CN208959900U - A kind of use for laboratory self-loopa chemical synthesis instrument - Google Patents
A kind of use for laboratory self-loopa chemical synthesis instrument Download PDFInfo
- Publication number
- CN208959900U CN208959900U CN201821525056.9U CN201821525056U CN208959900U CN 208959900 U CN208959900 U CN 208959900U CN 201821525056 U CN201821525056 U CN 201821525056U CN 208959900 U CN208959900 U CN 208959900U
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- China
- Prior art keywords
- reactive tank
- control cabinet
- fixedly connected
- reaction flask
- shaft
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a kind of use for laboratory self-loopa chemical synthesis instrument, including control cabinet and reactive tank, reactive tank to be fixedly connected on the top of control cabinet；The surface of control cabinet is fixedly connected with PLC controller and power switch, and power switch is located at the right side of PLC controller, and the bottom of control cabinet is fixedly connected with supporting leg, and the middle part of control cabinet is equipped with discharge nozzle that is vertical and running through control cabinet；Reactive tank uses glass material blow molding, electric heating tube, reaction flask and temperature sensor are equipped in reactive tank, electric heating tube is evenly distributed on the inner wall of reactive tank, reaction flask is located at the middle part of reactive tank and is equipped with fixing seat between reactive tank, and the two sides of fixing seat are equipped with symmetrical temperature sensor.The utility model is observed the reaction of solution convenient for experimenter by using the reactive tank of glass material, improves the intuitive of experimentation, is designed by simple structure, reduces production cost and maintenance cost.
Description
Technical field
The utility model relates to chemosynthesis technical field, specially a kind of use for laboratory self-loopa chemical synthesis instrument.
Background technique
Chemical synthesis instrument, which can be catalyzed, completes addition, substitution, esterification, hydrolysis, alkane (acyl) base, polymerization, condensation, cyclization and oxygen
The physics mistakes such as the solvent extraction of the organic of many types, drug and the biochemical reactions such as change and food, natural products and mineral
Journey.Suitable for Synthetic Organic Chemistry, pharmaceutical chemistry, Food Science, quarantine epidemic prevention, military chemistry, molecular biology, analysisization
The related fieldss such as, inorganic chemistry, petrochemical industry, material science, biomedicine.
Currently, the chemical synthesis instrument in market is chiefly used in industrial production, product structure is complicated, and volume is big, is not suitable for experiment
The use of room brings inconvenience to the observation and regulation of experimenter, and production cost is higher, increases the cost and maintenance of experiment
Difficulty.It is solved for this reason, it may be necessary to design the new technical solution of one kind and give.
Utility model content
The purpose of this utility model is to provide a kind of use for laboratory self-loopa chemical synthesis instrument, by using glass material
Reactive tank, the reaction of solution is observed convenient for experimenter, improves the intuitive of experimentation, passes through simple structure
Design reduces production cost and maintenance cost.
To achieve the above object, the utility model provides the following technical solutions: a kind of use for laboratory self-loopa chemical synthesis
Instrument, including control cabinet and reactive tank, the reactive tank are fixedly connected on the top of control cabinet；The surface of the control cabinet is fixed to be connected
It is connected to PLC controller and power switch, the power switch is located at the right side of PLC controller, and the bottom of the control cabinet is fixed
It is connected with supporting leg, the middle part of the control cabinet is equipped with discharge nozzle that is vertical and running through control cabinet；The reactive tank uses glass
Material blow molding, the reactive tank is interior to be equipped with electric heating tube, reaction flask and temperature sensor, and the electric heating tube is uniformly distributed
In the inner wall of reactive tank, the reaction flask is located at the middle part of reactive tank and is equipped with fixing seat, the fixing seat between reactive tank
Two sides be equipped with symmetrical temperature sensor, the electric heating tube and temperature sensor be connected with PLC controller respectively,
The top of the reactive tank is equipped with fluid reservoir and motor, and the fluid reservoir is fixedly connected at least provided with two and with reactive tank,
Connecting tube is equipped between the fluid reservoir and reaction flask, the motor output end runs through the top of reactive tank and is fixedly connected with
Rotating disc.
