CN208829576U - A kind of hot oxygen crosslinking apparatus of energy-saving poly arylidene thio-ester resinoid - Google Patents
A kind of hot oxygen crosslinking apparatus of energy-saving poly arylidene thio-ester resinoid Download PDFInfo
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Abstract
The utility model discloses a kind of hot oxygen crosslinking apparatus of energy-saving poly arylidene thio-ester resinoid, belong to chemical equipment technical field, including hot air supplier and reaction warehouse, the reaction warehouse includes the lower warehouse for being equipped with opening positioned at bottom, both ends above the lower warehouse are equipped with the dismountable hopper being open and the bottom above the hopper offers the upper warehouse of opening, discharge pipe is provided in the upper portion side wall of the upper warehouse, the discharge pipe is communicated with the air inlet of the first air-introduced machine by pipeline, the hot air supplier is connected to by flexible duct with the lower warehouse, the bottom of the lower warehouse is provided with lift drive mechanism, the second air-introduced machine is provided on the flexible duct, the feed hopper bottom opening is provided with reticular structure.The application passes through the setting of integral type reaction warehouse, keeps occupation area of equipment small, and consume energy low, easy to operate, high production efficiency.
Description
Technical field
The utility model relates to chemical technology fields, and in particular to a kind of energy-saving hot oxygen crosslinking dress of poly arylidene thio-ester resinoid
It sets.
Background technique
Poly arylidene thio-ester resinoid includes polyphenylene sulfide, polyaryl thioether sulfone, polyarylene sulfide ketone, polyarylene imide sulfide and poly- virtue
Thioether nitrile etc. refers to that polymeric backbone structure is a kind of high molecular polymer that sulphur replaces connection with heteroaryl structure, by
In the rigidity of particularity and molecular structure that this quasi polymer is constituted, so that they have excellent high temperature resistant, corrosion-resistant, resistance to
Radiation, fire-retardant, electrical property, physical mechanical property and good dimensional stability, being widely used as structural high molecular material makes
With development and application prospect is very wide.
Currently, the production technology of domestic poly arylidene thio-ester resinoid is also immature, resin molecular weight is generally relatively low, molecular weight point
Cloth is wider, causes the various physical mechanical properties of resin poor, significantly limits its application in related fields.
The crosslinking of hot oxygen be improve resin molecular weight and reduce range of molecular weight distributions is the most frequently used, most economical practical method it
One.Equipment used by hot oxygen is crosslinked at present mainly has baking oven, double-cone dryer, boiled bed drying machine etc., these equipment are often
Belong to autonomous device and in one line, respectively between need conveying pump or fan, take up a large area, consume energy it is high, operate
The tail gas of defect cumbersome, production efficiency is low, generation also pollutes the environment, not environmentally, additionally due to heat cross-linking effect is paid no attention to
Think, so that naval stores performance is unstable, poor repeatability.
Utility model content
Occupation area of equipment used by being crosslinked for above-mentioned hot oxygen is big, energy consumption is high, cumbersome, production efficiency lowly
Defect, the purpose of this utility model is to provide a kind of energy-saving hot oxygen crosslinking apparatus of poly arylidene thio-ester resinoid, the poly- virtue of the application
The reaction of the hot oxygen crosslinking of thioether resinoid need to only be carried out in reaction warehouse, and reaction warehouse is the equipment of integral type from bottom to up, takes up an area face
Product is small, and consume energy low, easy to operate, high production efficiency.
To achieve the goals above, the utility model adopts the technical scheme that a kind of energy-saving polyarylphosphorus ethers tree
The hot oxygen crosslinking apparatus of rouge, including hot air supplier and reaction warehouse, the reaction warehouse include positioned at the lower storehouse for being equipped with opening of bottom
Body, the both ends above the lower warehouse are equipped with dismountable hopper of opening and the bottom above the hopper opens up
There is the upper warehouse of opening, discharge pipe is provided in the upper portion side wall of the upper warehouse, the discharge pipe is communicated with by pipeline
The air inlet of one air-introduced machine, the hot air supplier are connected to by flexible duct with the lower warehouse, the bottom of the lower warehouse
It is provided with lift drive mechanism, the second air-introduced machine, the feed hopper bottom opening setting are provided on the flexible duct
There is reticular structure.
