CN208878618U - Thermostatical oil bath - Google Patents
Thermostatical oil bath Download PDFInfo
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- CN208878618U CN208878618U CN201821447652.XU CN201821447652U CN208878618U CN 208878618 U CN208878618 U CN 208878618U CN 201821447652 U CN201821447652 U CN 201821447652U CN 208878618 U CN208878618 U CN 208878618U
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- oil
- blender
- heater
- thermostatical
- experimental
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- 230000001050 lubricating effect Effects 0.000 claims abstract description 40
- 238000002474 experimental method Methods 0.000 claims abstract description 33
- 238000010438 heat treatment Methods 0.000 claims abstract description 14
- 230000001737 promoting effect Effects 0.000 claims abstract description 4
- 239000000523 sample Substances 0.000 claims description 35
- 238000001514 detection method Methods 0.000 claims description 4
- 230000005611 electricity Effects 0.000 claims description 3
- 238000012360 testing method Methods 0.000 abstract description 9
- 238000010586 diagram Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000012827 research and development Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 238000013461 design Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- WLDHEUZGFKACJH-UHFFFAOYSA-K amaranth Chemical compound [Na+].[Na+].[Na+].C12=CC=C(S([O-])(=O)=O)C=C2C=C(S([O-])(=O)=O)C(O)=C1N=NC1=CC=C(S([O-])(=O)=O)C2=CC=CC=C12 WLDHEUZGFKACJH-UHFFFAOYSA-K 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000015927 pasta Nutrition 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
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- Devices For Use In Laboratory Experiments (AREA)
Abstract
The utility model relates to a kind of thermostatical oil baths, for carrying out oil bath experiment to experiment sample, thermostatical oil bath includes the oil drum for containing conduction oil, the lubricating cup for containing experimental oil, the heater for heating conduction oil, the blender for promoting conduction oil to flow, the sensor and control circuit for detecting thermally conductive oil temperature and experimental oil temperature respectively;Lubricating cup is set in oil drum and at least part of lubricating cup immerses in conduction oil, and control circuit is connected with heater, blender, sensor respectively, and experiment sample hangs and is infiltrated in experimental oil.The utility model can be improved experimental data accuracy, reduce repetition test frequency, improves working efficiency, adapts to the requirements at the higher level tested to oil bath.
Description
Technical field
The utility model belongs to field of experiment equipment, and in particular to a kind of experiment of oil resistant, thermostabilization experiment or other oil baths
Thermostatical oil bath used in environmental experiment.
Background technique
Oil resistant experiment and thermostabilization experiment be high molecular material design R&D process in be often in contact with oil bath experiment,
The experimental facilities structure that each material enterprise uses is all similar.Oil resistant experiment usually dumbbell plate, which is put into, fills experiment oil
Beaker in, then beaker be put into setting experimental temperature baking oven in complete.Thermostabilization experiment is generally used for test PVC material
Thermal stability, sample tube is placed in and fills glycerol, is heated to 200 DEG C of beaker, is stirred in beaker bottom using stirrer paddle
Mix device heating.Currently, individual businesses, which will use the ancillary equipments such as the oil bath pan cooperation beaker that purchase comes, reaches raising experimental precision
Effect.But beaker is easily broken the irrationality that more or less there are some designs with oil bath pan heating, so as to experiment
Effect improves limited.
Existing experimental facilities can satisfy research and development laboratory at present substantially and examine the requirement in laboratory.But along with research and development
And the quickening of progress is examined, the accuracy and reproducibility test to oil resistant and thermostabilization require to improve, and existing this kind of experiment is set
It is standby to be difficult to meet the requirements.It is emphasis to experimental facilities high-precision and efficient demand, it is therefore desirable to which designing one kind can
Reach high-precision, the novel experimental equipment of high efficiency demand.
Summary of the invention
The purpose of the utility model is to provide one kind can be improved experimental data accuracy, reduces repetition test frequency, mentions
The thermostatical oil bath of high working efficiency.
In order to achieve the above objectives, the technical solution adopted in the utility model is:
A kind of thermostatical oil bath, for carrying out oil bath experiment to experiment sample, the thermostatical oil bath includes that splendid attire is thermally conductive
The oil drum of oil contains the lubricating cup of experimental oil, the heater for heating the conduction oil, for promoting the conduction oil flowing
Blender, the sensor and control circuit for detecting the thermally conductive oil temperature and the experimental oil temperature respectively;The lubricating cup is set
It is placed in the oil drum and at least part of the lubricating cup immerses in the conduction oil, the control circuit adds with described respectively
Hot device, the blender, the sensor are connected, and the experiment sample hangs and is infiltrated in the experimental oil.
