CN209302227U - A kind of crystallization filter device for chemical reagent preparation - Google Patents
A kind of crystallization filter device for chemical reagent preparation Download PDFInfo
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- CN209302227U CN209302227U CN201821967513.XU CN201821967513U CN209302227U CN 209302227 U CN209302227 U CN 209302227U CN 201821967513 U CN201821967513 U CN 201821967513U CN 209302227 U CN209302227 U CN 209302227U
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- rose box
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- chemical reagent
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- support base
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Abstract
The utility model discloses a kind of crystallization filter devices for chemical reagent preparation, including Rose Box, support base, motor, shaft coupling, the support base is provided with above the Rose Box, the motor is provided between the support base, the shaft coupling is provided with below the motor, the support base side is provided with feed pipe, sealing cover is provided with above the feed pipe, the Rose Box side is provided with electric cylinder, the Rose Box other side is provided with discharge nozzle, is provided with piston rod on the electric cylinder.Beneficial effect is: the utility model passes through setting motor and agitating shaft, chemical reagent can be made enough uniformly to mix with water energy, it ensure that crystallization effect, pass through setting electric cylinder and push plate, Rose Box can be discharged in crystallization automatically, improve the degree of automation of device, by the way that observation window is arranged, Rose Box inner case can be observed, convenient for grasping processing progress.
Description
Technical field
The utility model relates to filter plant fields, filter dress more particularly to a kind of crystallization for chemical reagent preparation
It sets.
Background technique
Inside chemistry, after hot saturated solution is cooling, solute is precipitated in the form of crystal, this process is crystallization.
The process that solute is precipitated from solution can be divided into nucleus and generate (nucleation) and two stages of crystal growth, two ranks
The motive force of section is all the degree of supersaturation (value of the concentration of solute more than its saturation solubility in crystallization solution) of solution.Nucleus
Form there are three types of generating: i.e. primary homogeneous nucleation, primary nonhomogen-ous nucleation and secondary nucleation.Under high degree of supersaturation, solution is certainly
Hair ground generates the process of nucleus, referred to as primary homogeneous nucleation；Solution generates under the induction of exotic (micronic dust in such as atmosphere)
The process of nucleus, referred to as primary nonhomogen-ous nucleation；And the nucleation process in the solution containing solute crystals, it is referred to as secondary at
Core.Secondary nucleation also belongs to nonhomogen-ous nucleation process, it is between crystal or crystal and other solids (wall, blender etc.)
Occur under the induction of generated tiny crystal grains when collision.
But the crystal block that the crystal block that has of the crystallization filter device of present chemical reagent preparation has greatly is small, crystallization effect compared with
Difference, and need that cabinet manually is discharged in crystallization, increase the labor intensity of worker, it is therefore desirable to do on this basis further
Improvement.
Utility model content
The purpose of this utility model is that solve the above-mentioned problems and provides a kind of knot for chemical reagent preparation
Brilliant filter device, the utility model can be such that chemical reagent enough uniformly mixes with water energy, be guaranteed by setting motor and agitating shaft
Crystallization effect, by setting electric cylinder and push plate, can automatically will crystallization discharge Rose Box, improve the automation of device
Degree can observe Rose Box inner case, by the way that observation window is arranged convenient for grasping processing progress.
