CN208878618U - Thermostatical oil bath - Google Patents

Thermostatical oil bath Download PDF

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Publication number
CN208878618U
CN208878618U CN201821447652.XU CN201821447652U CN208878618U CN 208878618 U CN208878618 U CN 208878618U CN 201821447652 U CN201821447652 U CN 201821447652U CN 208878618 U CN208878618 U CN 208878618U
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Prior art keywords
oil
blender
heater
thermostatical
experimental
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CN201821447652.XU
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张玉平
徐建岐
栾珊珊
王兴宁
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JIANGSU DEWEI ADVANCED MATERIALS CO Ltd
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JIANGSU DEWEI ADVANCED MATERIALS CO Ltd
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Abstract

The utility model relates to a kind of thermostatical oil baths, for carrying out oil bath experiment to experiment sample, thermostatical oil bath includes the oil drum for containing conduction oil, the lubricating cup for containing experimental oil, the heater for heating conduction oil, the blender for promoting conduction oil to flow, the sensor and control circuit for detecting thermally conductive oil temperature and experimental oil temperature respectively;Lubricating cup is set in oil drum and at least part of lubricating cup immerses in conduction oil, and control circuit is connected with heater, blender, sensor respectively, and experiment sample hangs and is infiltrated in experimental oil.The utility model can be improved experimental data accuracy, reduce repetition test frequency, improves working efficiency, adapts to the requirements at the higher level tested to oil bath.

Description

Thermostatical oil bath
Technical field
The utility model belongs to field of experiment equipment, and in particular to a kind of experiment of oil resistant, thermostabilization experiment or other oil baths Thermostatical oil bath used in environmental experiment.
Background technique
Oil resistant experiment and thermostabilization experiment be high molecular material design R&D process in be often in contact with oil bath experiment, The experimental facilities structure that each material enterprise uses is all similar.Oil resistant experiment usually dumbbell plate, which is put into, fills experiment oil Beaker in, then beaker be put into setting experimental temperature baking oven in complete.Thermostabilization experiment is generally used for test PVC material Thermal stability, sample tube is placed in and fills glycerol, is heated to 200 DEG C of beaker, is stirred in beaker bottom using stirrer paddle Mix device heating.Currently, individual businesses, which will use the ancillary equipments such as the oil bath pan cooperation beaker that purchase comes, reaches raising experimental precision Effect.But beaker is easily broken the irrationality that more or less there are some designs with oil bath pan heating, so as to experiment Effect improves limited.
Existing experimental facilities can satisfy research and development laboratory at present substantially and examine the requirement in laboratory.But along with research and development And the quickening of progress is examined, the accuracy and reproducibility test to oil resistant and thermostabilization require to improve, and existing this kind of experiment is set It is standby to be difficult to meet the requirements.It is emphasis to experimental facilities high-precision and efficient demand, it is therefore desirable to which designing one kind can Reach high-precision, the novel experimental equipment of high efficiency demand.
Summary of the invention
The purpose of the utility model is to provide one kind can be improved experimental data accuracy, reduces repetition test frequency, mentions The thermostatical oil bath of high working efficiency.
In order to achieve the above objectives, the technical solution adopted in the utility model is:
A kind of thermostatical oil bath, for carrying out oil bath experiment to experiment sample, the thermostatical oil bath includes that splendid attire is thermally conductive The oil drum of oil contains the lubricating cup of experimental oil, the heater for heating the conduction oil, for promoting the conduction oil flowing Blender, the sensor and control circuit for detecting the thermally conductive oil temperature and the experimental oil temperature respectively;The lubricating cup is set It is placed in the oil drum and at least part of the lubricating cup immerses in the conduction oil, the control circuit adds with described respectively Hot device, the blender, the sensor are connected, and the experiment sample hangs and is infiltrated in the experimental oil.
The oil drum includes the staving of double-layer structure, is filled with insulating in the double-layer structure.
The bung hole of the oil drum is provided with bung, and the through-hole to match with the lubricating cup is offered on the bung, described Lubricating cup is hung in the through-hole, and the rim of a cup of the lubricating cup is provided with outwardly extending flange, and is provided with dustproof cover.
The lubricating cup includes cup body, and the step structure comprising step surface, the step surface are formed on the wall of cup of the cup body On be erected with inner cover, it is described in cover the link for being used to hang the experiment sample equipped with several.
