CN205785979U - A kind of Chemical cleaning evaluation gas collection measurement apparatus - Google Patents

A kind of Chemical cleaning evaluation gas collection measurement apparatus Download PDF

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Publication number
CN205785979U
CN205785979U CN201620754743.2U CN201620754743U CN205785979U CN 205785979 U CN205785979 U CN 205785979U CN 201620754743 U CN201620754743 U CN 201620754743U CN 205785979 U CN205785979 U CN 205785979U
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China
Prior art keywords
bottle
inner bag
measurement apparatus
gas collection
chemical cleaning
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Active
Application number
CN201620754743.2U
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Chinese (zh)
Inventor
刘斌
李新民
宋利君
鲁俊东
张于
朱海建
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China General Nuclear Power Corp
CGN Power Co Ltd
Guangdong Nuclear Power Joint Venture Co Ltd
Suzhou Nuclear Power Research Institute Co Ltd
Original Assignee
China General Nuclear Power Corp
CGN Power Co Ltd
Guangdong Nuclear Power Joint Venture Co Ltd
Suzhou Nuclear Power Research Institute Co Ltd
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Application filed by China General Nuclear Power Corp, CGN Power Co Ltd, Guangdong Nuclear Power Joint Venture Co Ltd, Suzhou Nuclear Power Research Institute Co Ltd filed Critical China General Nuclear Power Corp
Priority to CN201620754743.2U priority Critical patent/CN205785979U/en
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Publication of CN205785979U publication Critical patent/CN205785979U/en
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Abstract

This utility model relates to a kind of Chemical cleaning evaluation gas collection measurement apparatus, it includes bottle, is sealingly mounted at described bottle top and extends to its internal inner bag, closing lid bottle cap on described inner bag, be arranged on described bottle cap and the flexible pipe, the valve being arranged on described flexible pipe that are connected with described inner bag and be connected with described bottle bottom and higher than the graded tube of described valve, the sectional area of described graded tube is less than the sectional area of described bottle.Add reactant liquor by graded tube to whole gas collection measurement apparatus and submerge in inner bag, such that it is able to react with being placed on incrustation scale therein, the gas so produced is enriched in the top of bottle and makes the liquid level of graded tube increase, finally realize the measurement to gas volume, there is the advantages such as degree of accuracy height, compact conformation, easy and simple to handle, safe and reliable, good stability.

