CN208883492U - A kind of nitric acid equipment for purifying - Google Patents

A kind of nitric acid equipment for purifying Download PDF

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Publication number
CN208883492U
CN208883492U CN201821365720.8U CN201821365720U CN208883492U CN 208883492 U CN208883492 U CN 208883492U CN 201821365720 U CN201821365720 U CN 201821365720U CN 208883492 U CN208883492 U CN 208883492U
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China
Prior art keywords
nitric acid
cooler
connect
pipe
pipeline
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Active
Application number
CN201821365720.8U
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Chinese (zh)
Inventor
骆家栓
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KUNSHAN SIGO MICROELECTRONICS MATERIALS Co Ltd
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KUNSHAN SIGO MICROELECTRONICS MATERIALS Co Ltd
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Priority to CN201821365720.8U priority Critical patent/CN208883492U/en
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Abstract

A kind of nitric acid equipment for purifying, including evaporator, evaporator outer surface is equipped with steam delivery port and steam outlet, evaporator and purification column are connected with each other by steam conveying pipe and vapor discharge channel, the top of purification column is connect by nitric acid vapor pipeline with the first cooler, make to connect at the top of the first cooler and bleaching tower by first pipe, decoloration tower bottom is connect by second pipe with the second cooler, second cooler upper surface is equipped with third pipeline, and third pipeline is equipped with nitric acid outlet;The application passes through steam rectification and purification mode, compared to the energy consumption that power consumption can reduce 35 percent, and using 70 percent nitric acid as purification raw material, make it while reducing concentration, the purity needed for it can equally be obtained, reach reduction environmental pollution, saves the beneficial effect of energy resource.

Description

A kind of nitric acid equipment for purifying
Technical field
The utility model relates to a kind of nitric acid equipment for purifying, especially one kind can reduce disposal of pollutants, save energy money The nitric acid equipment for purifying in source.
Background technique
Nitric acid is that one kind has strong oxidizing property, corrosive strong acid, and the involved range used is very wide, is commonly used in agriculture The fields such as industry, chemistry, and the nitric acid after purification must be used to be made under the conditions of certain specific as raw material, otherwise can The quality of product is influenced, usual nitric acid purification is using using electric heating rectifying, and which energy consumption is higher, and raw material uses percentage 98 or more fuming nitric aicd, there are a large amount of acidic materials, ultimately cause and improve environmental pollution, waste energy resource Consequence.
Summary of the invention
To solve the above problems, the utility model provides a kind of nitric acid equipment for purifying.
The technical scheme adopted by the utility model to solve the technical problem is as follows: a kind of nitric acid equipment for purifying, including evaporation Device, it is characterised in that: the evaporator outer surface is equipped with steam delivery port and steam outlet, by steam conveying pipe and Vapor discharge channel is connected with each other evaporator and purification column, and the vapor discharge channel bottom is equipped with valve, the valve bottom Portion is equipped with waste liquid discharge conduit, and waste liquid discharge conduit end is equipped with waste liquid discharge port, and the top of the purification column is steamed by nitric acid Steam pipe road is connect with the first cooler, and first cooler is equipped with Waste gas outlet, makes described first by first pipe It is connect at the top of cooler and bleaching tower, bleaching tower lower outside surface is equipped with air compressor machine installing port, the decoloration tower bottom It is connect by second pipe with the second cooler, first cooler and the second cooler both ends are symmetrically arranged with cooling water inlet And coolant outlet, second cooler upper surface are equipped with third pipeline, the third pipeline is equipped with nitric acid outlet, described Second cooler bottom is equipped with hydrops and empties pipeline, and nitric acid tank outer surface is equipped with nitric acid delivery port, and bottom is equipped with nitric acid waste Discharge conduit, and connect with waste liquid discharge conduit, the nitric acid tank is connect with purification column by nitric acid pipe.
The beneficial effects of the utility model are: the application can be dropped by steam rectification and purification mode compared to power consumption Low 35 percent energy consumption, and using 70 percent nitric acid as purification raw material, reducing it by concentration Meanwhile the purity needed for it can be equally obtained, reach reduction environmental pollution, saves the beneficial effect of energy resource.
Detailed description of the invention
Fig. 1 is the structural schematic diagram according to the utility model embodiment.
Appended drawing reference: evaporator 1, purification column 2, the first cooler 3, first pipe 4, bleaching tower 5, second pipe 6, second Cooler 7, nitric acid tank 8, waste liquid discharge conduit 9, steam delivery port 11, steam outlet 12, steam conveying pipe 13, steam row Put pipeline 14, nitric acid vapor pipeline 21, cooling water inlet 31, coolant outlet 32, Waste gas outlet 33, air compressor machine installing port 51, Three pipelines 71, nitric acid outlet 72, hydrops empty pipeline 73, nitric acid delivery port 81, nitric acid pipe 82, nitric acid waste discharge conduit 83, waste liquid discharge port 91, valve 121.
Specific embodiment
For the technical solution of the utility model is more clearly understood, specific embodiment is practical new to this with reference to the accompanying drawing Type is described further.
As shown in Fig. 1, according to a kind of nitric acid equipment for purifying of the utility model embodiment, including evaporator 1, the steaming It sends out 1 outer surface of device and is equipped with steam delivery port 11 and steam outlet 12, pass through steam conveying pipe 13 and steam discharge pipe Road 14 is connected with each other evaporator 1 and purification column 2, and 14 bottom of vapor discharge channel is equipped with valve 121, the valve 121 bottoms are equipped with waste liquid discharge conduit 9, and 9 end of waste liquid discharge conduit is equipped with waste liquid discharge port 91, the top of the purification column 2 Portion is connect by nitric acid vapor pipeline 21 with the first cooler 3, and first cooler 3 is equipped with Waste gas outlet 33, is led to Crossing first pipe 4 makes to connect at the top of first cooler 3 and bleaching tower 5, and the 5 lower outside surface of bleaching tower is equipped with Air compressor machine installing port 51,5 bottom of bleaching tower are connect by second pipe 6 with the second cooler 7, and described first is cooling Device 3 and 7 both ends of the second cooler are symmetrically arranged with cooling water inlet 31 and coolant outlet 32,7 upper surface of the second cooler Equipped with third pipeline 71, the third pipeline 71 is equipped with nitric acid outlet 72, and 7 bottom of the second cooler is equipped with hydrops Empty pipeline 73,8 outer surface of nitric acid tank is equipped with nitric acid delivery port 81, and bottom is equipped with nitric acid waste discharge conduit 83, and with it is useless Liquid discharge conduit 9 connects, and connect the nitric acid tank 8 with purification column 2 by nitric acid pipe 82.
As shown in Fig. 1, when needing to purify to nitric acid using the application, when removing impurity, firstly, closing valve 121, then the nitric acid of required purification is transported in nitric acid tank 8 by nitric acid delivery port 81, the nitric acid in nitric acid tank 8 will It is flowed by nitric acid pipe 82 in the pipeline of evaporator 1, then air compressor machine is mounted on bleaching tower 5 by air compressor machine installing port 51 On, appropriate cold water is added into the first cooler 3 and the second cooler 7 by cooling water inlet 31, and start condenser, it is quasi- After ready, steam is imported in evaporator 1 by steam delivery port 11, since steam and nitric acid cannot be contacted directly, because This, the pipeline in evaporator 1 is all double-layer structure, and nitric acid flows into interior conduit, and the steam imported table on the outside of interior conduit Face is heated across nitric acid of the interior conduit to its inside, so that it is become steam and is floated up into purification column 2, purification column 2 The interior filtrate being equipped with to nitric acid vapor can filter its internal impurity and float all the way up, pass through when nitric acid vapor passes through Nitric acid vapor pipeline 21, which enters in the first cooler 3, to be condensed, and nitric acid vapor is made to be converted into nitric acid liquid, generated useless It abandons and is discharged from Waste gas outlet 33, and the liquid converted is further flowed into bleaching tower 5 by first pipe 4 and is taken off Color, the air compressor machine in bleaching tower 5 it can be dried filtering decoloration, and temperature is higher in decolorization can reach significant Effect, nitric acid after being decolourized flows into the second cooler 7 through second pipe 6 to cool down, and can finally be discharged from nitric acid Mouth 72 collects the nitric acid of purifying, can open valve 121 after purification, and the waste liquid in rapid steamer 1 is passed through waste liquid and is drained Pipeline 9 is drained from waste liquid discharge port 91, if needing to clear up the second cooler 7, hydrops is emptied on pipeline 73 Valve opening the hydrops inside pipeline can be emptied, it is cleared up later, by this way nitric acid purified Filter, has reached reduction environmental pollution, has saved the beneficial effect of energy resource.
Above embodiments can be combined with each other in the case where not being antagonistic mutually, further implement.
The preferable specific embodiment of the above, only the utility model, but the protection scope of the utility model is not It is confined to this, anyone skilled in the art is within the technical scope disclosed by the utility model, practical according to this Novel technical solution and its utility model design are subject to equivalent substitution or change, should all cover the protection model in the utility model Within enclosing.