The utility model achieves the above object through the following technical schemes:
A kind of crystallization filter device for chemical reagent preparation, including Rose Box, support base, motor, shaft coupling, it is described
It is provided with the support base above Rose Box, the motor is provided between the support base, is arranged below the motor
Shaft coupling is stated, the support base side is provided with feed pipe, is provided with sealing cover, the Rose Box side above the feed pipe
It is provided with electric cylinder, the Rose Box other side is provided with discharge nozzle, and piston rod, the work are provided on the electric cylinder
Stopper rod is provided with push plate far from one end of the electric cylinder, and second solenoid valve, the discharge nozzle are provided on the discharge nozzle
Lower section is provided with drainpipe, and the Rose Box is internally provided with shaft, and the shaft two sides are provided with agitating shaft, the agitating shaft
Side is provided with heater box, and the agitating shaft other side is provided with temperature sensor, the temperature sensor model PT-100,
The heater box is internally provided with heating plate, and baffle is provided with below the heater box, is provided with water-supply-pipe below the baffle,
The first solenoid valve is provided on the water-supply-pipe, first solenoid valve is connected through a screw thread with the water-supply-pipe, the water delivery
Filter screen is provided with below pipe, the Rose Box front is provided with observation window, is provided with control cabinet below the observation window, described
Control cabinet is internally provided with controller, the controller model MAM-200, and the control cabinet front is provided with display screen, institute
It states and is provided with control button below display screen, the control button, the temperature sensor, first solenoid valve, described the
Two solenoid valves, the heating plate, the electric cylinder, the motor and the display screen are electrically connected with the controller.
So set, chemical reagent can be made enough uniformly to mix with water energy by the way that the motor and the agitating shaft is arranged,
It ensure that crystallization effect, by the way that the electric cylinder and the push plate is arranged, the Rose Box can be discharged in crystallization automatically, mentioned
High the degree of automation of device can observe the Rose Box inner case by the way that the observation window is arranged, be convenient for
Grasp processing progress.
In above structure, chemical reagent is mixed according to a certain percentage with water, device is then connected into external power supply, up time
Needle rotates the sealing cover, mixed solution is transported to the Rose Box by the feed pipe, then rotate counterclockwise described close
Capping, by the control button setup parameter, the controller brings into operation, the motor, the heating plate and the temperature
It spends sensor to start to work, the motor drives the shaft to rotate by the shaft coupling, and the shaft drives the stirring
Axis rotation, the agitating shaft are stirred mixed solution, and the heating plate heats mixed solution, the temperature sensing
Device detects the temperature of mixed solution, when the temperature of mixed solution reaches setting value, the motor and the heating plate
Out of service, mixed solution is begun to cool, and after observing mixed solution crystallization by the observation window, opens described first
Solenoid valve, crystallization and liquid are discharged by the water-supply-pipe, and the filter screen is filtered crystallization, and liquid is from the drainpipe
The Rose Box is discharged, after liquid all filters, the electric cylinder and the second solenoid valve are opened, the electronic gas
Cylinder drives the piston rod flexible, and the piston rod drives the push plate to do iterative motion, and crystallization is pushed by the push plate
Into the discharge nozzle, the Rose Box is discharged from the discharge nozzle in crystallization.
Further, the support base and the Rose Box weld, and the motor is bolted with the support base,
The motor is connect with the shaft by the shaft coupling, and the agitating shaft and the shaft are welded.
So set, welding is bolted and improves institute so that the support base and the Rose Box stable connection are reliable
The stability for stating motor, ensure that the safety of the motor, and the shaft coupling allows the motor that the shaft is driven to turn
It is dynamic, it ensure that the smooth transmitting of kinetic energy, welding is not easily to fall off so that the agitating shaft is fixed in the shaft.
Further, the feed pipe and the Rose Box weld, and the sealing cover and the feed pipe are connected by screw thread
It connects.
So set, welding is so that the feed pipe and the Rose Box stable connection are reliable, threaded connection is so that described
Sealing cover and the feed pipe are completely embedded reliably.
Further, the heating plate is connected by screw to the heater box, the temperature sensor and the filtering
Case is connected by screw to, and the baffle and the Rose Box weld, and the water-supply-pipe and the baffle weld.
So set, screw connection improves the stability of the heating plate, being normally carried out for heating work, spiral shell ensure that
Nail connection is so that the temperature sensor is fixed on the Rose Box, and not easily to fall off, welding is so that the baffle and the mistake
Filter box stable connection is reliable, and welding improves the leakproofness of device, avoids the leakage of liquid.
Further, the discharge nozzle and the Rose Box weld, and the second solenoid valve and the discharge nozzle pass through spiral shell
Line connection.
So set, welding is so that the discharge nozzle and the Rose Box stable connection are reliable, threaded connection is so that described
Second solenoid valve can preferably control the on-off of the discharge nozzle.