The heater is set to the bottom of the oil drum, and the blender is obliquely installed in the conduction oil.
The sensor includes being set at a certain distance from the bucket wall apart from the oil drum and being in contact with the conduction oil Conduction oil temperature probe, the experimental oil temperature probe that is set to the lubricating cup center and is contacted with the experimental oil.
The blender includes decelerating motor, the stirrer paddle on the output shaft for being installed on the decelerating motor.
The control circuit includes:
The power supply line being connected with external power supply;
It is connected with the power supply line, for controlling the blender starting work or stopping working, and in the stirring The blender control module of status signal is issued when machine steady operation;
It is connected respectively with the power supply line, the blender control module, the sensor, for being based on the state Signal controls the heater starting work and is later than the blender, stops working earlier than the blender, or in the biography Sensor detects that controlling the heater when the thermally conductive oil temperature or the experimental oil temperature are more than corresponding setting value stops work The heater control module of work.
The blender control module includes being connected with the power supply line and the blender and capable of exporting the shape The blender controller of state signal;
The heater control module includes the first intermediate relay, the second intermediate relay, first contactor, heater Controller is connected with the sensor and detects that the thermally conductive oil temperature or the experimental oil temperature are super in the sensor The temp controlled meter of output oil temperature detection signal when crossing corresponding setting value;
The coil of first intermediate relay is connected with the power supply line, the coil of second intermediate relay with The temp controlled meter is connected and receives the oil temperature detection signal, the normally opened node of first intermediate relay, described second The normally closed node of intermediate relay and the coil of the first contactor be connected in series and be connected with the blender controller and The status signal is received, normally opened node, the heater controller, the heater of the first contactor are connected in series simultaneously It is connected with the power supply line.
The thermostatical oil bath further includes for hanging setting sample rack and/or being set to the oil drum bottom for the experiment sample The oil drain pan in portion.
Since above-mentioned technical proposal is used, the utility model has the advantage that the utility model compared with prior art It can be improved experimental data accuracy, reduce and repeat test frequency, improve working efficiency, adapt to test oil bath higher wants It asks.
Detailed description of the invention
Attached drawing 1 is the partial structure diagram of the thermostatical oil bath of the utility model.
Attached drawing 2 is the enlarged diagram of lubricating cup in the thermostatical oil bath of the utility model.
Attached drawing 3 is the schematic diagram of separation structure in the middle part of the thermostatical oil bath of the utility model.
Attached drawing 4 is the partial circuit diagram of control circuit in the thermostatical oil bath of the utility model.
Attached drawing 5 is another part circuit diagram of control circuit in the thermostatical oil bath of the utility model.
In the figures above: 1, oil drum;2, lubricating cup;3, conduction oil;4, experimental oil;5, bung;6, decelerating motor;7, agitating paddle Leaf;8, heater;9, inner cover;10, conduction oil temperature probe;11, experimental oil temperature probe;12, bracket;13, link;14, prevent Dirt lid;15, oil drain pan;16, sample rack is set;17, experiment sample.
Specific embodiment
Embodiment shown in reference to the accompanying drawing is further described the utility model.
Embodiment one: as shown in attached drawing 1 to attached drawing 3, one kind testing constant temperature oil bath for carrying out oil bath to experiment sample 17 Device, including oil drum 1, lubricating cup 2, heater 8, blender, sensor and control circuit.
Oil drum 1 is cylindrical, is inside loaded with conduction oil 3.Oil drum 1 includes staving, and the bucket of oil drum 1 is formed on the top of staving Mouthful.Staving is by stainless steel plate through the hollow staving for rolling the double-layer structure being welded, and double-layer structure is interior to be filled with heat-insulated guarantor Adiabator and form insulating, so as to reduce oil-bath temperature losses.Heater 8 uses electric heater, and setting exists 1 bottom of oil drum, for heating the conduction oil 3 in oil drum 1.Blender is obliquely installed in conduction oil 3, for promoting conduction oil 3 Flowing.Blender includes decelerating motor 6, the stirrer paddle 7 on the output shaft for being installed on decelerating motor 6.Decelerating motor 6 can make With lower-powered silent reducing motor 6, speed ratio (1:25).Blender is mounted on the oil of thermostatical oil bath with certain tilt angle In bucket 1, stirrer paddle 7 allows about 3 conduction oil to roll circulation and left and right circulation, ensure that peripheral conduction oil 3 from upper It arrives down, mobility from left to right.