As an improvement of the above technical solution, the shaft of rotation connection, the surface of the shaft are equipped in the reaction flask
It is fixedly connected with the first permanent magnet and paddle, first permanent magnet is located at the top of paddle.
As an improvement of the above technical solution, the upper and lower ends of the shaft are respectively equipped with rotation seat, the rotation seat with
Reaction flask is fixedly connected, and is respectively equipped with rotation seat by the both ends in shaft, convenient to shaft convenient for shaft is fixed
Position is fixed.
As an improvement of the above technical solution, the lower surface of the rotating disc is fixedly connected with the second permanent magnet, and described
Two permanent magnets are opposite with the first permanent magnet opposite face magnetic pole.
As an improvement of the above technical solution, the junction of the connecting tube and fluid reservoir is equipped with electromagnetic throttle valve, described
The junction of discharge nozzle and reaction flask is equipped with electromagnetic switch valve, and the electromagnetic throttle valve and electromagnetic switch valve are controlled with PLC respectively
Device is connected.
Compared with prior art, the beneficial effects of the utility model are as follows:
The utility model is observed the reaction of solution convenient for experimenter by using the reactive tank of glass material,
The intuitive for improving experimentation, is designed by simple structure, is reduced the volume of chemical synthesis instrument, is conveniently used for laboratory
It is interior, while production cost and maintenance cost are reduced, by being equipped with electromagnetic throttle valve, electromagnetic switch valve and PLC controller, it is convenient for
Chemical synthesis work is completed, stoste automatic cycle enters next synthesis link.
Detailed description of the invention
Fig. 1 is use for laboratory self-loopa chemical synthesis instrument surface structure schematic diagram described in the utility model；
Fig. 2 is use for laboratory self-loopa chemical synthesis instrument schematic cross-sectional view described in the utility model.
In figure: control cabinet -1, reactive tank -2, PLC controller -3, power switch -4, supporting leg -5, discharge nozzle -6, electricity add
Heat pipe -7, reaction flask -8, temperature sensor -9, fixing seat -10, fluid reservoir -11, motor -12, connecting tube -13, rotating disc -
14, shaft -15, the first permanent magnet -16, paddle -17, rotation seat -18, the second permanent magnet -19, electromagnetic throttle valve -20, electromagnetism
Switch valve -21.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe.
It please refers to Fig. 1-2 the utility model and a kind of technical solution is provided: a kind of use for laboratory self-loopa chemical synthesis instrument, packet
Control cabinet 1 and reactive tank 2 are included, the reactive tank 2 is fixedly connected on the top of control cabinet 1；The surface of the control cabinet 1 is fixed to be connected
It is connected to PLC controller 3 and power switch 4, the power switch 4 is located at the right side of PLC controller 3, the bottom of the control cabinet 1
It is fixedly connected with supporting leg 5, the middle part of the control cabinet 1 is equipped with discharge nozzle 6 that is vertical and running through control cabinet 1；The reactive tank 2
The reaction of solution is seen convenient for experimenter by using the reactive tank 2 of glass material using glass material blow molding
It surveys, improves the intuitive of experimentation, electric heating tube 7, reaction flask 8 and temperature sensor 9 are equipped in the reactive tank 2, it is described
Electric heating tube 7 is evenly distributed on the inner wall of reactive tank 2, and the reaction flask 8 is located at the middle part of reactive tank 2 and between reactive tank 2
Equipped with fixing seat 10, the two sides of the fixing seat 10 are equipped with symmetrical temperature sensor 9, the electric heating tube 7 and temperature
Sensor 9 is connected with PLC controller 3 respectively, and the top of the reactive tank 2 is equipped with fluid reservoir 11 and motor 12, the storage
Flow container 11 is fixedly connected at least provided with two and with reactive tank 2, and connecting tube 13 is equipped between the fluid reservoir 11 and reaction flask 8,
12 output end of motor runs through the top of reactive tank 2 and is fixedly connected with rotating disc 14, is designed, is subtracted by simple structure
The volume of small chemical synthesis instrument, is conveniently used in laboratory, while reducing production cost and maintenance cost.
