CN208888091U - The measurement device of hydrogen content in a kind of silicone oil - Google Patents

Abstract

The utility model discloses a kind of measurement devices of hydrogen content in silicone oil, including pedestal, the side of the base top outer wall is equipped with reactor tank by bolt, and one end of reactor tank top exterior walls is equipped with inlet tube by bolt, one side bottom of the reactor tank outer circumferential walls is equipped with outlet tube by bolt, and the outer circumferential walls of outlet tube are equipped with liquid valve by bolt, by bearing installation, there are three the rotating bars equidistantly distributed between the both ends of the reactor tank circumferential inner wall, and the outer circumferential walls of rotating bar are welded with the paddle of arcuate structure.Rotating bar and paddle is set to carry out rotation stirring using driving motor, paddle uses arcuate structure, the liquid for reacting pot bottom is set to be stirred to top, and the wears groove of round-like structure is offered on paddle, utilize the aperture both ends mobility of different sizes for increasing liquid in reactor tank, it is reacted to make to come into full contact between silicone oil and lye, keeps hydrogen preparation complete.

Description

The measurement device of hydrogen content in a kind of silicone oil

Technical field

The utility model relates to a kind of measurement devices of hydrogen content in silicone oil production technical field more particularly to silicone oil.

Background technique

Containing hydrogen silicone oil is a kind of siliconated important object, is mainly used for the waterproofing agent and softening agent of fabric, contains Contain active Si -- H bond in hydrogen silicone oil, is the main component of containing hydrogen silicone oil function and effect, therefore the hydrogen content of containing hydrogen silicone oil is One important indicator of containing hydrogen silicone oil often needs to contain the silicone oil produced in the generation process of containing hydrogen silicone oil The detection of hydrogen amount.

To the hydrogeneous measurement top of silicone oil using volumetric method in general production process, in the presence of the substances such as akaline liquid Under, molecule in silicone oil and alkaline reaction displacing hydrogen, after being collected by eudiometer tube, the hydrogen released by the eudiometer tube First Astronautic Research Institute for Measurement and Test Volume, then using formula obtain hydrogen content number, but measurement device used at present, often due to hydrogen in silicone oil Not exclusively, leading to the data measured, there are biggish errors for preparation.

Utility model content

Purpose of the utility model is to solve disadvantages existing in the prior art, and hydrogeneous in a kind of silicone oil proposed The measurement device of amount.

To achieve the goals above, the utility model adopts the technical scheme that

The measurement device of hydrogen content in a kind of silicone oil, including pedestal, the side of the base top outer wall pass through bolt and pacify Equipped with reactor tank, and one end of reactor tank top exterior walls is equipped with inlet tube by bolt, and the one of the reactor tank outer circumferential walls Side bottom is equipped with outlet tube by bolt, and the outer circumferential walls of outlet tube are equipped with liquid valve, the reactor tank by bolt By bearing installation, there are three the rotating bars equidistantly distributed between the both ends of circumferential inner wall, and the outer circumferential walls of rotating bar are welded There is the paddle of arcuate structure, the top exterior walls of the paddle offer the perforation equidistantly distributed, the top of the reactor tank Portion's outer wall is equipped with attachment base by bolt, and the bottom outer wall of attachment base offers the air drain that connects of round-like structure, the company The top exterior walls of joint chair offer placing groove, and offer between the bottom interior wall of placing groove and the top internal diameter for connecing air drain logical Hole, the top and bottom between the inner wall of the placing groove two sides pass through bolt and are equipped with strainer, and fill between two strainers There is anhydrous cupric sulfate.

Preferably, the three described one end of rotating bar outer circumferential walls far from inlet tube are connected with same by bevel gear set Horizontal positioned driving motor.

Preferably, the side of the base top outer wall far from reactor tank passes through bolt respectively and is equipped with measurement pipe and reference Pipe is equipped with the connecting tube of the same arcuate structure by bolt between the bottom of measurement pipe and the bottom outer wall of reference pipe.

Preferably, the top exterior walls of the attachment base are equipped with intermediate tube by bolt, and intermediate tube is far from attachment base One end outer wall is connected by the top exterior walls of bolt and measurement pipe, and the circumferential inner wall of measurement pipe slidably connects floating block.

Preferably, the top with reference to pipe outer circumferential walls is threaded with cover board, and the bottom outer wall of cover board passes through spiral shell It is circular fixed plate that bolt, which is equipped with cross section,.

Preferably, the bottom outer wall of the fixed plate is bonded with the rubber pad of cyclic structure, and with reference to pipe circumferential inner wall Top offers the seal groove of cyclic structure, matches between rubber pad and seal groove.

Preferably, the bottom outer wall of the cover board is welded with the link block of cyclic structure, and opens with reference to the top exterior walls of pipe Equipped with link slot corresponding with link block, match between link block and link slot.