Lubricating cup 2 is for containing experimental oil 4 comprising cup body, formed on the wall of cup of cup body include step surface step structure. Lubricating cup 2 is removable installed in oil drum 1, and at least part of lubricating cup 2 immerses in conduction oil 3, and not with the bucket wall of oil drum 1 and The contact of bucket bottom is that experimental oil 4 heats so as to pass through conduction pattern using conduction oil 3, flows outside oil bath, and internal stationary is real It tests and uses oil, guarantee that temperature is stablized, solve the problems, such as that baking oven heating or rotor heat transport are unstable, effectively improve experimental precision.Lubricating cup 2 Detachably, then switch with can be convenient.Inner cover 9 is erected on 2 step surface of lubricating cup, inner cover 9 is equipped with several for hanging reality The link 13 of sample 17 is tested, and the handle taken is set, so that experiment sample 17 be hung and be infiltrated in experimental oil 4.It is logical Link 13 is crossed, multiple groups experiment sample 17 can be tested simultaneously, improve conventional efficient.The Step-edge Junction of inner cover 9 and lubricating cup 2 Structure can solve experiment sample 17 and be placed in lubricating cup 2 the problem of needing to keep height same and complete wetting.
In order to be arranged lubricating cup 2 in oil drum 1, bung 5 is set in the bung hole of oil drum 1 in the present embodiment, and on bung 5 The through-hole to match with lubricating cup 2 is opened up, so that lubricating cup 2 be hung in through-hole.And lubricating cup 2 is then outwardly extending in rim of a cup setting Flange, and it is provided with dustproof cover 14.By the flange of bung 5 and dustproof cover 14 and lubricating cup 2, contaminated product can be prevented, that is, is prevented Experimental oil 4 is mixed into conduction oil 3, realizes that conduction oil 3 and experimental oil 4 separate.
In this programme by the way of hanging lubricating cup 2, the internal stent that is arranged in oil drum 1 can be used also to support oil Cup 2, but its flowing that may influence conduction oil 3, therefore it is not recommended that using.Bung 5 uses whole high-intensitive stainless steel Metal plate production, guarantees that the vibration of blender does not influence complete equipment, and can support lubricating cup 2 and the wherein weight of experimental oil 4 Amount.The outer diameter precision of the size and lubricating cup 2 of placing the through-hole of lubricating cup 2 thereon is controlled when processing bung 5, also to guarantee to make The shaking for not generating lubricating cup 2 in avoids the actual effect for influencing to test.
For sensor for detecting 3 temperature of conduction oil and 4 temperature of experimental oil respectively, it includes the bucket being set to apart from oil drum 1 The conduction oil temperature probe 10 that is in contact at a certain distance from wall and with conduction oil 3 is set to 2 center of lubricating cup and connects with experimental oil 4 The experimental oil temperature probe 11 of touching.Usually according on the basis of the depth of conduction oil 3 or experimental oil 4, corresponding temperature probe is arranged Near 0.618 times of position of pasta total height.Sensor can be installed by hang.
In addition, the thermostatical oil bath can also include for hanging setting sample rack 16 and/or being set to oil for experiment sample 17 The oil drain pan 15 of 1 bottom of bucket, so as to conveniently hang experiment sample 17 and the processing to sample after experiment.And the present embodiment Middle setting bracket 12 is for hanging setting sensor and blender.
The size of each part of the above thermostatical oil bath can according to need customization, the volume of usual experimental oil 4 and conduction oil 3 Than about 1:4.
Control circuit is connected with heater 8, blender, sensor respectively.As shown in figures 4 and 5, control circuit Including power supply line, blender control module and heater control module.
Power supply line electric energy needed for external power supply is connected to provide comprising phase line and zero curve.
Blender control module is connected in power supply line, is also connected with blender, for controlling blender starting work Or it stops working, and issue status signal in blender steady operation.Blender control module includes and power supply line and stirring Machine is connected and is capable of the blender controller of output status signal.