Further, the filter screen is connected by screw to the Rose Box, the electric cylinder and the Rose Box
It is bolted.
So set, screw connects so that the installation and replacement of the filter screen are all very convenient, it is bolted so that institute
It states electric cylinder to be fixed on the Rose Box, ensure that the safety of the electric cylinder.
Further, the control cabinet is connected by screw to the Rose Box, and the controller and the control cabinet are logical
Cross screw connection.
So set, screw connection is so that the control cabinet and the Rose Box stable connection are reliable, screw connection is improved
The stability of the controller, ensure that the normal operation of device.
Compared with prior art, the beneficial effects of the utility model are as follows:
1, by setting motor and agitating shaft, chemical reagent can be made enough uniformly to mix with water energy, ensure that crystallization effect；
2, by setting electric cylinder and push plate, Rose Box can be discharged in crystallization automatically, improves the automation of device
Degree；
3, by setting observation window, Rose Box inner case can be observed, convenient for grasping processing progress.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment
Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only
Some embodiments of the utility model, for those of ordinary skill in the art, in the premise of not making the creative labor property
Under, it is also possible to obtain other drawings based on these drawings.
Fig. 1 is a kind of internal structure signal of crystallization filter device for chemical reagent preparation described in the utility model
Figure；
Fig. 2 is a kind of main view of crystallization filter device for chemical reagent preparation described in the utility model；
Fig. 3 is that the amplification of control cabinet in a kind of crystallization filter device for chemical reagent preparation described in the utility model is left
Depending on schematic diagram of internal structure；
Fig. 4 is a kind of circuit structure flow chart element of crystallization filter device for chemical reagent preparation described in the utility model
Figure.
The reference numerals are as follows:
1, Rose Box；2, support base；3, motor；4, shaft coupling；5, feed pipe；6, sealing cover；7, shaft；8, agitating shaft；
9, heater box；10, heating plate；11, temperature sensor；12, baffle；13, water-supply-pipe；14, the first solenoid valve；15, electric cylinder；
16, piston rod；17, push plate；18, filter screen；19, discharge nozzle；20, second solenoid valve；21, drainpipe；22, observation window；23, it controls
Case processed；24, controller；25, display screen；26, control button.
Specific embodiment
In the description of the present invention, it should be understood that term " center ", " longitudinal direction ", " transverse direction ", "upper", "lower",
The orientation or positional relationship of the instructions such as "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outside" is
It is based on the orientation or positional relationship shown in the drawings, is merely for convenience of describing the present invention and simplifying the description, rather than indicate
Or imply that signified device or element must have a particular orientation, be constructed and operated in a specific orientation, therefore cannot understand
For limitations of the present invention.In addition, term " first ", " second " etc. are used for description purposes only, and should not be understood as indicating
Or it implies relative importance or implicitly indicates the quantity of indicated technical characteristic." first ", " second " etc. are defined as a result,
Feature can explicitly or implicitly include one or more of the features.It is in the description of the present invention, unless another
It is described, the meaning of " plurality " is two or more.
In the description of the present invention, it should be noted that unless otherwise clearly defined and limited, term " is pacified
Dress ", " connected ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or integrally
Connection；It can be mechanical connection, be also possible to be electrically connected；Can be directly connected, can also indirectly connected through an intermediary,
It can be the connection inside two elements.For the ordinary skill in the art, on being understood by concrete condition
State the concrete meaning of term in the present invention.