The oil drum includes the staving of double-layer structure, is filled with insulating in the double-layer structure.
The bung hole of the oil drum is provided with bung, and the through-hole to match with the lubricating cup is offered on the bung, described
Lubricating cup is hung in the through-hole, and the rim of a cup of the lubricating cup is provided with outwardly extending flange, and is provided with dustproof cover.
The lubricating cup includes cup body, and the step structure comprising step surface, the step surface are formed on the wall of cup of the cup body
On be erected with inner cover, it is described in cover the link for being used to hang the experiment sample equipped with several.
The heater is set to the bottom of the oil drum, and the blender is obliquely installed in the conduction oil.
The sensor includes being set at a certain distance from the bucket wall apart from the oil drum and being in contact with the conduction oil
Conduction oil temperature probe, the experimental oil temperature probe that is set to the lubricating cup center and is contacted with the experimental oil.
The blender includes decelerating motor, the stirrer paddle on the output shaft for being installed on the decelerating motor.
The control circuit includes:
The power supply line being connected with external power supply;
It is connected with the power supply line, for controlling the blender starting work or stopping working, and in the stirring
The blender control module of status signal is issued when machine steady operation;
It is connected respectively with the power supply line, the blender control module, the sensor, for being based on the state
Signal controls the heater starting work and is later than the blender, stops working earlier than the blender, or in the biography
Sensor detects that controlling the heater when the thermally conductive oil temperature or the experimental oil temperature are more than corresponding setting value stops work
The heater control module of work.
The blender control module includes being connected with the power supply line and the blender and capable of exporting the shape
The blender controller of state signal;
The heater control module includes the first intermediate relay, the second intermediate relay, first contactor, heater
Controller is connected with the sensor and detects that the thermally conductive oil temperature or the experimental oil temperature are super in the sensor
The temp controlled meter of output oil temperature detection signal when crossing corresponding setting value;
The coil of first intermediate relay is connected with the power supply line, the coil of second intermediate relay with
The temp controlled meter is connected and receives the oil temperature detection signal, the normally opened node of first intermediate relay, described second
The normally closed node of intermediate relay and the coil of the first contactor be connected in series and be connected with the blender controller and
The status signal is received, normally opened node, the heater controller, the heater of the first contactor are connected in series simultaneously
It is connected with the power supply line.
The thermostatical oil bath further includes for hanging setting sample rack and/or being set to the oil drum bottom for the experiment sample
The oil drain pan in portion.
Since above-mentioned technical proposal is used, the utility model has the advantage that the utility model compared with prior art
It can be improved experimental data accuracy, reduce and repeat test frequency, improve working efficiency, adapt to test oil bath higher wants
It asks.
Detailed description of the invention
Attached drawing 1 is the partial structure diagram of the thermostatical oil bath of the utility model.
Attached drawing 2 is the enlarged diagram of lubricating cup in the thermostatical oil bath of the utility model.
Attached drawing 3 is the schematic diagram of separation structure in the middle part of the thermostatical oil bath of the utility model.
Attached drawing 4 is the partial circuit diagram of control circuit in the thermostatical oil bath of the utility model.
Attached drawing 5 is another part circuit diagram of control circuit in the thermostatical oil bath of the utility model.
In the figures above: 1, oil drum;2, lubricating cup;3, conduction oil;4, experimental oil;5, bung;6, decelerating motor;7, agitating paddle
Leaf;8, heater;9, inner cover;10, conduction oil temperature probe;11, experimental oil temperature probe;12, bracket;13, link;14, prevent
Dirt lid;15, oil drain pan;16, sample rack is set;17, experiment sample.
Specific embodiment
Embodiment shown in reference to the accompanying drawing is further described the utility model.
Embodiment one: as shown in attached drawing 1 to attached drawing 3, one kind testing constant temperature oil bath for carrying out oil bath to experiment sample 17
Device, including oil drum 1, lubricating cup 2, heater 8, blender, sensor and control circuit.
Oil drum 1 is cylindrical, is inside loaded with conduction oil 3.Oil drum 1 includes staving, and the bucket of oil drum 1 is formed on the top of staving
Mouthful.Staving is by stainless steel plate through the hollow staving for rolling the double-layer structure being welded, and double-layer structure is interior to be filled with heat-insulated guarantor
Adiabator and form insulating, so as to reduce oil-bath temperature losses.Heater 8 uses electric heater, and setting exists
1 bottom of oil drum, for heating the conduction oil 3 in oil drum 1.Blender is obliquely installed in conduction oil 3, for promoting conduction oil 3
Flowing.Blender includes decelerating motor 6, the stirrer paddle 7 on the output shaft for being installed on decelerating motor 6.Decelerating motor 6 can make
With lower-powered silent reducing motor 6, speed ratio (1:25).Blender is mounted on the oil of thermostatical oil bath with certain tilt angle
In bucket 1, stirrer paddle 7 allows about 3 conduction oil to roll circulation and left and right circulation, ensure that peripheral conduction oil 3 from upper
It arrives down, mobility from left to right.