Working principle: removing hopper, and the material that need to react is added into hopper, by material send to lower warehouse and upper warehouse it
Between, make lower warehouse, the vertical central axis of hopper and upper warehouse is located on same vertical line, and lift drive mechanism drives on lower warehouse
It moves, lower warehouse, hopper and upper warehouse is compressed, hot air supplier generates hot-air, by the second air-introduced machine by hot-air from soft
Property pipeline enters in hopper, hot-air blows afloat material in hopper, and material is being expected to lower warehouse from the through-hole of feed hopper bottom
Vertical space between bucket and upper warehouse comes into full contact with hot-air and is heated, and carries out cross-linking reaction, the tail generated in reaction
It is processed that gas enters discharge pipe discharge, and after reaction, lift drive mechanism drives lower warehouse decline, lower warehouse, hopper and on
It is unclamped between warehouse, hopper is pulled out and discharged;The reticular structure of feed hopper bottom opening setting makes the material in hopper will not
It is spilt from feed hopper bottom, gas can enter hopper by reticular structure.The application charging after, by lower warehouse, hopper and on
Warehouse sealing gland, reaction effect is good, after reaction unclamps lower warehouse, hopper and upper warehouse gas, facilitates discharging, pass through integral type
The setting of reaction warehouse keeps occupation area of equipment small, and consume energy low, easy to operate, high production efficiency, solves above-mentioned hot oxygen crosslinking institute
The defect that the occupation area of equipment of use is big, energy consumption is high, cumbersome, production efficiency is low.
Further, it is connected with air-exhausting duct on the air outlet of first air-introduced machine, is provided with first on the air-exhausting duct
Valve, is provided with backwind tube on the air-exhausting duct between first air-introduced machine and first valve, on the backwind tube
It is provided with the second valve, the hot air supplier includes hot wind cavity and the mixing chamber that is connected to the hot wind cavity, institute
The one end for stating hot wind cavity is communicated with backwind tube, and another end opening is provided in the mixing chamber, described mixing chamber one end
It is open and covers at the hot wind containment portion, the other end is communicated with the flexible duct.The first valve is closed, the second valve is opened
Door, the hot gas come out from reaction warehouse enter backwind tube after discharge pipe and the first air-introduced machine and enter mixing chamber by hot wind cavity
Body enters hopper by flexible duct after heating again, realizes recycling for thermal energy;Mixing chamber is open at one end and is provide with
In the hot wind containment portion, there are small gaps therebetween, not only can be with to make part cold air enter hot air supplier
Guarantee the oxygen for having sufficient in reaction warehouse, hot wind loss can also be supplemented, adjust the temperature inside hot air supplier.
Further, electric heating tube is provided in the hot air supplier.Electric heater for heating air and tail gas.
Further, the hopper two sides are symmetrically arranged with bracket, are rotatablely connected between the hopper and bracket, the branch
Frame bottom is provided with multiple universal wheels, and push rod is additionally provided on the bracket, and temperature sensor is provided in the hopper, described
Controller is provided in hopper exterior side wall, the temperature sensor is electrically connected with the controller.Bracket and its bottom are universal
The setting of wheel facilitates hopper to be put between movable cabin and upper warehouse, is also convenient for hopper and pulls out discharging or charging, hopper and bracket it
Between the setting that is rotatablely connected facilitate charging and discharging;Temperature when heat cross-linking reaction in temperature sensor real-time monitoring hopper occurs
Degree, and controller is transmitted information to, controller shows information, that is, needs to heat or cool down.
Further, at least two cloth bag retainer plate, Mei Gesuo are disposed with from bottom to up along inner wall in the upper storehouse body
It states and is provided with cloth bag on cloth bag retainer plate, the nozzle of the discharge pipe is located at the top of cloth bag retainer plate described in top.Cloth bag
Barrier effect is risen to material, prevents material from entering discharge pipe with tail gas, prevents loss of material, yield is high.
Further, it is additionally provided with pulser on the upper warehouse, the pulser includes air accumulator, is located at gas storage
Tank side and the pulse tracheae being connected to the upper warehouse, positioned at multiple gas outlets of the upper storehouse intracorporal pulse tracheae lower part
And the pulser controller on the pulse tracheae of the external side of the upper storehouse.At the end of reaction, impulse controller control will
Dry air moment pours pulse tracheae in air accumulator, pours upper warehouse from multiple gas outlet moments, interpulse period is about
20S/ times, the resin for being adhered to top warehouse is back in hopper, closes pulse airgun controller after opening 3~5min, wait
It carries out turning material after 5min.