The utility model is described in further detail with reference to the accompanying drawing:
First embodiment:
As Figure 1-Figure 4, it is a kind of for chemical reagent preparation crystallization filter device, including Rose Box 1, support base 2,
Motor 3, shaft coupling 4, are provided with support base 2 above Rose Box 1, and support base 2 is provided with to fixed motor 3 between support base 2
Motor 3, motor 3 are provided with shaft coupling 4, shaft coupling 4 is to connect 3 He of motor to convert electrical energy into kinetic energy below motor 3
Shaft 7,2 side of support base are provided with feed pipe 5, and feed pipe 5 is provided with sealing cover 6 to feed above feed pipe 5, sealing
Lid 6 is provided with electric cylinder 15 to close feed pipe 5,1 side of Rose Box, and electric cylinder 15 is to control stretching for piston rod 16
Contracting, 1 other side of Rose Box are provided with discharge nozzle 19, and discharge nozzle 19 is provided with piston rod on electric cylinder 15 crystallization is discharged
16, for piston rod 16 to fixed push plate 17, piston rod 16 is provided with push plate 17 far from one end of electric cylinder 15, push plate 17 to
Crystallization is pushed, second solenoid valve 20, on-off of the second solenoid valve 20 to control discharge nozzle 19, discharging are provided on discharge nozzle 19
Drainpipe 21 is provided with below pipe 19, drainpipe 21 is internally provided with shaft 7 filtered liquid, Rose Box 1 is discharged, and turns
Axis 7 is provided with agitating shaft 8 to fixed agitating shaft 8,7 two sides of shaft, and agitating shaft 8 is to be stirred work, 8 side of agitating shaft
It is provided with heater box 9, for heater box 9 to fixed heating plate 10,8 other side of agitating shaft is provided with temperature sensor 11, and temperature passes
11 model PT-100 of sensor, to detect the temperature of mixed solution, heater box 9 is internally provided with heating plate 10, heating plate 10
To heat mixed solution, it is provided with baffle 12 below heater box 9, water-supply-pipe 13 is provided with below baffle 12, water-supply-pipe 13 is used
To convey liquid and crystallization, the first solenoid valve 14 is provided on water-supply-pipe 13, the first solenoid valve 14 is to control water-supply-pipe 13
On-off, the first solenoid valve 14 are connected through a screw thread with water-supply-pipe 13, and filter screen 18 is provided with below water-supply-pipe 13, and filter screen 18 is used
With filtering for crystallizing, 1 front of Rose Box is provided with observation window 22, and observation window 22 is to observe 1 internal state of Rose Box, observation window 22
Lower section is provided with control cabinet 23, and for control cabinet 23 to protect controller 24, control cabinet 23 is internally provided with controller 24, controller
24 model MAM-200 are run to control device, and 23 front of control cabinet is provided with display screen 25, and display screen 25 is to show
Parameter is provided with control button 26 below display screen 25, and control button 26 is to setup parameter, control button 26, temperature sensing
Device 11, the first solenoid valve 14, second solenoid valve 20, heating plate 10, electric cylinder 15, motor 3 and display screen 25 and controller 24
Electrical connection.
Second embodiment:
The difference of second embodiment and first embodiment is: support base 2 and Rose Box 1 weld, motor 3 and support base 2
It is bolted, motor 3 is connect with shaft 7 by shaft coupling 4, and agitating shaft 8 and shaft 7 are welded.
Specifically, support base 2 and Rose Box 1 weld, and weld so that support base 2 and 1 stable connection of Rose Box are reliable；Motor
3 are bolted with support base 2, are bolted the stability for improving motor 3, ensure that the safety of motor 3；Motor 3 with
Shaft 7 is connected by shaft coupling 4, and shaft coupling 4 allows motor 3 that shaft 7 is driven to rotate, and ensure that the smooth transmitting of kinetic energy；
Agitating shaft 8 and shaft 7 are welded, and welding is not easily to fall off so that agitating shaft 8 is fixed in shaft 7.
3rd embodiment:
The difference of 3rd embodiment and first embodiment is: heating plate 10 is connected by screw to heater box 9, and temperature passes
Sensor 11 is connected by screw to Rose Box 1, and baffle 12 and Rose Box 1 weld, and water-supply-pipe 13 and baffle 12 weld.
Specifically, heating plate 10 is connected by screw to heater box 9, and screw connects the stability for improving heating plate 10,
It ensure that being normally carried out for heating work；Temperature sensor 11 is connected by screw to Rose Box 1, and screw connects so that temperature passes
Sensor 11 is not easily to fall off, ensure that being normally carried out for detection work；Baffle 12 and Rose Box 1 weld, welding so that baffle 12 with
1 stable connection of Rose Box is reliable；Water-supply-pipe 13 and baffle 12 weld, welding so that water-supply-pipe 13 and baffle 12 be completely embedded can
It leans on, avoids the leakage of liquid.