Description

A kind of Chemical cleaning evaluation gas collection measurement apparatus
Technical field
This utility model relates to a kind of gas collection measurement apparatus, is specifically related to a kind of Chemical cleaning evaluation gas collection and measures dress Put.
Background technology
Heat power equipment Chemical cleaning, be make heating surface inner surface cleaning, prevent heating surface because of corrosion and fouling cause accident Requisite measure, be the most also simultaneously to improve the thermal efficiency, improve the effective measures of media qualities.The main object of Chemical cleaning has calcium and magnesium Dirt, Ferric oxide scale, copper dirt, silicate scale, grease and other dirts, these dirts contact with acid cleansing medium and mostly can produce Gas, it is necessary to accurately collect and carry out chromatography, it is to avoid hydrogen Local enrichment causes blast because of naked light.
Additionally, PWR nuclear power plant is along with the growth of the time of operation, steam generator secondary side tube sheet, tube support plate, biography Tube surface and pipe aperture all can deposit attack products.Use water under high pressure machinery to rinse and periodically remove deposit, be to prevent material One of important measures that material burn into extends steam generator service life.One of the assessment of vaporizer water developing result important interior Appearance is to rinse the size of iron content in residue, and iron content is the lowest, and developing result is the best.
For above two occasion, traditional gas collecting apparatus is collected gas by drainage, is needed pyriform funnel, solid-liquid anti- Zero accessory such as Ying Guan, plug, inducing QI sebific duct, gas collecting bottle, aspirator, hermetic seal checks the most defective, and remains in solid-liquid Air interference in reaction tube and inducing QI sebific duct produces the composition of gas.If course of reaction gas generated less time, gas Collecting more difficulty, the error causing assessment developing result is bigger.
Summary of the invention
This utility model purpose is to provide a kind of Chemical cleaning evaluation gas collection to survey to overcome the deficiencies in the prior art Amount device.
For reaching above-mentioned purpose, the technical solution adopted in the utility model is: a kind of Chemical cleaning evaluation gas collection is measured Device, it includes bottle, is sealingly mounted at described bottle top and extends to its internal inner bag, closing lid on described inner bag Bottle cap, be arranged on described bottle cap and be connected with described inner bag flexible pipe, the valve being arranged on described flexible pipe and with institute Stating the graded tube that bottle bottom is connected and is higher than described valve, the sectional area of described graded tube is less than the cross section of described bottle Long-pending.
Optimally, the connectivity part of described graded tube and described bottle is provided with sand core filter.
Further, it is placed with magnetic stir bar in described bottle.
Further, it is the sieve aperture of 5 ~ 20 mm that the sidewall of described inner bag offers bottom it, the aperture of described sieve aperture It is 2 ~ 5 mm.
Owing to technique scheme is used, this utility model compared with prior art has the advantage that this utility model Chemical cleaning evaluation gas collection measurement apparatus, adds reactant liquor and the inner bag that submerges by graded tube to whole gas collection measurement apparatus In, such that it is able to react with being placed on incrustation scale therein, the gas so produced is enriched in the top of bottle and makes scale The liquid level of pipe rises, and finally realizes the measurement to gas volume, have degree of accuracy height, compact conformation, easy and simple to handle, safe can Lean on, the advantage such as good stability.
Accompanying drawing explanation
Accompanying drawing 1 is the structural representation of this utility model Chemical cleaning evaluation gas collection measurement apparatus;
Wherein, 1, water-bath;2, bottle;3, inner bag;4, bottle cap;5, valve;6, flexible pipe;7, graded tube;8, core filters Device;9, magnetic stir bar.
Detailed description of the invention
This utility model is further described by the embodiment shown in below in conjunction with the accompanying drawings.
Chemical cleaning evaluation gas collection measurement apparatus as shown in Figure 1, mainly includes bottle 2, inner bag 3, bottle cap 4, valve 5 With graded tube 7 etc..
Wherein, in bottle 2 is generally positioned at water-bath 1.Inner bag 3(can be glass material) it is arranged on the top of bottle 2 Portion, and extend to the inside of bottle 2, for holding the incrustation scale scraped off or other question response solid matter;The bottom of inner bag 3 Without perforate, the uniformly perforate of the surrounding at the certain altitude of bottom of its sidewall (perforate height can select as required, preferably 5 ~ 20 mm), aperture is Ф 2 ~ 5 mm.In the present embodiment, the bottleneck of bottle 2 is trapezoidal and band external screw thread, interior frosted, it is simple to interior The installation of gallbladder 3, take out and seal, prevent gas leakage;Bottle 2 inwall is round and smooth, and surrounding rounded corners processes, it is to avoid bubble adsorbs and molten Liquid is detained.Graded tube 7 is connected with the bottom of bottle 3, and (in the present embodiment, graded tube 7 is connected with the bottom of bottle 3 side Logical), in bottle 3, add reactant liquor by graded tube 7;Their the built-in sand core filter of connectivity part (aperture Ф 10 ~ 15 μ M), this sand core filter acid-alkali-corrosive-resisting and redox reaction, there is the effect filtering precipitate and washing gas, prevent anti- Gas and byproduct of reaction should be produced because of in the violent diffusion mobility of stirring to graded tube 7;Graded tube 7 is with scale, as required Select measurement scope and precision size (typically regulate different cross section size and regulate certainty of measurement).The corresponding closing lid of bottle cap 4 exists On inner bag 3, in order to ensure to seal, gasket seal can be installed in bottle cap 4;Bottle cap 4 is provided with the flexible pipe being connected with inner bag 3 6, and the valve 5 controlling its break-make is set on flexible pipe 6;Bottle cap 4 is made up of Kynoar (PVDF) material, built-in fluorubber Sealing gasket, flexible pipe 6 and valve 5 are PTFE material, have pressure, high temperature resistant, the property of acid-alkali-corrosive-resisting, resistance to oxidation reduction reaction Matter, should be noted that cleanout fluid accident overflow when preventing valve 5 fault in use.Such gas collection measurement apparatus does not has attached joining Part, efficiently solves the difficulty that in conventional apparatus, in solid-liquid reaction pipe and inducing QI sebific duct, residual gas cannot accurately measure, and improves The accuracy measured;Reaction can be accurately conversed by the liquid level difference association reaction temperature before and after reaction in record graded tube 7 The gas flow produced.
Need first to check the air-tightness of whole gas collection measurement apparatus before the use, prevent it from leaking gas, particularly as follows: by water-bath Pot 1 adds water to certain altitude so that water surface elevation exceeds the valve 5(of this gas collection measurement apparatus and i.e. adds water so that bottle 2 immerses water Below body lotion face), it is ensured that not effervescent;If effervescent, the sealing gasket in bottle cap 4 need to be changed.In use, can be in water-bath Add water to certain altitude in pot 1, controlled the temperature of chemical reaction process by the temperature of regulation water.In the present embodiment, carve The height of degree pipe 7 is higher than the height of valve 5, to prevent reactant liquor from overflowing;The sectional area of graded tube 7 is less than the cross section of bottle 2 Long-pending, such graded tube 7 is the thinnest and precision of gas collection measurement apparatus is the highest;Reference zero graduation correspondence bottle cap 4 crown valve of graded tube 7 The position of door 5, its range correspondence bottle 2 sectional area and inner bag 3 product highly.In the present embodiment, it is placed with magnetic in bottle 2 Power stirrer 9, olive shape magnetic stir bar (length 35mm, the diameter that magnetic stir bar 9 is wrapped up for polytetrafluoroethylene (PTFE) 13mm), the mixing speed of chemical reaction is controlled by bottom magnetic force agitating heating device rotational speed regulation.
This gas collection measurement apparatus has self termination defencive function, when reaction is excessively strong, produces gas flow beyond measuring pipe During range, corresponding bottle cohesion collection gas is also by the bottom of cleaning solution liquid level extruding to glass inner bag, and solution departs from solid Contact, sluggish terminates.
Above-described embodiment only for technology of the present utility model design and feature are described, its object is to allow and is familiar with technique Personage will appreciate that content of the present utility model and implement according to this, protection domain of the present utility model can not be limited with this. All according to this utility model spirit made equivalence change or modify, all should contain protection domain of the present utility model it In.