Further, the air-exhausting duct is connected to exhaust gas processing device, and the exhaust gas processing device includes lye tank (vat), is located at
Tower body above the lye tank (vat) and the offgas duct at the top of the tower body pass through between the lye tank (vat) and the tower body
Alkali liquor pipe is connected to, and is provided with lye pump on the alkali liquor pipe, Multi-layer supporting net, every layer of supporting network are provided in the tower body
Top be provided with inert ceramic balls stratum granulosum, the intracorporal lye tube end of tower is provided with alkaline liquor distributor, the lye
Distributor is located at the top of inert ceramic balls stratum granulosum described in top, and the end of the air-exhausting duct is provided with gas in the tower body
Distributor, the gas distributor are located at the lower section of supporting network described in the bottom.Tail gas in reaction warehouse is through discharge pipe stream and row
Air hose enters from tower body bottom, at the same lye through liquid-feeding tube under tower body overhead stream, tail gas and lye counter current contacting, by tail gas
In sulfur dioxide, sulfur trioxide, amine gas and pernicious gas be fully absorbed, it is processed after clean tail gas from offgas duct
Emptying;Because of the large specific surface area of inert ceramic balls particle, gas good dispersion, uniform air distribution;Alkaline liquor distributor falls lye dispersion
Under, gas distributor makes tail gas be evenly distributed.
Further, the side of the upper warehouse is provided with transparent visual window.Convenient for the reaction condition in observing response storehouse,
Convenient artificial control and adjusting.
Further, the lift drive mechanism is cylinder.Facilitate operation.
A kind of method of the hot oxygen crosslinking of energy-saving poly arylidene thio-ester resinoid, comprising the following steps:
S1: material is added in the movable cabin into hopper;
S2: being pushed into position and fixation between lower warehouse and upper warehouse for hopper, opens cylinder for the intracorporal activity in lower storehouse
Storehouse, hopper and upper warehouse compress:
S3: the offer hot-air of hot air supplier is gone forward side by side in material bin, and material in hopper is blown afloat, and material is in hopper and upper
Vertical space between warehouse comes into full contact with hot-air and is heated, and carries out cross-linking reaction:
S4: after temperature needed for the temperature in hopper reaches reaction, tail gas in reaction warehouse through discharge pipe stream and air-exhausting duct,
Enter from tower body bottom, at the same lye through liquid-feeding tube under tower body overhead stream, tail gas and lye counter current contacting, by two in tail gas
Sulfur oxide, sulfur trioxide, amine gas and pernicious gas are fully absorbed, and clean tail gas is emptied from offgas duct after processed.
S5: after completion of the reaction, exhaust gas processing device, unbalanced pulse device 3- are closed in the material cooling in feed hopper later
5min makes in the intracorporal material whole return value hopper of upper storehouse;
S6: opening cylinder, and cylinder stretches downwards, separates hopper with upper warehouse and lower warehouse, and hopper is pushed into spaciousness
Place discharging.
This method passes through the reaction warehouse of the integral type of setting, so that simple and convenient, simple process, hot oxygen in reaction warehouse
Oxygen supply is sufficient when crosslinking and reaction warehouse in temperature stablize so that hot oxygen cross-linking effect is ideal, so that naval stores performance is steady
Fixed, stability is high;By to vent gas treatment, by the sulfur dioxide generated in cross-linking reaction, sulfur trioxide, amine gas and nocuousness
Gas empties after being absorbed by lye, does not pollute the environment, safety and environmental protection;It is successfully realized recycling for hot wind.