It is further improved ground, as shown in Figure 2: the shaft 15 of rotation connection is equipped in the reaction flask 8, the shaft 15
Surface is fixedly connected with the first permanent magnet 16 and paddle 17, and first permanent magnet 16 is located at the top of paddle 17, passes through
The shaft 15 with paddle 17 is equipped in reaction flask 8, it is convenient that reaction solution in reaction flask 8 is stirred, improve solution
Reaction speed and reaction efficiency.
It is further improved ground, as shown in Figure 2: the upper and lower ends of the shaft 15 are respectively equipped with rotation seat 18, the rotation
Seat 18 is fixedly connected with reaction flask 8, by being respectively equipped with rotation seat 18 at the both ends of shaft 15, convenient for consolidating to shaft 15
It is fixed, it is convenient that the position of shaft 15 is fixed.
It is further improved ground, as shown in Figure 2: the lower surface of the rotating disc 14 is fixedly connected with the second permanent magnet 19, institute
The second permanent magnet 19 and 16 opposite face magnetic pole of the first permanent magnet are stated on the contrary, by being fixedly connected in the lower surface of rotating disc 14
Two permanent magnets 19 drive shaft 15 by the active force in magnetic field convenient for attracting the first permanent magnet 16 mutually with the second permanent magnet 19
It is rotated in reaction flask 8, it is convenient that reaction solution is stirred.
Specifically with improvement, as shown in Figs. 1-2: the connecting tube 13 and the junction of fluid reservoir 11 are equipped with electromagnetic throttle valve
20, the junction of the discharge nozzle 6 and reaction flask 8 is equipped with electromagnetic switch valve 21, the electromagnetic throttle valve 20 and electromagnetic switch valve
21 are connected with PLC controller 3 respectively, by being equipped with electromagnetic throttle valve 20 in the junction of connecting tube 13 and fluid reservoir 11, just
It is controlled in the dosage that stoste is added, reacts solution sufficiently, by being equipped in discharge nozzle 6 and the junction of reaction flask 8
Electromagnetic switch valve 21, convenient for solution after the reaction was completed is discharged.
The control cabinet -1, reactive tank -2, PLC controller -3, power switch -4, supporting leg -5, discharge nozzle-of the utility model
6, electric heating tube -7, reaction flask -8, temperature sensor -9, fixing seat -10, fluid reservoir -11, motor -12, connecting tube -13, turn
Moving plate -14, shaft -15, the first permanent magnet -16, paddle -17, rotation seat -18, the second permanent magnet -19, electromagnetic throttle valve -
20, electromagnetic switch valve -21, component be universal standard part or component, its structure and principle as known to those skilled in the art all
It can be learnt by technical manual for this technology personnel or be known by routine experiment method, which is specially DKC-
Y110PLC controller, the electromagnetic throttle valve are specially THF-G03 electromagnetic throttle valve, electromagnetic switch valve 2W025-08 electromagnetic switch
Valve, the electric heating tube are specially GYQ123 electric heating tube, and the utility model is convenient for real by using the reactive tank 2 of glass material
It tests personnel to be observed the reaction of solution, improves the intuitive of experimentation, designed by simple structure, reduce chemistry and close
The volume of Cheng Yi, is conveniently used in laboratory, while reducing production cost and maintenance cost.
When the utility model is used, the stoste of reaction is poured into fluid reservoir 11, then poured into reactive tank 2 suitable
Then the water of amount presses power switch 4, chemical synthesis instrument is made to start to work, and PLC controller 3 controls electric heating tube 7 and added
Heat, temperature sensing are measured in real time to water temperature and feed back to PLC controller 3, when water temperature is in reaction required temperature, PLC
It controls electromagnetic throttle valve 20 to open, while a certain amount of different stostes being added into reaction flask 8, stoste carries out in reaction flask 8
Chemical reaction, PLC controller 3 controls electromagnetic switch valve 21 and opens after the reaction was completed, by the solution after reaction along 6 row of discharge nozzle
Out, the operation of chemical solution synthesis is completed, PLC controller 3 repeats the operation automatically, realizes and carries out automatic cycle to chemical solution
Synthesis.