The utility model has the following beneficial effects:

1, suitable lye is first added from inlet tube, adds quantitative silicone oil, then makes to rotate using driving motor Bar and paddle carry out rotation stirring, and paddle uses arcuate structure, and the liquid for reacting pot bottom is made to be stirred to top, and The wears groove that round-like structure is offered on paddle, using aperture both ends it is of different sizes increase reactor tank in liquid mobility, It is reacted to make to come into full contact between silicone oil and lye, makes hydrogen preparation completely, guarantee the accurate fixed of determination data.

2, it is arranged to inverted bucket-shaped structure at the top of reactor tank, and air drain will be connect and be arranged to round-like structure, thus convenient The hydrogen of preparation is stored to be measured, and is provided with anhydrous cupric sulfate in placing groove, because of reaction fever in reactor tank The vapor of production reduces the content of hydrone in measurement hydrogen by anhydrous slufuric acid Copper uptakie, to improve hydrogen volume measurement Accuracy.

3, hydrogen enters in measurement pipe from intermediate tube, measurement pipe, with reference in pipe and connecting tube filled with measurement liquid, hydrogen Entering in measurement pipe makes the water level for measuring liquid change, and judges hydrogen using the lifting distance in measurement pipe of water level The volume of preparation will be sealed at the top of reference pipe using cover board and fixed plate when not in use to be measured, utilize rubber Pad and the matching of seal groove and the matching of link block and link slot increase fixed plate and cover board and with reference to the sealing between pipe Property, reduce the evaporation of measurement liquid.

Detailed description of the invention

Fig. 1 be the utility model proposes a kind of silicone oil in hydrogen content measurement device overall structure diagram；

Fig. 2 be the utility model proposes a kind of silicone oil in hydrogen content measurement device reactor tank side view structure signal Figure；

Fig. 3 be the utility model proposes a kind of silicone oil in hydrogen content measurement device cover board partial enlargement structural representation Figure.

In figure: 1 pedestal, 2 reactor tanks, 3 inlet tubes, 4 outlet tubes, 5 rotating bars, 6 paddles, 7 perforation, 8 driving motors, 9 Attachment base, 10 connect air drain, 11 placing grooves, 12 strainers, 13 anhydrous cupric sulfates, 14 measurement pipes, 15 with reference to pipes, 16 connecting tubes, 17 float Block, 18 cover boards, 19 fixed plates, 20 rubber pads, 21 link blocks, 22 link slots.

Specific embodiment

The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.

Referring to Fig.1-3, in a kind of silicone oil hydrogen content measurement device, the side of including pedestal 1,1 top exterior walls of pedestal is logical It crosses bolt and reactor tank 2 is installed, and one end of 2 top exterior walls of reactor tank is equipped with inlet tube 3,2 circumference of reactor tank by bolt One side bottom of outer wall is equipped with outlet tube 4 by bolt, and the outer circumferential walls of outlet tube 4 are equipped with liquid valve by bolt, The top of reactor tank 2 is in inverted bucket-shaped structure, and by bearing installation, there are three equidistantly between the both ends of 2 circumferential inner wall of reactor tank Rotating bar 5 from distribution, and the outer circumferential walls of rotating bar 5 are welded with the paddle 6 of arcuate structure, the top exterior walls of paddle 6 The perforation 7 equidistantly distributed is offered, and the top internal diameter of perforation 7 is greater than its bottom inner diameter, the top exterior walls of reactor tank 2 pass through Bolt is equipped with attachment base 9, and the bottom outer wall of attachment base 9 offer round-like structure connect air drain 10, connect the bottom of air drain 10 Portion's internal diameter is greater than its top internal diameter, and the bottom inner diameter for connecing air drain 10 is equal to the top internal diameter of reactor tank 2, the top of attachment base 9 Outer wall offers placing groove 11, and offers through-hole between the bottom interior wall of placing groove 11 and the top internal diameter for connecing air drain 10, puts It sets the top and bottom between 11 two sides inner wall of slot and passes through bolt and strainer 12 is installed, and be filled with nothing between two strainers 12 Brochanite 13.

In the utility model, three one end of 5 outer circumferential walls of rotating bar far from inlet tube 3 are connected with together by bevel gear set One horizontal positioned driving motor 8, and the bottom outer wall of driving motor 8 is connect by bolt with the top exterior walls of pedestal 1, bottom Seat side of 1 top exterior walls far from reactor tank 2 is equipped with support rod by bolt, and the top exterior walls of two support rods are led to respectively It crosses bolt measurement pipe 14 is installed and refers to pipe 15, passes through bolt between the bottom of measurement pipe 14 and the bottom outer wall of reference pipe 15 The connecting tube 16 of the same arcuate structure is installed, the bottom outer wall of connecting tube 16 is connected by the top exterior walls of bolt and pedestal 1 It connects, the top exterior walls of attachment base 9 are equipped with intermediate tube by bolt, and intermediate tube passes through spiral shell far from one end outer wall of attachment base 9 Bolt is connect with the top exterior walls of measurement pipe 14, and measurement pipe 14 is filled with measurement liquid with reference to the inside of pipe 15 and connecting tube 16, is surveyed The circumferential inner wall of buret 14 slidably connects floating block 17, is threaded with cover board 18 with reference to the top of 15 outer circumferential walls of pipe, and cover It is circular fixed plate 19 that the bottom outer wall of plate 18, which is equipped with cross section by bolt, and the outer circumferential walls of fixed plate 19 and reference are managed 15 circumferential inner wall is slidably connected, and the bottom outer wall of fixed plate 19 is bonded with the rubber pad 20 of cyclic structure, and with reference to the circle of pipe 15 The seal groove of cyclic structure is offered at the top of all inner walls, is matched between rubber pad 20 and seal groove, with reference to the top of pipe 15 It is arranged to funnel-shaped structure, and is greater than the volume of measurement pipe 14 with reference to the volume of pipe 15, the bottom outer wall of cover board 18 is welded with ring The link block 21 of shape structure, and link slot 22 corresponding with link block 21, link block 21 are offered with reference to the top exterior walls of pipe 15 Cross section with link slot 22 is triangle, is matched between link block 21 and link slot 22.