Based on described above, the utility model compared with prior art, after having the advantages that (1) charging, will live
Dynamic storehouse, hopper and upper warehouse sealing gland, reaction effect is good, after reaction unclamps movable cabin, hopper and upper warehouse gas, conveniently goes out
Material, by the setting of integral type reaction warehouse, keeps occupation area of equipment small, and consume energy low, easy to operate, high production efficiency;(2) success
Realize recycling for hot wind;(3) return air cover is close with air inlet but does not contact, to make part cold air enter hot wind supply
Device can not only guarantee the oxygen for having sufficient in reaction warehouse, can also supplement hot wind loss, adjust inside hot air supplier
Temperature;(4) setting of bracket and its Universal wheel at bottom facilitates hopper to be put between movable cabin and upper warehouse, is also convenient for hopper drawing
Discharging or charging, the setting being rotatablely connected between hopper and bracket facilitate charging and discharging;(5) bag, which plays material, stops to make
With preventing material from entering discharge pipe with tail gas, prevent loss of material, yield is high;(6) this method is simple and convenient, technique letter
It is single, in reaction warehouse when the crosslinking of hot oxygen oxygen supply is sufficient and reaction warehouse in temperature stablize so that hot oxygen cross-linking effect is ideal so that
Naval stores performance is stablized, and stability is high;(7) by the way that vent gas treatment, the sulfur dioxide generated in cross-linking reaction, three are aoxidized
Sulphur, amine gas and pernicious gas empty after being absorbed by lye, do not pollute the environment, safety and environmental protection.
Detailed description of the invention
Fig. 1 be the utility model proposes a kind of energy-saving hot oxygen crosslinking apparatus of poly arylidene thio-ester resinoid structural representation
Figure;
Fig. 2 be the utility model proposes a kind of energy-saving hot oxygen crosslinking apparatus of poly arylidene thio-ester resinoid pulser
Structural schematic diagram.
In figure: 1- hot air supplier, warehouse under 2-, 3- hopper, 4- bracket, 5- universal wheel, the upper warehouse of 6-, 7- discharge pipe,
The first air-introduced machine of 8-, 9- air-exhausting duct, the first valve of 10-, 11- backwind tube, the second valve of 12-, 13- hot wind cavity, 14- gas point
Cloth device, 15- lye tank (vat), 16- lye pump, 17- alkali liquor pipe, 18- alkaline liquor distributor, 19- tower body, 20- offgas duct, 21- electric heating
Pipe, 22- cloth bag retainer plate, 23- visual window, 24- appendix, 25- mixing chamber, 26- cylinder, 27- air accumulator, 28- pulse air
Controller, 29- pulse tracheae, 31- supporting network, 32- inert ceramic balls stratum granulosum.
In the technical solution of the application: → indicate airflow direction direction.
Specific embodiment
In order to make those skilled in the art more fully understand the technical solution of the utility model, below with reference to specific implementation
The utility model is described in further detail for example.
Embodiment 1
As shown in Figure 1, a kind of hot oxygen crosslinking apparatus of energy-saving poly arylidene thio-ester resinoid, including hot air supplier 1 and reaction
Storehouse, it is characterised in that: the reaction warehouse includes the lower warehouse 2 for being equipped with opening positioned at bottom, above the lower warehouse 2
Both ends are equipped with the dismountable hopper 3 being open and the bottom above the hopper 3 offers the upper warehouse 6 of opening, described
Discharge pipe 7 is provided in the upper portion side wall of upper warehouse 6, the discharge pipe 7 is communicated with the air inlet of the first air-introduced machine 8 by pipeline
Mouthful, the hot air supplier 1 is connected to by flexible duct 24 with the lower warehouse 2, and the bottom of the lower warehouse 2 is provided with lifting
Driving mechanism is provided with the second air-introduced machine on the flexible duct 24, is provided with reticular structure at 3 bottom opening of hopper.
Working principle: removing hopper 3, and the material that need to be reacted is added into hopper 3, material is sent to lower warehouse 2 and upper storehouse
Between body 6, make lower warehouse 2, the vertical central axis of hopper 3 and upper warehouse 6 is located on same vertical line, and lift drive mechanism drives
Lower warehouse 2 moves up, and warehouse 2, hopper 3 and upper warehouse 6 are compressed, and hot air supplier 1 generates hot-air, passes through the second air-introduced machine
Hot-air is delivered to lower warehouse 2 from flexible duct 24, and is entered in hopper 3 from the through-hole of 3 bottom of hopper, hot-air is by hopper
Material is blown afloat in 3, and vertical space of the material between hopper 3 and upper warehouse 6 comes into full contact with hot-air and be heated, and is handed over
Connection reaction, the tail gas generated in reaction enter discharge pipe 7 and are discharged processed, and after reaction, lift drive mechanism drives lower storehouse
Body 2 declines, and unclamps between lower warehouse 2, hopper 3 and upper warehouse 6, hopper 3 is pulled out and discharged;It is arranged at 3 bottom opening of hopper
Reticular structure spill the material in hopper 3 will not from 3 bottom of hopper, gas can enter hopper 3 by reticular structure.