Heater control module is connected with power supply line, blender control module, sensor respectively, it is used to be based on state Signal control heater 8 starts work and is later than blender, stops working earlier than blender, or detects conduction oil in sensor Control heater 8 stops working when 3 temperature or the temperature of experimental oil 4 are more than corresponding setting value.Heater control module includes First intermediate relay 2KA1, the second intermediate relay 2KA2, first contactor 1KM2, heater controller and temp controlled meter.Its Middle temp controlled meter is connected with sensor and detects the temperature of conduction oil 3 in sensor or the temperature of experimental oil 4 is more than corresponding to set Oil temperature is exported when definite value detects signal.Since sensor includes two temperature probes, respectively conduction oil temperature probe 10 and reality Oily temperature probe 11 is tested, therefore they respectively correspond and are provided with temp controlled meter, respectively conduction oil temp controlled meter and experimental oil temp controlled meter.The The coil of one intermediate relay 2KA1 is connected with power supply line, and the coil of the second intermediate relay 2KA2 is connected simultaneously with temp controlled meter Receive oil temperature detect signal, the normally opened node of the first intermediate relay 2KA1, the second intermediate relay 2KA2 normally closed node and The coil of first contactor 1KM2 is connected in series and is connected and reception state signal with blender controller, first contactor 1KM2 Normally opened node, heater controller, heater be connected in series and be connected with power supply line.
In addition, control circuit can also include second contactor 1KM1 and multiple indicator lights.Second contactor 1KM1's Coil is connected with power supply line, and its normally opened contact is then arranged on the power supply line in front of power supply line blender controller.Instruction Lamp is included connection power work indicator light on the power line, is connected with blender controller and is lighted based on status signal Work light, the heating work indicator light being connected with heater 8 etc. are stirred, the simultaneously base that is connected with temp controlled meter can also be set In the overtemperature alarm that oil temperature detects signal and alarms.
In the thermostatical oil bath course of work, the starting of blender need to cooperate heater 8 and sensor, can use oncontacting Point solid-state relay and heating PID fuzzy control are realized and stablize, uniformly, accurately heat.It must before starting heater 8 works Blender need first be started, only blender could 8 power supply of turn on automatically heater after working normally.As blender breaks down It has no idea to start computer heating control after alarm.In heating process, sensor one detects overtemperature (such as larger than set temperature 3 DEG C), it is switched off 8 power supply of heater and stops heating, and issue alarm signal, at this point, blender need to continue to operate normally, prevent Conduction oil 3 generates coking on heater 8 after overtemperature.Heating is automatically cut off if blender failure in the process of running 8 power supply of device stops heating.
Specific in above-mentioned control circuit, when connecting external power supply and after connecting switch 1Q1, second contactor 1KM1's Coil obtains electric, so that its normally opened contact 1KM1 is closed, power work indicator light lighted, and turns off the switch 1Q2, blender controller control The decelerating motor 6 of blender processed starts work.After 6 the operation is stable of decelerating motor, blender controller output status signal, and Light stirring work light.Meanwhile after closure switch 2QA1, the coil of the first intermediate relay 2KA1 obtain it is electric so that The normally opened node of one intermediate relay 2KA1 is closed, thus the normally opened node of the first intermediate relay 2KA1, the second intermediate relay The series via that the normally closed node of device 2KA2 and the coil of first contactor 1KM2 are constituted obtains status signal, so that the first contact The normally opened node of device 1KM2 is closed, then heater controller obtains electric and controls the start-up operation of heater 8.Two thermometrics of sensor Probe detects the temperature of conduction oil 3 and experimental oil 4 respectively, when the temperature detected is more than the setting value in corresponding temp controlled meter, Temp controlled meter exports oil temperature and detects signal.Overtemperature alarm is alarmed at this time, and the coil of the second intermediate relay AKA2 obtains Electricity, so that its normally closed node 2KA2 is disconnected, then the coil losing electricity of first contactor 1KM2, to disconnect its normally opened node 1KM2 makes heater 8 stop working, and blender works on.
The above embodiments are only for explaining the technical ideas and features of the present invention, and its object is to allow be familiar with technique Personage can understand the content of the utility model and implement accordingly, do not limit the protection scope of the present invention. All equivalent change or modifications according to made by the spirit of the present invention essence, should all cover the protection scope of the utility model it It is interior.