Working principle: from suitable lye is first added in inlet tube 3 into reactor tank 2, quantitative silicone oil is added, then So that rotating bar 5 and paddle 6 is carried out rotation stirring using driving motor 8, using paddle 67 both ends pore size of perforation not With the mobility for increasing liquid in reactor tank, the hydrogen generated in reactor tank 2 enters in placing groove 11 from air drain 10 is connect, and utilizes Anhydrous cupric sulfate 13 absorbs the steam in gas, and then hydrogen enters in measurement pipe 14, is measuring floating block 17 and measurement liquid SEA LEVEL VARIATION in pipe 14 realizes the measurement of hydrogen content to obtain the volume of hydrogen preparation.

The preferable specific embodiment of the above, only the utility model, but the protection scope of the utility model is not It is confined to this, anyone skilled in the art is within the technical scope disclosed by the utility model, practical according to this Novel technical solution and its utility model design are subject to equivalent substitution or change, should all cover the protection model in the utility model Within enclosing.

Claims (7)

1. the measurement device of hydrogen content in a kind of silicone oil, including pedestal (1), which is characterized in that pedestal (1) top exterior walls Side is equipped with reactor tank (2) by bolt, and one end of reactor tank (2) top exterior walls is equipped with inlet tube (3) by bolt, One side bottom of reactor tank (2) outer circumferential walls is equipped with outlet tube (4) by bolt, and the outer circumferential walls of outlet tube (4) Liquid valve is installed by bolt, there are three equidistant by bearing installation between the both ends of reactor tank (2) circumferential inner wall The rotating bar (5) of distribution, and the outer circumferential walls of rotating bar (5) are welded with the paddle (6) of arcuate structure, the paddle (6) Top exterior walls offer the perforation (7) equidistantly distributed, the top exterior walls of the reactor tank (2) are equipped with connection by bolt Seat (9), and the bottom outer wall of attachment base (9) offers connecing air drain (10) for round-like structure, outside the top of the attachment base (9) Wall offers placing groove (11), and offers between the bottom interior wall of placing groove (11) and the top internal diameter for connecing air drain (10) logical Hole, the top and bottom between the inner wall of placing groove (11) two sides pass through bolt and are equipped with strainer (12), and two strainers (12) anhydrous cupric sulfate (13) are filled between.

2. the measurement device of hydrogen content in a kind of silicone oil according to claim 1, which is characterized in that three rotating bars (5) one end of outer circumferential walls far from inlet tube (3) is connected with the same horizontal positioned driving motor (8) by bevel gear set.

3. the measurement device of hydrogen content in a kind of silicone oil according to claim 1, which is characterized in that pedestal (1) top Portion's outer wall passes through bolt far from the side of reactor tank (2) respectively and is equipped with measurement pipe (14) and with reference to pipe (15), measurement pipe (14) Bottom and bottom outer wall with reference to pipe (15) between the connecting tube (16) of the same arcuate structure is installed by bolt.

4. the measurement device of hydrogen content in a kind of silicone oil according to claim 1, which is characterized in that the attachment base (9) Top exterior walls intermediate tube is equipped with by bolt, and one end outer wall of the intermediate tube far from attachment base (9) passes through bolt and measurement The top exterior walls connection of (14) is managed, the circumferential inner wall of measurement pipe (14) slidably connects floating block (17).

5. the measurement device of hydrogen content in a kind of silicone oil according to claim 3, which is characterized in that described with reference to pipe (15) The top of outer circumferential walls is threaded with cover board (18), and the bottom outer wall of cover board (18) is equipped with cross section by bolt as circle The fixed plate (19) of shape.

6. the measurement device of hydrogen content in a kind of silicone oil according to claim 5, which is characterized in that the fixed plate (19) Bottom outer wall be bonded with the rubber pad (20) of cyclic structure, and with reference to offering cyclic structure at the top of pipe (15) circumferential inner wall Seal groove, match between rubber pad (20) and seal groove.

7. the measurement device of hydrogen content in a kind of silicone oil according to claim 5, which is characterized in that the cover board (18) Bottom outer wall is welded with the link block (21) of cyclic structure, and offer with reference to the top exterior walls of pipe (15) it is right with link block (21) The link slot (22) answered, matches between link block (21) and link slot (22).