After the application charging, by 6 sealing gland of lower warehouse 2, hopper 3 and upper warehouse, reaction effect is good, after reaction by lower warehouse 2, hopper
3 and 6 gas of upper warehouse unclamp, facilitate discharging, by the setting of integral type reaction warehouse, keep occupation area of equipment small, consume energy it is low, operate
Simply, high production efficiency, solves that occupation area of equipment used by above-mentioned hot oxygen is crosslinked is big, energy consumption is high, cumbersome, produces
The defect of inefficiency.
The upper opening of lower warehouse 2 matches with the bottom of hopper 3, and the upper opening of hopper 3 and the bottom of upper warehouse are opened
Mouth matches.
Flexible duct 24 is flexible duct that is extending and shortening, with lower warehouse in convenient lower warehouse process of rising or falling
It elongates or shortens.
Embodiment 2
Based on embodiment 1, as shown in Figure 1, air-exhausting duct (9) are connected on the air outlet of first air-introduced machine (8), it is described
It is provided on air-exhausting duct (9) the first valve (10), the row between first air-introduced machine (8) and first valve (10)
It is provided on air hose (9) backwind tube (11), is provided with the second valve (12), the hot air supplier on the backwind tube (11)
(1) mixing chamber (25) for including hot wind cavity (13) and being connected to the hot wind cavity (13), the hot wind cavity (13)
One end be communicated with backwind tube (11), another end opening is provided in the mixing chamber (25), the mixing chamber (25) one
End opening simultaneously covers at hot wind cavity (13) outside, and the other end is communicated with the flexible duct (24).
The first valve 10 is closed, the second valve 12 is opened, the hot gas come out from reaction warehouse is through discharge pipe 7 and the first air-introduced machine
Enter backwind tube 11 after 8 and mixing chamber 25 is entered by hot wind cavity 13, hopper is entered by flexible duct 24 after heating again
3, realize recycling for thermal energy;Mixing chamber 25 is open at one end and covers at outside hot wind cavity 13, therebetween there are
Small gap can not only guarantee the oxygen for having sufficient in reaction warehouse, may be used also to make part cold air enter hot air supplier 1
To supplement hot wind loss, the temperature inside hot air supplier 1 is adjusted;The hot wind cavity 13 is that wide-mouth is tubaeform, can make to come from
The hot-air of backwind tube 11 is evenly spread out.
Embodiment 3
Based on embodiment 1, as shown in Figure 1, being provided with electric heating tube 21 in the hot air supplier 1.
Electric heating tube 21 heats air and tail gas;Electric heating tube 21 is provided with switch on power supply, just by extraneous power supply power supply
In power supply or power-off.
Embodiment 4
Based on embodiment 1, as shown in Figure 1,3 two sides of the hopper are symmetrically arranged with bracket 4, the hopper 3 and bracket 4 it
Between be rotatablely connected, 4 bottom of bracket is provided with multiple universal wheels 5, push rod is additionally provided on the bracket 4, in the hopper 3
It is provided with temperature sensor, controller, the temperature sensor and controller electricity are provided in 3 exterior side wall of hopper
Connection.
The setting of bracket 4 and its Universal wheel at bottom 5 facilitates hopper 3 to be put between movable cabin 25 and upper warehouse 6, is also convenient for
Hopper 3 pulls out discharging or charging, the setting being rotatablely connected between hopper 3 and bracket 4 facilitate charging and discharging, each universal wheel 5
On be provided with brake block, facilitate fixed universal wheel 5;Occur when heat cross-linking reaction in temperature sensor real-time monitoring hopper 3
Temperature, and controller is transmitted information to, controller shows information, that is, needs to heat or cool down.
