CN208771417U - Reaction kettle is used in a kind of production of reagent - Google Patents
Reaction kettle is used in a kind of production of reagent Download PDFInfo
- Publication number
- CN208771417U CN208771417U CN201821362957.0U CN201821362957U CN208771417U CN 208771417 U CN208771417 U CN 208771417U CN 201821362957 U CN201821362957 U CN 201821362957U CN 208771417 U CN208771417 U CN 208771417U
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- CN
- China
- Prior art keywords
- autoclave body
- reaction kettle
- inner tube
- production reaction
- outer ring
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 70
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 23
- 239000003153 chemical reaction reagent Substances 0.000 title claims abstract description 16
- 239000007788 liquid Substances 0.000 claims abstract description 21
- 230000002093 peripheral effect Effects 0.000 claims abstract description 16
- 239000007787 solid Substances 0.000 claims 1
- 239000000376 reactant Substances 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 238000000605 extraction Methods 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 239000010865 sewage Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000013475 authorization Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a kind of reagent production reaction kettles, it is related to chemical equipment technical field, situations such as being easy to appear layering between the liquid reactant for solving each layer and lead to the insufficient contact between reactant, the problem of reducing production efficiency, its key points of the technical solution are that: including autoclave body, agitating device is equipped in autoclave body, its short transverse of autoclave body outer is fitted with outer ring, sink is provided on outer ring inner peripheral surface, several through-holes for being connected to sink are provided on autoclave body outer peripheral surface, autoclave body is externally connected with the pump housing, the pump housing is equipped with inlet tube and drain pipe, sink is connected to inlet tube or drain pipe.Reach and reaction solution has been sufficiently mixed, has improved the effect of its production efficiency.
Description
Technical field
The utility model relates to chemical equipment technical fields, more specifically, it relates to which reaction kettle is used in a kind of production of reagent.
Background technique
Reaction kettle has the container physically or chemically reacted, by the structure design and parameter configuration to container, realizes work
The mixed function of heating, evaporation, cooling and low high speed that skill requires.It is widely used in petroleum, chemical industry, rubber, pesticide, dye
Material, medicine, food, for completing the pressure vessel of the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation, such as instead
Answer device, reaction pot, decompose pot, polymeric kettle etc..
Currently, the Chinese patent that Authorization Notice No. is CN207576388U discloses a kind of reaction kettle, including autoclave body, stirring
Device, temperature measuring equipment and fixed frame, agitating device lower end are arranged in autoclave body, and agitating device upper end is fixedly connected with fixed frame,
Temperature measuring equipment is set in autoclave body, and the autoclave body includes the interior autoclave body being arranged in external kettle body and external kettle body, is set among interior autoclave body bottom
Discharge duct is set, sewage pipe is set among external kettle body bottom, discharge duct upper end is located inside sewage pipe, and discharge duct lower end passes through blowdown
Pipe is located on the outside of sewage pipe.
Although the utility model can facilitate discharge dirt by the way that sewage pipe to be set among external kettle body bottom.But it is single
Situations such as pure is stirred, and is easy to appear layering between the liquid reactant of each layer and cause the contact between reactant not filled
Point, reduce production efficiency.
Utility model content
It in view of the deficiencies of the prior art, can be right the purpose of the utility model is to provide a kind of reagent production reaction kettle
Reaction solution is sufficiently mixed, its production efficiency is improved.
The above-mentioned technical purpose of the utility model has the technical scheme that
A kind of reagent production reaction kettle, including autoclave body, the autoclave body is interior to be equipped with agitating device, its height of the autoclave body outer
Degree direction is fitted with outer ring, and sink is provided on the outer ring inner peripheral surface, is provided on the autoclave body outer peripheral surface and several is connected to water
The through-hole of slot, the autoclave body are externally connected with the pump housing, and the pump housing is equipped with inlet tube and drain pipe, and the sink is connected to inlet tube
Or drain pipe.