In above structure, chemical reagent is mixed according to a certain percentage with water, device is then connected into external power supply, up time
Mixed solution is transported to Rose Box 1 by feed pipe 5 by needle rotary seal lid 6, and another mistake hour hands rotary seal lid 6 passes through control
26 setup parameter of button, controller 24 bring into operation, and motor 3, heating plate 10 and temperature sensor 11 are started to work, and motor 3 is logical
Crossing shaft coupling 4 drives shaft 7 to rotate, and shaft 7 drives agitating shaft 8 to rotate, and agitating shaft 8 is stirred mixed solution, heating plate
10 pairs of mixed solutions heat, and temperature sensor 11 detects the temperature of mixed solution, when the temperature of mixed solution reaches
When to setting value, motor 3 and heating plate 10 are out of service, and mixed solution is begun to cool, and observe that mixing is molten by observation window 22
After liquid crystallizes, the first solenoid valve 14 is opened, crystallization and liquid are discharged by water-supply-pipe 13, and 18 pairs of filter screen crystallizations carried out
Filter, Rose Box 1 is discharged from drainpipe 21 in liquid, and after liquid all filters, electric cylinder 15 and second solenoid valve 20 are opened,
Electric cylinder 15 drives piston rod 16 flexible, and piston rod 16 drives push plate 17 to do iterative motion, and crystallization is pushed by push plate 17
Into discharge nozzle 19, Rose Box 1 is discharged from discharge nozzle 19 in crystallization.
The basic principles and main features and advantage of the utility model have been shown and described above.The technical staff of the industry
It should be appreciated that the present utility model is not limited to the above embodiments, the above embodiments and description only describe this
The principle of utility model, on the premise of not departing from the spirit and scope of the utility model, the utility model also has various change
And improvement, these various changes and improvements fall within the scope of the claimed invention.
Claims (7)
1. it is a kind of for chemical reagent preparation crystallization filter device, it is characterised in that: including Rose Box (1), support base (2),
Motor (3), shaft coupling (4), Rose Box (1) top are provided with the support base (2), are arranged between the support base (2)
Have the motor (3), is provided with the shaft coupling (4) below the motor (3), support base (2) side is provided with charging
It manages (5), is provided with sealing cover (6) above the feed pipe (5), Rose Box (1) side is provided with electric cylinder (15), institute
It states Rose Box (1) other side to be provided with discharge nozzle (19), is provided with piston rod (16), the piston on the electric cylinder (15)
Bar (16) is provided with push plate (17) far from the one end of the electric cylinder (15), is provided with the second electromagnetism on the discharge nozzle (19)
Valve (20), discharge nozzle (19) lower section are provided with drainpipe (21), and the Rose Box (1) is internally provided with shaft (7), described
Shaft (7) two sides are provided with agitating shaft (8), and agitating shaft (8) side is provided with heater box (9), and the agitating shaft (8) is another
Side is provided with temperature sensor (11), and the heater box (9) is internally provided with heating plate (10), is set below the heater box (9)
It is equipped with baffle (12), is provided with water-supply-pipe (13) below the baffle (12), is provided with the first electromagnetism on the water-supply-pipe (13)
Valve (14), first solenoid valve (14) are connected through a screw thread with the water-supply-pipe (13), setting below the water-supply-pipe (13)
Have filter screen (18), Rose Box (1) front is provided with observation window (22), is provided with control cabinet below the observation window (22)
(23), the control cabinet (23) is internally provided with controller (24), and control cabinet (23) front is provided with display screen (25), institute
It states and is provided with control button (26) below display screen (25), the control button (26), the temperature sensor (11), described the
One solenoid valve (14), the second solenoid valve (20), the heating plate (10), the electric cylinder (15), the motor (3) and
The display screen (25) is electrically connected with the controller (24).