Embodiment 5
Based on embodiment 1, as shown in Figure 1, being disposed at least two cloth from bottom to up along inner wall in the upper warehouse 6
Bag retainer plate 22, is provided with cloth bag on each cloth bag retainer plate 22, the nozzle of the discharge pipe 7 is located at described in top
The top of cloth bag retainer plate 22.
Cloth bag plays barrier effect to material, prevents material from entering discharge pipe 7 with tail gas, prevents loss of material, and yield is high.
Embodiment 6
Based on embodiment 1, as shown in Figs. 1-2, pulser, the pulser packet are additionally provided on the upper warehouse 6
Air accumulator 27 is included, positioned at 27 side of air accumulator and the pulse tracheae 29 that is connected to the upper warehouse 6, is located in the upper warehouse 6
29 lower part of pulse tracheae multiple gas outlets and the pulser control on the pulse tracheae 29 in 6 outside of upper warehouse
Device processed.
At the end of reaction, air moment dry in air accumulator 27 is poured pulse tracheae 29 by impulse controller control, from
Multiple gas outlet moments pour warehouse 6, and interpulse period about 20S/ times, the resin for being adhered to top warehouse is back to material
In bucket 3, pulse airgun controller 28 is closed after opening 3~5min, carries out turning material after waiting 5min.
Embodiment 7
Based on embodiment 1, as shown in Figure 1, the air-exhausting duct 9 is connected to exhaust gas processing device, the exhaust gas processing device
Including lye tank (vat) 15, the tower body 19 above the lye tank (vat) 15 and the offgas duct 20 positioned at 19 top of tower body, institute
It states and is connected between lye tank (vat) 15 and the tower body 19 by alkali liquor pipe 17, lye pump 16 is provided on the alkali liquor pipe 17, it is described
Multi-layer supporting net 31 is provided in tower body 19, the top of every layer of supporting network 31 is provided with inert ceramic balls stratum granulosum 32, institute
It states 17 end of alkali liquor pipe in tower body 19 and is provided with alkaline liquor distributor 18, the alkaline liquor distributor 18 is located at lazy described in top
The top of property porcelain variole granulosa 32, the end of the air-exhausting duct 9 is provided with gas distributor 14, the gas in the tower body 19
Distributor 14 is located at the lower section of supporting network 31 described in the bottom.
Tail gas in reaction warehouse enters, while lye is through liquid-feeding tube through the stream of discharge pipe 7 and air-exhausting duct 9 from 19 bottom of tower body
Under 19 overhead stream of tower body, tail gas and broken liquid counter current contacting, by tail gas sulfur dioxide, sulfur trioxide, amine gas and have
Evil gas is fully absorbed, and clean tail gas is emptied from offgas duct 20 after processed;Because of the large specific surface area of inert ceramic balls particle,
Gas good dispersion, uniform air distribution;Alkaline liquor distributor 18 falls lye dispersion, and gas distributor 14 makes tail gas be evenly distributed.
Embodiment 8
Based on embodiment 1, as shown in Figure 1, the side of the upper warehouse 6 is provided with transparent visual window 23.
Convenient for the reaction condition in observing response storehouse, convenient artificial control and adjusting.
Embodiment 8
Based on embodiment 1, as shown in Figure 1,
The lift drive mechanism is cylinder 26.Lift drive mechanism may be hydraulic cylinder, and cylinder 26 and hydraulic cylinder are equal
For the prior art, respectively has switch and control its automatic control module risen or decline.
Embodiment 10
A kind of method of the hot oxygen crosslinking of energy-saving poly arylidene thio-ester resinoid, comprising the following steps:
S1: material is added in the movable cabin 25 into hopper 3;
S2: hopper 3 is pushed into position and fixation between lower warehouse 2 and upper warehouse 6, opening cylinder 26 will be in lower warehouse 2
Movable cabin 25, hopper 3 and upper warehouse 6 compress;
S3: the offer hot-air of hot air supplier 1 is gone forward side by side in material bin 3, material in hopper 3 is blown afloat, material is in hopper 3
Vertical space between upper warehouse 6 comes into full contact with hot-air and is heated, and carries out cross-linking reaction;
S4: after temperature needed for the temperature in hopper 3 reaches reaction, the tail gas in reaction warehouse is flowed through discharge pipe 7 and air draft
Pipe 9 enters from 19 bottom of tower body, at the same lye through liquid-feeding tube under 19 overhead stream of tower body, tail gas and lye counter current contacting, by tail
Sulfur dioxide, sulfur trioxide, amine gas and pernicious gas in gas are fully absorbed, it is processed after clean tail gas from tail gas
Pipe 20 empties.