Actual production and application, the application especially in chemical synthesis has been put into the product that this programme is protected at present
Achieve certain success, it is clear that confirmed the product technical solution be it is beneficial, meet society need, be also suitable for
Batch production and popularization and use.
The basic principles and main features of the present invention and the advantages of the present invention have been shown and described above, for
For those skilled in the art, it is clear that the present invention is not limited to the details of the above exemplary embodiments, and without departing substantially from this
In the case where the spirit or essential attributes of utility model, the utility model can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the utility model is by institute
Attached claim rather than above description limit, it is intended that will fall within the meaning and scope of the equivalent elements of the claims
All changes are embraced therein.It should not treat any reference in the claims as limiting related right
It is required that.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (4)
1. a kind of use for laboratory self-loopa chemical synthesis instrument, including control cabinet (1) and reactive tank (2), it is characterised in that: described anti-
Slot (2) is answered to be fixedly connected on the top of control cabinet (1)；The surface of the control cabinet (1) be fixedly connected with PLC controller (3) and
Power switch (4), the power switch (4) are located at the right side of PLC controller (3), and the bottom of the control cabinet (1) is fixedly connected
Have supporting leg (5), the middle part of the control cabinet (1) is equipped with discharge nozzle (6) that is vertical and running through control cabinet (1)；
The reactive tank (2) uses glass material blow molding, is equipped with electric heating tube (7), reaction flask in the reactive tank (2)
(8) and temperature sensor (9), the electric heating tube (7) are evenly distributed on the inner wall of reactive tank (2), and the reaction flask (8) is located at
The middle part of reactive tank (2) and fixing seat (10) are equipped between reactive tank (2), the two sides of the fixing seat (10) are equipped with symmetrical point
The temperature sensor (9) of cloth, the electric heating tube (7) and temperature sensor (9) are connected with PLC controller (3) respectively, described
The top of reactive tank (2) be equipped with fluid reservoir (11) and motor (12), the fluid reservoir (11) at least provided with two and with react
Slot (2) is fixedly connected, and is equipped with connecting tube (13) between the fluid reservoir (11) and reaction flask (8), motor (12) output
End runs through the top of reactive tank (2) and is fixedly connected with rotating disc (14).
2. a kind of use for laboratory self-loopa chemical synthesis instrument according to claim 1, it is characterised in that: the reaction flask
(8) shaft (15) of rotation connection is equipped in, the surface of the shaft (15) is fixedly connected with the first permanent magnet (16) and stirring
Leaf (17), first permanent magnet (16) are located at the top of paddle (17).
3. a kind of use for laboratory self-loopa chemical synthesis instrument according to claim 2, it is characterised in that: the shaft (15)
Upper and lower ends be respectively equipped with rotation seat (18), the rotation seat (18) is fixedly connected with reaction flask (8), by shaft (15)
Both ends be respectively equipped with rotation seat (18), it is convenient that the position of shaft (15) is fixed convenient for shaft (15) is fixed.
4. a kind of use for laboratory self-loopa chemical synthesis instrument according to claim 2, it is characterised in that: the rotating disc
(14) lower surface is fixedly connected with the second permanent magnet (19), second permanent magnet (19) and the first permanent magnet (16) opposite face
Magnetic pole is opposite.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821525056.9U CN208959900U (en) | 2018-09-18 | 2018-09-18 | A kind of use for laboratory self-loopa chemical synthesis instrument |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821525056.9U CN208959900U (en) | 2018-09-18 | 2018-09-18 | A kind of use for laboratory self-loopa chemical synthesis instrument |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208959900U true CN208959900U (en) | 2019-06-11 |
Family
ID=66756341
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821525056.9U Expired - Fee Related CN208959900U (en) | 2018-09-18 | 2018-09-18 | A kind of use for laboratory self-loopa chemical synthesis instrument |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208959900U (en) |
-
2018
- 2018-09-18 CN CN201821525056.9U patent/CN208959900U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190611 Termination date: 20200918 |