By using above-mentioned technical proposal: the reaction solution on different height is extracted by inlet tube into the pump housing out of autoclave body
It is interior, then be drained into autoclave body in the reaction solution of different height by the pump housing by drain pipe, it realizes between the reaction solution of different height
Quickly adequately contact mixing, improves the reaction efficiency of reaction solution, improves production efficiency；It will by the setting of outer ring and through-hole
The reaction solution of different location is extracted and is discharged in autoclave body, reduces the reaction as caused by the extraction of single position unevenly,
Cause partial region to still need to futher stir after reaction to wait the complete reaction of all reaction solutions to terminate, improves anti-
Answer efficiency.
The utility model is further arranged to: corresponding inlet tube is spaced in the vertical direction with the outer ring of corresponding drain pipe to be set
It sets.
By using above-mentioned technical proposal: the setting of outer ring, which facilitates, is equably extracted the upper reaction solution of each height
Or discharge, the reaction in each height is drawn into the reaction solution for being emitted into each height again together, the anti-of each height is made
It answers and is come into full contact between liquid, improve reaction efficiency.
The utility model is further arranged to: the projection of through-hole in the horizontal plane in adjacent outer ring is arranged in a staggered manner.
By using above-mentioned technical proposal: preventing from being easy to constitute back to the extraction of reaction solution and discharge between adjacent outer ring
Road guarantees that the reaction solution being emitted on different height can be carried out stirring and reaction, improves reaction efficiency.
The utility model is further arranged to: through hole is communicated with the kettle inner tube towards autoclave body center line, the kettle inner tube
It is closed at one end far from through-hole, and the liquid separating port in several outsides in kettle inner tube is arranged along the axial direction of on kettle inner tube periphery wall.
By using above-mentioned technical proposal: will extract and discharge the position of reaction solution by the setting of kettle inner tube and liquid separating port
The different position of autoclave body is set, prevents from causing when extracting and discharge by the through-hole being arranged on autoclave body circumferential surface close to autoclave body center
Reaction solution reaction efficiency it is relatively low, make different location in autoclave body reaction solution react it is more uniform, improve reaction kettle in
General reaction efficiency.
The utility model is further arranged to: the liquid separating port opening is arranged along the vertical direction.
By using above-mentioned technical proposal: due to the setting of kettle inner tube, so for stirring in general agitating device
Stirrer paddle can be staggered with kettle inner tube, and liquid separating port is provided with along the vertical direction to be conducive to change at the stirrer paddle above or below it
Reaction solution environment, the reaction solution at this is extracted or is discharged other reaction solution, improve reaction efficiency.
The utility model is further arranged to: the kettle inner tube is equipped with prism close to one end outer peripheral surface of autoclave body side wall
Block is correspondingly provided with mounting base on the autoclave body inner sidewall, is equipped with the rib hole to match with prism block, the peace in the mounting base
Seat is filled equipped with the fixing piece for fixing position between prism block and rib hole.
By using above-mentioned technical proposal: kettle inner tube is detachably arranged, it is convenient that kettle inner tube is dismounted in autoclave body
Or replacement；Due to needing to guarantee the position of liquid separating port, the mode being directly connected through a screw thread is difficult to ensure the vertical of liquid separating port, therefore
Kettle inner tube is plugged in mounting base, by the movement and rotation of prism block and the cooperation limitation kettle inner tube radial direction in rib hole, then by
The position of the fixed kettle inner tube of fixing piece.
The utility model is further arranged to: the mounting base is that cylindric and its outer peripheral surface is equipped with screw thread, fixing piece
Including the sleeve being threadedly connected to outside mounting base, the sleeve is connected to the end of prism block far from the inner sidewall of autoclave body side wall one end
Face.
By using above-mentioned technical proposal: limiting kettle inner tube moving along its axial direction by sleeve, and to prism block and rib
Play certain sealing effect in gap between hole.
The utility model is further arranged to: it is equipped with horizontal treadle along its short transverse on the autoclave body internal perisporium, it is described
Treadle is fixed on autoclave body internal perisporium at U-shaped and its both ends.
By using above-mentioned technical proposal: user steps on treadle entrance when facilitating installation or replacing to kettle inner tube
The intracorporal part of kettle is installed or replaced in autoclave body.