S5: after completion of the reaction, exhaust gas processing device, unbalanced pulse device 3- are closed in the material cooling in feed hopper 3 later
5min makes in the material whole return value hopper 3 in warehouse 6;
S6: opening cylinder 26, and cylinder 26 is flexible downwards, separates hopper 3 with upper warehouse 6 and lower warehouse 2, and by hopper 3
It is pushed into spacious place discharging.
This method passes through the reaction warehouse of the integral type of setting, so that simple and convenient, simple process, hot oxygen in reaction warehouse
Oxygen supply is sufficient when crosslinking and reaction warehouse in temperature stablize so that hot oxygen cross-linking effect is ideal, so that naval stores performance is steady
Fixed, stability is high;By to vent gas treatment, by the sulfur dioxide generated in cross-linking reaction, sulfur trioxide, amine gas and nocuousness
Gas empties after being absorbed by lye, does not pollute the environment, safety and environmental protection;It is successfully realized recycling for hot wind.
Technical staff in the field should be appreciated that the first air-introduced machine 8 described in this programme, the second air-introduced machine, gas distribution
Device 14, alkaline liquor distributor 18, cylinder 26, pulse airgun controller 28, belonging to the prior art can adopt on the market according to specific requirements
The product of different model and specification is bought, such as the model of the first air-introduced machine and the first air-introduced machine is in the utility model
GD30K2-12, the model XHTB-1001 of gas distributor, the model TX03 of alkaline liquor distributor, cylinder SCJ, pulse airgun controller
Model MCY-64.
The above are the main feature of this programme and its advantages, It should be understood by those skilled in the art that this programme is not
It is restricted to the described embodiments, the above embodiments and description only describe the principles of this programme, are not departing from this
Under the premise of scheme spirit and scope, this programme be will also have various changes and improvements, these changes and improvements both fall within requirement and protect
In the scope of the utility model of shield, this programme is claimed range and is defined by the appending claims and its equivalent thereof.
In the description of the present invention, it should also be noted that, unless otherwise clearly defined and limited, term " is set
Set ", " installation ", " connected ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, be also possible to dismantling connection, or
It is integrally connected;It can be mechanical connection, be also possible to be electrically connected;It can be directly connected, intermediate media's letter can also be passed through
It is situated between and is connected, can be the connection inside two elements.It for the ordinary skill in the art, can be as the case may be
Understand the concrete meaning of above-mentioned term in the present invention.
Claims (9)
1. a kind of hot oxygen crosslinking apparatus of energy-saving poly arylidene thio-ester resinoid, including hot air supplier (1) and reaction warehouse, feature exist
In: the reaction warehouse includes the lower warehouse (2) for being equipped with opening positioned at bottom, is located at the both ends above the lower warehouse (2) and sets
The bottom for having dismountable hopper (3) of opening and being located above the hopper (3) offers the upper warehouse (6) of opening, described
It is provided with discharge pipe (7) in the upper portion side wall of upper warehouse (6), the discharge pipe (7) is communicated with the first air-introduced machine (8) by pipeline
Air inlet, the hot air supplier (1) is connected to by flexible duct (24) with the lower warehouse (2), the lower warehouse (2)
Bottom is provided with lift drive mechanism, and the second air-introduced machine, hopper (3) bottom opening are provided on the flexible duct (24)
Place is provided with reticular structure.
2. a kind of energy-saving hot oxygen crosslinking apparatus of poly arylidene thio-ester resinoid according to claim 1, it is characterised in that: described
It is connected on the air outlet of first air-introduced machine (8) air-exhausting duct (9), is provided with the first valve (10) on the air-exhausting duct (9), it is described
Backwind tube (11), the return air are provided on the air-exhausting duct (9) between first air-introduced machine (8) and first valve (10)
Pipe (11) on be provided with the second valve (12), the hot air supplier (1) include hot wind cavity (13) and with the hot air cavity
The mixing chamber (25) of body (13) connection, one end of the hot wind cavity (13) are communicated with backwind tube (11), and another end opening is set
It being equipped in the mixing chamber (25), the mixing chamber (25) is open at one end and covers at hot wind cavity (13) outside,
The other end is communicated with the flexible duct (24).