Claims (4)

1. a Chemical cleaning evaluation gas collection measurement apparatus, it is characterised in that: it includes bottle, is sealingly mounted at described bottle Top and extend to its internal inner bag, closing lid bottle cap on described inner bag, be arranged on described bottle cap and with described inner bag The flexible pipe being connected, the valve being arranged on described flexible pipe and be connected with described bottle bottom and higher than quarter of described valve Degree pipe, the sectional area of described graded tube is less than the sectional area of described bottle.
Chemical cleaning evaluation gas collection measurement apparatus the most according to claim 1, it is characterised in that: described graded tube and institute The connectivity part stating bottle is provided with sand core filter.
Chemical cleaning evaluation gas collection measurement apparatus the most according to claim 1 and 2, it is characterised in that: in described bottle It is placed with magnetic stir bar.
Chemical cleaning evaluation gas collection measurement apparatus the most according to claim 1 and 2, it is characterised in that: described inner bag It is the sieve aperture of 5 ~ 20 mm that sidewall offers bottom it, and the aperture of described sieve aperture is 2 ~ 5 mm.
CN201620754743.2U 2016-07-19 2016-07-19 A kind of Chemical cleaning evaluation gas collection measurement apparatus Active CN205785979U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620754743.2U CN205785979U (en) 2016-07-19 2016-07-19 A kind of Chemical cleaning evaluation gas collection measurement apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620754743.2U CN205785979U (en) 2016-07-19 2016-07-19 A kind of Chemical cleaning evaluation gas collection measurement apparatus

Publications (1)

Publication Number Publication Date
CN205785979U true CN205785979U (en) 2016-12-07

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114577550A (en) * 2020-12-01 2022-06-03 中国石油天然气股份有限公司 Device and method for collecting top gas of rock debris tank

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114577550A (en) * 2020-12-01 2022-06-03 中国石油天然气股份有限公司 Device and method for collecting top gas of rock debris tank
CN114577550B (en) * 2020-12-01 2024-06-25 中国石油天然气股份有限公司 Device and method for collecting rock debris tank top gas

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