Claims (10)

1. a kind of thermostatical oil bath, for carrying out oil bath experiment to experiment sample, it is characterised in that: the thermostatical oil bath includes The oil drum of conduction oil is contained, the lubricating cup of experimental oil is contained, is the heater for heating the conduction oil, described thermally conductive for promoting The dynamic blender of oil stream, the sensor and control circuit for detecting the thermally conductive oil temperature and the experimental oil temperature respectively;Institute State that lubricating cup is set in the oil drum and at least part of the lubricating cup immerses in the conduction oil, the control circuit difference It is connected with the heater, the blender, the sensor, the experiment sample hangs and is infiltrated on the experimental oil In.
2. thermostatical oil bath according to claim 1, it is characterised in that: the oil drum includes the staving of double-layer structure, institute It states in double-layer structure filled with insulating.
3. thermostatical oil bath according to claim 1, it is characterised in that: the bung hole of the oil drum is provided with bung, described The through-hole to match with the lubricating cup is offered on bung, the lubricating cup is hung in the through-hole, and the rim of a cup of the lubricating cup is set It is equipped with outwardly extending flange, and is provided with dustproof cover.
4. thermostatical oil bath according to claim 1, it is characterised in that: the lubricating cup includes cup body, the cup of the cup body The step structure comprising step surface is formed on wall, inner cover is erected on the step surface, and interior cover is used for equipped with several Hang the link of the experiment sample.
5. thermostatical oil bath according to claim 1, it is characterised in that: the heater is set to the bottom of the oil drum Portion, the blender are obliquely installed in the conduction oil.
6. thermostatical oil bath according to claim 1, it is characterised in that: the sensor includes being set to apart from the oil Bucket bucket wall at a certain distance from and be in contact with the conduction oil conduction oil temperature probe, be set to the lubricating cup center and with The experimental oil temperature probe of the experimental oil contact.
7. thermostatical oil bath according to claim 1, it is characterised in that: the blender includes decelerating motor, is installed on Stirrer paddle on the output shaft of the decelerating motor.
8. thermostatical oil bath according to claim 1, it is characterised in that: the control circuit includes:
The power supply line being connected with external power supply;
It is connected with the power supply line, for controlling the blender starting work or stopping working, and it is steady in the blender The blender control module of status signal is issued when working surely;
It is connected respectively with the power supply line, the blender control module, the sensor, for being based on the status signal It controls the heater starting work be later than the blender, stop working earlier than the blender, or in the sensor It detects and controls what the heater stopped working when the thermally conductive oil temperature or the experimental oil temperature are more than corresponding setting value Heater control module.
9. thermostatical oil bath according to claim 8, it is characterised in that: the blender control module includes and the electricity Source line is connected with the blender and can export the blender controller of the status signal;
The heater control module includes the first intermediate relay, the second intermediate relay, first contactor, heater control Device is connected with the sensor and detects that the thermally conductive oil temperature or the experimental oil temperature are more than pair in the sensor The temp controlled meter of output oil temperature detection signal when answering setting value;
The coil of first intermediate relay is connected with the power supply line, the coil of second intermediate relay with it is described Temp controlled meter is connected and receives oil temperature detection signal, the normally opened node of first intermediate relay, among described second The normally closed node of relay and the coil of the first contactor are connected in series and are connected with the blender controller and receive The status signal, normally opened node, the heater controller, the heater of the first contactor be connected in series and with institute Power supply line is stated to be connected.
10. thermostatical oil bath according to claim 1, it is characterised in that: the thermostatical oil bath further includes for hanging The oil drain pan of the experiment sample set sample rack and/or be set to the oil drum bottom.
CN201821447652.XU 2018-09-05 2018-09-05 Thermostatical oil bath Active CN208878618U (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109078665A (en) * 2018-09-05 2018-12-25 江苏德威新材料股份有限公司 Thermostatical oil bath
CN113274764A (en) * 2021-06-18 2021-08-20 中触媒新材料股份有限公司 Liquid phase adsorption separation system and temperature control process method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109078665A (en) * 2018-09-05 2018-12-25 江苏德威新材料股份有限公司 Thermostatical oil bath
CN113274764A (en) * 2021-06-18 2021-08-20 中触媒新材料股份有限公司 Liquid phase adsorption separation system and temperature control process method thereof

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