In conclusion the utility model has the following beneficial effects:
The reaction solution of different height, different location is extracted by the setting of outer ring and kettle inner tube, then is injected into
To different height, different location autoclave body inside, make the reaction solution of each position inside autoclave body carry out coming into full contact with mixing, raising
Production efficiency.
Detailed description of the invention
Fig. 1 is a kind of overall structure diagram for reagent production reaction kettle that embodiment provides；
Fig. 2 is cross-sectional view of the Fig. 1 along the direction A-A；
Fig. 3 is cross-sectional view of the Fig. 1 along the part-structure in the direction B-B;
Fig. 4 is the enlarged drawing of C portion in Fig. 3.
In figure: 1, autoclave body；11, outer ring；111, sink；12, through-hole；13, mounting base；131, rib hole；132, sleeve；14,
Treadle；15, support；16, feed inlet；17, discharge port；18, lid；2, agitating shaft；21, motor；22, stirrer paddle；3, the pump housing；
31, inlet tube；32, drain pipe；4, kettle inner tube；41, liquid separating port；42, prism block.
Specific embodiment
The utility model is described in further detail below in conjunction with attached drawing.
Embodiment:
The utility model embodiment discloses a kind of reagent production reaction kettle, referring to Figures 1 and 2, including autoclave body 1, kettle
Body 1 includes the lid 18 of its top surface, is connected between lid 18 and autoclave body 1 by bolt, and lid 18 is equipped with feed inlet 16, kettle
1 bottom surface of body is communicated with discharge port 17, is equipped with agitating device in autoclave body 1, agitating device includes the agitating shaft 2 coaxial with autoclave body 1, kettle
It is connected with the motor 21 that driving agitating shaft 2 rotates above body 1, is arranged along the axial direction of 3 groups of stirrer paddles 22, kettle on agitating shaft 2
The fitting of its short transverse of 1 outer of body is fixed with 4 circle outer rings 11, and stirrer paddle 22 and outer ring 11 are spaced setting in the vertical direction.
Referring to Fig. 2, enter the part installed or replaced in autoclave body 1 in autoclave body 1 for the convenience of the users, in autoclave body 1
It is equipped with horizontal treadle 14 along its short transverse on peripheral wall, treadle 14 is fixed on 1 internal perisporium of autoclave body at U-shaped and its both ends.
Referring to Figures 1 and 2, it is provided with sink 111 on 11 inner peripheral surface of outer ring, is provided with two on 1 outer peripheral surface of autoclave body and is connected to correspondence
The through-hole 12(of sink 111 is as shown in Figure 3), autoclave body 1 is externally connected with the pump housing 3, and the pump housing 3 is equipped with inlet tube 31 and drain pipe 32, water
Slot 111 is connected to inlet tube 31 or drain pipe 32.Reaction solution on different height is extracted in the pump housing 3 out of autoclave body 1, then is arranged
Enter and in the reaction solution of different height, realizes quickly adequately contact mixing between the reaction solution of different height into autoclave body 1, improve
The reaction efficiency of reaction solution improves production efficiency.
Referring to Figures 1 and 2, corresponding inlet tube 31 is spaced setting with the outer ring 11 of corresponding drain pipe 32 in the vertical direction.
Facilitate and the upper reaction solution of each height equably extracted or discharged, then uniform discharge is into the reaction solution of each height,
Make to come into full contact between the reaction solution of each height, improves reaction efficiency.
Referring to Fig. 2 and Fig. 3, the projection of through-hole 12 in the horizontal plane in adjacent outer ring 11 is arranged in a staggered manner, in the present embodiment,
Four through-holes 12 in adjacent outer ring 11 are mutually set to 90 degrees.It prevents from holding the extraction of reaction solution and discharge between adjacent outer ring 11
Circuit is easily constituted, reaction efficiency is improved.