Lubricating cup 2 is for containing experimental oil 4 comprising cup body, formed on the wall of cup of cup body include step surface step structure.
Lubricating cup 2 is removable installed in oil drum 1, and at least part of lubricating cup 2 immerses in conduction oil 3, and not with the bucket wall of oil drum 1 and
The contact of bucket bottom is that experimental oil 4 heats so as to pass through conduction pattern using conduction oil 3, flows outside oil bath, and internal stationary is real
It tests and uses oil, guarantee that temperature is stablized, solve the problems, such as that baking oven heating or rotor heat transport are unstable, effectively improve experimental precision.Lubricating cup 2
Detachably, then switch with can be convenient.Inner cover 9 is erected on 2 step surface of lubricating cup, inner cover 9 is equipped with several for hanging reality
The link 13 of sample 17 is tested, and the handle taken is set, so that experiment sample 17 be hung and be infiltrated in experimental oil 4.It is logical
Link 13 is crossed, multiple groups experiment sample 17 can be tested simultaneously, improve conventional efficient.The Step-edge Junction of inner cover 9 and lubricating cup 2
Structure can solve experiment sample 17 and be placed in lubricating cup 2 the problem of needing to keep height same and complete wetting.
In order to be arranged lubricating cup 2 in oil drum 1, bung 5 is set in the bung hole of oil drum 1 in the present embodiment, and on bung 5
The through-hole to match with lubricating cup 2 is opened up, so that lubricating cup 2 be hung in through-hole.And lubricating cup 2 is then outwardly extending in rim of a cup setting
Flange, and it is provided with dustproof cover 14.By the flange of bung 5 and dustproof cover 14 and lubricating cup 2, contaminated product can be prevented, that is, is prevented
Experimental oil 4 is mixed into conduction oil 3, realizes that conduction oil 3 and experimental oil 4 separate.
In this programme by the way of hanging lubricating cup 2, the internal stent that is arranged in oil drum 1 can be used also to support oil
Cup 2, but its flowing that may influence conduction oil 3, therefore it is not recommended that using.Bung 5 uses whole high-intensitive stainless steel
Metal plate production, guarantees that the vibration of blender does not influence complete equipment, and can support lubricating cup 2 and the wherein weight of experimental oil 4
Amount.The outer diameter precision of the size and lubricating cup 2 of placing the through-hole of lubricating cup 2 thereon is controlled when processing bung 5, also to guarantee to make
The shaking for not generating lubricating cup 2 in avoids the actual effect for influencing to test.
For sensor for detecting 3 temperature of conduction oil and 4 temperature of experimental oil respectively, it includes the bucket being set to apart from oil drum 1
The conduction oil temperature probe 10 that is in contact at a certain distance from wall and with conduction oil 3 is set to 2 center of lubricating cup and connects with experimental oil 4
The experimental oil temperature probe 11 of touching.Usually according on the basis of the depth of conduction oil 3 or experimental oil 4, corresponding temperature probe is arranged
Near 0.618 times of position of pasta total height.Sensor can be installed by hang.
In addition, the thermostatical oil bath can also include for hanging setting sample rack 16 and/or being set to oil for experiment sample 17
The oil drain pan 15 of 1 bottom of bucket, so as to conveniently hang experiment sample 17 and the processing to sample after experiment.And the present embodiment
Middle setting bracket 12 is for hanging setting sensor and blender.
The size of each part of the above thermostatical oil bath can according to need customization, the volume of usual experimental oil 4 and conduction oil 3
Than about 1:4.
Control circuit is connected with heater 8, blender, sensor respectively.As shown in figures 4 and 5, control circuit
Including power supply line, blender control module and heater control module.
Power supply line electric energy needed for external power supply is connected to provide comprising phase line and zero curve.
Blender control module is connected in power supply line, is also connected with blender, for controlling blender starting work
Or it stops working, and issue status signal in blender steady operation.Blender control module includes and power supply line and stirring
Machine is connected and is capable of the blender controller of output status signal.