Claims (1)

1. a kind of nitric acid equipment for purifying, including evaporator (1), it is characterised in that: evaporator (1) outer surface is equipped with steam Delivery port (11) and steam outlet (12) make evaporator (1) by steam conveying pipe (13) and vapor discharge channel (14) It is connected with each other with purification column (2), vapor discharge channel (14) bottom is equipped with valve (121), and valve (121) bottom is set Have waste liquid discharge conduit (9), waste liquid discharge conduit (9) end is equipped with waste liquid discharge port (91), and the top of the purification column (2) is logical Pernitric acid jet chimney (21) is connect with the first cooler (3), and first cooler (3) is equipped with Waste gas outlet (33), Make to connect at the top of first cooler (3) and bleaching tower (5) by first pipe (4), bleaching tower (5) the lower outside table Face is equipped with air compressor machine installing port (51), and bleaching tower (5) bottom is connect by second pipe (6) with the second cooler (7), institute It states the first cooler (3) and the second cooler (7) both ends is symmetrically arranged with cooling water inlet (31) and coolant outlet (32), described Two coolers (7) upper surface is equipped with third pipeline (71), and the third pipeline (71) is equipped with nitric acid outlet (72), and described the Two coolers (7) bottom is equipped with hydrops emptying pipeline (73), and nitric acid tank (8) outer surface is equipped with nitric acid delivery port (81), bottom It is connect equipped with nitric acid waste discharge conduit (83), and with waste liquid discharge conduit (9), the nitric acid tank is made by nitric acid pipe (82) (8) it is connect with purification column (2).
CN201821365720.8U 2018-08-23 2018-08-23 A kind of nitric acid equipment for purifying Active CN208883492U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821365720.8U CN208883492U (en) 2018-08-23 2018-08-23 A kind of nitric acid equipment for purifying

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821365720.8U CN208883492U (en) 2018-08-23 2018-08-23 A kind of nitric acid equipment for purifying

Publications (1)

Publication Number Publication Date
CN208883492U true CN208883492U (en) 2019-05-21

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821365720.8U Active CN208883492U (en) 2018-08-23 2018-08-23 A kind of nitric acid equipment for purifying

Country Status (1)

Country Link
CN (1) CN208883492U (en)

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