inside body 1；Finally, observing the crystallization process in oleic acid by observation window 11, until oleic acid crystallization finishes, pass through control
Button 2 opens solenoid valve 12, and the other impurities solution in reactor main body 1 is flowed out by discharge port 13, later, that is, can be taken off height
The oleic acid of purity crystallizes.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and
And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms
Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new
The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in
All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting
Related claim.
Claims (6)
1. a kind of for extracting the reaction kettle of high-purity oleic acid, including reactor main body (1), it is characterised in that: the reaction kettle
The side of main body (1) is equipped with control panel (4), and the other side of reactor main body (1) is provided with refrigeration compressor (9), institute
The bottom end for stating reactor main body (1) is connected with discharge port (13), and the front surface of reactor main body (1) is embedded with observation window
(11), the top of the reactor main body (1) is connected with feed inlet (7), and servo electricity is provided with above reactor main body (1)
The inside of machine (6), the reactor main body (1) is equipped with cooling tube (15), and the front surface of the control panel (4) is embedded with temperature
It spends display (3), and the front surface of control panel (4) is provided with control button (2), institute below temperature indicator (3)
The top for stating refrigeration compressor (9) is fixed with connecting tube (8), and refrigeration compressor (9) connects close to the side of reactor main body (1)
It is connected to cold air efferent duct (10), the side of the connecting tube (8) is connected with cold air and enters pipe (5), outside the discharge port (13)
Surface is equipped with solenoid valve (12), and the bottom end of the servo motor (6) is internally connected with rotation axis close to reactor main body (1)
(14), the bottom end of the rotation axis (14) is connected with scraping blender (16), and the two sides of rotation axis (14) are stirred close to scraping
It is provided on the inside of device (16) connecting rod (18), and the side of rotation axis (14) is equipped with PT- below connecting rod (18)
100 temperature sensors (17).
2. according to claim 1 a kind of for extracting the reaction kettle of high-purity oleic acid, it is characterised in that: the scraping is stirred
The inner wall of the outer wall and reactor main body (1) of mixing device (16) fits, and the servo motor (6) passes through with scraping blender (16)
Rotation axis (14) rotation connection.
3. according to claim 1 a kind of for extracting the reaction kettle of high-purity oleic acid, it is characterised in that: the cold air into
The output end for entering pipe (5) is connect with the input terminal of cooling tube (15), the input terminal and cooling tube of the cold air efferent duct (10)
(15) output end connection, the cooling tube (15) is in the inside of reactor main body (1) helically structural arrangement.
4. according to claim 1 a kind of for extracting the reaction kettle of high-purity oleic acid, it is characterised in that: the PT-100
Temperature sensor (17) and temperature indicator (3) by PLC controller electric connection, and PT-100 temperature sensor (17) with watch
Motor (6) is taken to be electrically connected by PLC controller.
5. according to claim 1 a kind of for extracting the reaction kettle of high-purity oleic acid, it is characterised in that: the control is pressed
Button (2) and solenoid valve (12) are electrically connected, and the servo motor (6) is connect with reactor main body (1) by fixed link.
6. according to claim 1 a kind of for extracting the reaction kettle of high-purity oleic acid, it is characterised in that: the connecting rod
(18) it is connected on the inside of outside and scraping blender (16), and the quantity of connecting rod (18) is two.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821613002.8U CN208990283U (en) | 2018-09-30 | 2018-09-30 | It is a kind of for extracting the reaction kettle of high-purity oleic acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821613002.8U CN208990283U (en) | 2018-09-30 | 2018-09-30 | It is a kind of for extracting the reaction kettle of high-purity oleic acid |
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| Publication Number | Publication Date |
|---|---|
| CN208990283U true CN208990283U (en) | 2019-06-18 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821613002.8U Active CN208990283U (en) | 2018-09-30 | 2018-09-30 | It is a kind of for extracting the reaction kettle of high-purity oleic acid |
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| CN (1) | CN208990283U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114146443A (en) * | 2021-12-01 | 2022-03-08 | 美亚药业海安有限公司 | Crystallization kettle for cytidine acid preparation and preparation method thereof |
| CN116020389A (en) * | 2022-12-30 | 2023-04-28 | 湖南辰耀新型建材有限公司 | Enhanced expansion anti-cracking agent stirring reaction kettle |
-
2018
- 2018-09-30 CN CN201821613002.8U patent/CN208990283U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114146443A (en) * | 2021-12-01 | 2022-03-08 | 美亚药业海安有限公司 | Crystallization kettle for cytidine acid preparation and preparation method thereof |
| CN116020389A (en) * | 2022-12-30 | 2023-04-28 | 湖南辰耀新型建材有限公司 | Enhanced expansion anti-cracking agent stirring reaction kettle |
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