Heater control module is connected with power supply line, blender control module, sensor respectively, it is used to be based on state
Signal control heater 8 starts work and is later than blender, stops working earlier than blender, or detects conduction oil in sensor
Control heater 8 stops working when 3 temperature or the temperature of experimental oil 4 are more than corresponding setting value.Heater control module includes
First intermediate relay 2KA1, the second intermediate relay 2KA2, first contactor 1KM2, heater controller and temp controlled meter.Its
Middle temp controlled meter is connected with sensor and detects the temperature of conduction oil 3 in sensor or the temperature of experimental oil 4 is more than corresponding to set
Oil temperature is exported when definite value detects signal.Since sensor includes two temperature probes, respectively conduction oil temperature probe 10 and reality
Oily temperature probe 11 is tested, therefore they respectively correspond and are provided with temp controlled meter, respectively conduction oil temp controlled meter and experimental oil temp controlled meter.The
The coil of one intermediate relay 2KA1 is connected with power supply line, and the coil of the second intermediate relay 2KA2 is connected simultaneously with temp controlled meter
Receive oil temperature detect signal, the normally opened node of the first intermediate relay 2KA1, the second intermediate relay 2KA2 normally closed node and
The coil of first contactor 1KM2 is connected in series and is connected and reception state signal with blender controller, first contactor 1KM2
Normally opened node, heater controller, heater be connected in series and be connected with power supply line.
In addition, control circuit can also include second contactor 1KM1 and multiple indicator lights.Second contactor 1KM1's
Coil is connected with power supply line, and its normally opened contact is then arranged on the power supply line in front of power supply line blender controller.Instruction
Lamp is included connection power work indicator light on the power line, is connected with blender controller and is lighted based on status signal
Work light, the heating work indicator light being connected with heater 8 etc. are stirred, the simultaneously base that is connected with temp controlled meter can also be set
In the overtemperature alarm that oil temperature detects signal and alarms.
In the thermostatical oil bath course of work, the starting of blender need to cooperate heater 8 and sensor, can use oncontacting
Point solid-state relay and heating PID fuzzy control are realized and stablize, uniformly, accurately heat.It must before starting heater 8 works
Blender need first be started, only blender could 8 power supply of turn on automatically heater after working normally.As blender breaks down
It has no idea to start computer heating control after alarm.In heating process, sensor one detects overtemperature (such as larger than set temperature 3
DEG C), it is switched off 8 power supply of heater and stops heating, and issue alarm signal, at this point, blender need to continue to operate normally, prevent
Conduction oil 3 generates coking on heater 8 after overtemperature.Heating is automatically cut off if blender failure in the process of running
8 power supply of device stops heating.
Specific in above-mentioned control circuit, when connecting external power supply and after connecting switch 1Q1, second contactor 1KM1's
Coil obtains electric, so that its normally opened contact 1KM1 is closed, power work indicator light lighted, and turns off the switch 1Q2, blender controller control
The decelerating motor 6 of blender processed starts work.After 6 the operation is stable of decelerating motor, blender controller output status signal, and
Light stirring work light.Meanwhile after closure switch 2QA1, the coil of the first intermediate relay 2KA1 obtain it is electric so that
The normally opened node of one intermediate relay 2KA1 is closed, thus the normally opened node of the first intermediate relay 2KA1, the second intermediate relay
The series via that the normally closed node of device 2KA2 and the coil of first contactor 1KM2 are constituted obtains status signal, so that the first contact
The normally opened node of device 1KM2 is closed, then heater controller obtains electric and controls the start-up operation of heater 8.Two thermometrics of sensor
Probe detects the temperature of conduction oil 3 and experimental oil 4 respectively, when the temperature detected is more than the setting value in corresponding temp controlled meter,
Temp controlled meter exports oil temperature and detects signal.Overtemperature alarm is alarmed at this time, and the coil of the second intermediate relay AKA2 obtains
Electricity, so that its normally closed node 2KA2 is disconnected, then the coil losing electricity of first contactor 1KM2, to disconnect its normally opened node
1KM2 makes heater 8 stop working, and blender works on.
The above embodiments are only for explaining the technical ideas and features of the present invention, and its object is to allow be familiar with technique
Personage can understand the content of the utility model and implement accordingly, do not limit the protection scope of the present invention.
All equivalent change or modifications according to made by the spirit of the present invention essence, should all cover the protection scope of the utility model it
It is interior.