3. a kind of energy-saving hot oxygen crosslinking apparatus of poly arylidene thio-ester resinoid according to claim 1 or 2, it is characterised in that:
Electric heating tube (21) are provided in the hot air supplier (1).
4. a kind of energy-saving hot oxygen crosslinking apparatus of poly arylidene thio-ester resinoid according to claim 1, it is characterised in that: described
Hopper (3) two sides are symmetrically arranged with bracket (4), are rotatablely connected between the hopper (3) and bracket (4), bracket (4) bottom
It is provided with multiple universal wheels (5), push rod is additionally provided on the bracket (4), is provided with temperature sensor in the hopper (3),
It is provided with controller in hopper (3) exterior side wall, the temperature sensor is electrically connected with the controller.
5. a kind of energy-saving hot oxygen crosslinking apparatus of poly arylidene thio-ester resinoid according to claim 1, it is characterised in that: described
At least two cloth bag retainer plate (22), each cloth bag retainer plate are disposed with from bottom to up along inner wall in upper warehouse (6)
(22) cloth bag is provided on, the nozzle of the discharge pipe (7) is located at the top of cloth bag retainer plate (22) described in top.
6. a kind of energy-saving hot oxygen crosslinking apparatus of poly arylidene thio-ester resinoid according to claim 1, it is characterised in that: described
Pulser is additionally provided on upper warehouse (6), the pulser includes air accumulator (27), be located at air accumulator (27) side and with
The pulse tracheae (29) of the upper warehouse (6) connection, be located at pulse tracheae (29) lower part in the upper warehouse (6) it is multiple go out
Pulse airgun controller (28) on port and the pulse tracheae (29) being located on the outside of the upper warehouse (6).
7. a kind of energy-saving hot oxygen crosslinking apparatus of poly arylidene thio-ester resinoid according to claim 2, it is characterised in that: described
Air-exhausting duct (9) is connected to exhaust gas processing device, and the exhaust gas processing device includes lye tank (vat) (15), is located at the lye tank (vat) (15)
The tower body (19) of top and the offgas duct (20) being located at the top of the tower body (19), the lye tank (vat) (15) and the tower body
(19) it is connected between by alkali liquor pipe (17), is provided with lye pump (16) on the alkali liquor pipe (17), set in the tower body (19)
It is equipped with Multi-layer supporting net (31), the top of every layer of supporting network (31) is provided with inert ceramic balls stratum granulosum (32), the tower
Alkali liquor pipe (17) end in body (19) is provided with alkaline liquor distributor (18), and the alkaline liquor distributor (18) is located at described in top
The top of inert ceramic balls stratum granulosum (32), the end of the air-exhausting duct (9) is provided with gas distributor in the tower body (19)
(14), the gas distributor (14) is located at the lower section of supporting network (31) described in the bottom.
8. a kind of energy-saving hot oxygen crosslinking apparatus of poly arylidene thio-ester resinoid according to claim 1, it is characterised in that: described
The side of upper warehouse (6) is provided with transparent visual window (23).
9. a kind of energy-saving hot oxygen crosslinking apparatus of poly arylidene thio-ester resinoid according to claim 1, it is characterised in that: described
Lift drive mechanism is cylinder (26).
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CN201821211961.7U CN208829576U (en) | 2018-07-27 | 2018-07-27 | A kind of hot oxygen crosslinking apparatus of energy-saving poly arylidene thio-ester resinoid |
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CN201821211961.7U CN208829576U (en) | 2018-07-27 | 2018-07-27 | A kind of hot oxygen crosslinking apparatus of energy-saving poly arylidene thio-ester resinoid |
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Effective date of registration: 20230504 Address after: 620200 Zone A, Economic Development Zone, Danling County, Meishan City, Sichuan Province Patentee after: Sichuan Zhongke Hangyu New Materials Co.,Ltd. Address before: 620038 Jinxiang Chemical Industrial Park, Dongpo District, Meishan City, Sichuan Province Patentee before: SICHUAN ZHONGKE XINGYE HIGH-TECH MATERIALS CO.,LTD. |