2. a kind of crystallization filter device for chemical reagent preparation according to claim 1, it is characterised in that: the branch
It supports seat (2) and the Rose Box (1) to weld, the motor (3) is bolted with the support base (2), the motor (3)
It is connect with the shaft (7) by the shaft coupling (4), the agitating shaft (8) and the shaft (7) are welded.
3. it is according to claim 1 it is a kind of for chemical reagent preparation crystallization filter device, it is characterised in that: it is described into
Expects pipe (5) and the Rose Box (1) are welded, and the sealing cover (6) is connected through a screw thread with the feed pipe (5).
4. a kind of crystallization filter device for chemical reagent preparation according to claim 1, it is characterised in that: described to add
Hot plate (10) is connected by screw to the heater box (9), and the temperature sensor (11) and the Rose Box (1) pass through screw
Connection, the baffle (12) and the Rose Box (1) are welded, and the water-supply-pipe (13) and the baffle (12) are welded.
5. it is according to claim 1 it is a kind of for chemical reagent preparation crystallization filter device, it is characterised in that: it is described go out
Expects pipe (19) and the Rose Box (1) are welded, and the second solenoid valve (20) is connected through a screw thread with the discharge nozzle (19).
6. a kind of crystallization filter device for chemical reagent preparation according to claim 1, it is characterised in that: the mistake
Strainer (18) is connected by screw to the Rose Box (1), and the electric cylinder (15) and the Rose Box (1) are connected by bolt
It connects.
7. a kind of crystallization filter device for chemical reagent preparation according to claim 1, it is characterised in that: the control
Case (23) processed is connected by screw to the Rose Box (1), and the controller (24) and the control cabinet (23) are connected by screw
It connects.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821967513.XU CN209302227U (en) | 2018-11-27 | 2018-11-27 | A kind of crystallization filter device for chemical reagent preparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821967513.XU CN209302227U (en) | 2018-11-27 | 2018-11-27 | A kind of crystallization filter device for chemical reagent preparation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209302227U true CN209302227U (en) | 2019-08-27 |
Family
ID=67674753
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| Application Number | Title | Priority Date | Filing Date |
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| CN201821967513.XU Active CN209302227U (en) | 2018-11-27 | 2018-11-27 | A kind of crystallization filter device for chemical reagent preparation |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111939590A (en) * | 2020-08-22 | 2020-11-17 | 江西永宁科技有限责任公司 | High-vacuum low-temperature crystallization equipment for producing potassium perchlorate and use method thereof |
| CN112717862A (en) * | 2020-11-17 | 2021-04-30 | 南通恒兴电子材料有限公司 | Production device and method of diammonium hydrogen phosphate |
| CN113813913A (en) * | 2021-10-20 | 2021-12-21 | 李世星 | Quinones natural product extraction equipment convenient to take out recrystallization product |
| CN116023983A (en) * | 2023-03-21 | 2023-04-28 | 黑龙江莱睿普思环境科技发展有限公司 | A cold low pressure knockout drum for refining dechlorination of waste mineral oil |
-
2018
- 2018-11-27 CN CN201821967513.XU patent/CN209302227U/en active Active
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111939590A (en) * | 2020-08-22 | 2020-11-17 | 江西永宁科技有限责任公司 | High-vacuum low-temperature crystallization equipment for producing potassium perchlorate and use method thereof |
| CN112717862A (en) * | 2020-11-17 | 2021-04-30 | 南通恒兴电子材料有限公司 | Production device and method of diammonium hydrogen phosphate |
| CN112717862B (en) * | 2020-11-17 | 2022-08-16 | 南通恒兴电子材料有限公司 | Production device and method of diammonium hydrogen phosphate |
| CN113813913A (en) * | 2021-10-20 | 2021-12-21 | 李世星 | Quinones natural product extraction equipment convenient to take out recrystallization product |
| CN116023983A (en) * | 2023-03-21 | 2023-04-28 | 黑龙江莱睿普思环境科技发展有限公司 | A cold low pressure knockout drum for refining dechlorination of waste mineral oil |
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