Claims (10)
1. a kind of thermostatical oil bath, for carrying out oil bath experiment to experiment sample, it is characterised in that: the thermostatical oil bath includes
The oil drum of conduction oil is contained, the lubricating cup of experimental oil is contained, is the heater for heating the conduction oil, described thermally conductive for promoting
The dynamic blender of oil stream, the sensor and control circuit for detecting the thermally conductive oil temperature and the experimental oil temperature respectively;Institute
State that lubricating cup is set in the oil drum and at least part of the lubricating cup immerses in the conduction oil, the control circuit difference
It is connected with the heater, the blender, the sensor, the experiment sample hangs and is infiltrated on the experimental oil
In.
2. thermostatical oil bath according to claim 1, it is characterised in that: the oil drum includes the staving of double-layer structure, institute
It states in double-layer structure filled with insulating.
3. thermostatical oil bath according to claim 1, it is characterised in that: the bung hole of the oil drum is provided with bung, described
The through-hole to match with the lubricating cup is offered on bung, the lubricating cup is hung in the through-hole, and the rim of a cup of the lubricating cup is set
It is equipped with outwardly extending flange, and is provided with dustproof cover.
4. thermostatical oil bath according to claim 1, it is characterised in that: the lubricating cup includes cup body, the cup of the cup body
The step structure comprising step surface is formed on wall, inner cover is erected on the step surface, and interior cover is used for equipped with several
Hang the link of the experiment sample.
5. thermostatical oil bath according to claim 1, it is characterised in that: the heater is set to the bottom of the oil drum
Portion, the blender are obliquely installed in the conduction oil.
6. thermostatical oil bath according to claim 1, it is characterised in that: the sensor includes being set to apart from the oil
Bucket bucket wall at a certain distance from and be in contact with the conduction oil conduction oil temperature probe, be set to the lubricating cup center and with
The experimental oil temperature probe of the experimental oil contact.
7. thermostatical oil bath according to claim 1, it is characterised in that: the blender includes decelerating motor, is installed on
Stirrer paddle on the output shaft of the decelerating motor.
8. thermostatical oil bath according to claim 1, it is characterised in that: the control circuit includes:
The power supply line being connected with external power supply;
It is connected with the power supply line, for controlling the blender starting work or stopping working, and it is steady in the blender
The blender control module of status signal is issued when working surely;
It is connected respectively with the power supply line, the blender control module, the sensor, for being based on the status signal
It controls the heater starting work be later than the blender, stop working earlier than the blender, or in the sensor
It detects and controls what the heater stopped working when the thermally conductive oil temperature or the experimental oil temperature are more than corresponding setting value
Heater control module.
9. thermostatical oil bath according to claim 8, it is characterised in that: the blender control module includes and the electricity
Source line is connected with the blender and can export the blender controller of the status signal;
The heater control module includes the first intermediate relay, the second intermediate relay, first contactor, heater control
Device is connected with the sensor and detects that the thermally conductive oil temperature or the experimental oil temperature are more than pair in the sensor
The temp controlled meter of output oil temperature detection signal when answering setting value;
The coil of first intermediate relay is connected with the power supply line, the coil of second intermediate relay with it is described
Temp controlled meter is connected and receives oil temperature detection signal, the normally opened node of first intermediate relay, among described second
The normally closed node of relay and the coil of the first contactor are connected in series and are connected with the blender controller and receive
The status signal, normally opened node, the heater controller, the heater of the first contactor be connected in series and with institute
Power supply line is stated to be connected.
10. thermostatical oil bath according to claim 1, it is characterised in that: the thermostatical oil bath further includes for hanging
The oil drain pan of the experiment sample set sample rack and/or be set to the oil drum bottom.
Priority Applications (1)
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CN201821447652.XU CN208878618U (en) | 2018-09-05 | 2018-09-05 | Thermostatical oil bath |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201821447652.XU CN208878618U (en) | 2018-09-05 | 2018-09-05 | Thermostatical oil bath |
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CN208878618U true CN208878618U (en) | 2019-05-21 |
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ID=66511187
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109078665A (en) * | 2018-09-05 | 2018-12-25 | 江苏德威新材料股份有限公司 | Thermostatical oil bath |
CN113274764A (en) * | 2021-06-18 | 2021-08-20 | 中触媒新材料股份有限公司 | Liquid phase adsorption separation system and temperature control process method thereof |
-
2018
- 2018-09-05 CN CN201821447652.XU patent/CN208878618U/en active Active
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109078665A (en) * | 2018-09-05 | 2018-12-25 | 江苏德威新材料股份有限公司 | Thermostatical oil bath |
CN113274764A (en) * | 2021-06-18 | 2021-08-20 | 中触媒新材料股份有限公司 | Liquid phase adsorption separation system and temperature control process method thereof |
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