Referring to Fig. 3, the horizontal container inner tube 4 towards 1 center line of autoclave body, stirrer paddle 22 and kettle inner tube are communicated at through-hole 12
4 interval settings, kettle inner tube 4 is closed at one end far from through-hole 12, and two are arranged along the axial direction of on 4 periphery wall of kettle inner tube in kettle
The liquid separating port 41 in outside in pipe 4, in the present embodiment, outer peripheral surface of the liquid separating port 41 completely through kettle inner tube 4.It will extract and discharge is anti-
It answers the position of liquid that the different position of autoclave body 1 is set, the reaction solution of different location in autoclave body 1 is made to react more uniform, improve anti-
Answer the general reaction efficiency in kettle.
Referring to Fig. 3, the opening of liquid separating port 41 is arranged along the vertical direction.Liquid separating port 41 is provided with along the vertical direction to be conducive to change it
Above or below stirrer paddle 22 at reaction solution environment, the reaction solution at this is extracted or is discharged other reaction
Liquid improves reaction efficiency.
Referring to Fig. 4, due to needing to guarantee the position of liquid separating port 41, the mode being directly connected through a screw thread is difficult to ensure liquid separation
Mouthfuls 41 it is vertical, so, kettle inner tube 4 is equipped with rectangular prism block 42 close to one end outer peripheral surface of 1 side wall of autoclave body, in autoclave body 1
It is correspondingly provided with mounting base 13 on side wall, is equipped with the rib hole 131 to match with prism block 42 in mounting base 13, mounting base 13 is equipped with
For fixing the fixing piece of position between prism block 42 and rib hole 131.The cooperation in prism block 42 and rib hole 131 limits kettle inner tube 4
Radial movement and rotation, then the position by the fixed kettle inner tube 4 of fixing piece.
Referring to Fig. 4, mounting base 13 is that cylindric and its outer peripheral surface is equipped with screw thread (not shown), and fixing piece includes spiral shell
Line is connected to the sleeve 132 outside mounting base 13, and sleeve 132 is connected to prism block 42 far from the inner sidewall of 1 side wall one end of autoclave body
End face.Sleeve 132 limits the moving along its axial direction of kettle inner tube 4, and rises to the gap between prism block 42 and rib hole 131 certain close
Seal effect.
The course of work is summarized:
Reaction solution on different height is extracted in the pump housing 3 out of autoclave body 1, then is drained into different height in autoclave body 1
In reaction solution, the process of the extraction and discharge all passes through the liquid separating port 41 opened up in kettle inner tube 4 and carries out, and realizes the anti-of different height
Quickly adequately contact mixing between liquid is answered, the reaction solution of the different height in autoclave body 1 is sufficiently mixed, its life is improved
Produce efficiency.
The above is only the preferred embodiment of the utility model, and the protection scope of the utility model is not limited merely to
Above-described embodiment, technical solution belonging to the idea of the present invention belong to the protection scope of the utility model.It should refer to
Out, for those skilled in the art, it is without departing from the principle of the utility model it is several improvement and
Retouching, these improvements and modifications also should be regarded as the protection scope of the utility model.
Claims (8)
1. a kind of reagent production reaction kettle, including autoclave body (1), the autoclave body (1) is interior to be equipped with agitating device, it is characterised in that:
Its short transverse of autoclave body (1) outer is fitted with outer ring (11), is provided with sink (111) on outer ring (11) inner peripheral surface,
Several through-holes (12) for being connected to sink (111) are provided on autoclave body (1) outer peripheral surface, the autoclave body (1) is externally connected with the pump housing
(3), the pump housing (3) is equipped with inlet tube (31) and drain pipe (32), and the sink (111) is connected to inlet tube (31) or drain
It manages (32).
2. a kind of reagent production reaction kettle according to claim 1, it is characterised in that: corresponding inlet tube (31) with it is corresponding
The outer ring (11) of drain pipe (32) is spaced setting in the vertical direction.
3. a kind of reagent production reaction kettle according to claim 2, it is characterised in that: the through-hole in adjacent outer ring (11)
(12) projection in the horizontal plane is arranged in a staggered manner.
4. a kind of reagent production reaction kettle according to claim 3, it is characterised in that: through-hole is communicated with direction at (12)
The kettle inner tube (4) of autoclave body (1) center line, the kettle inner tube (4) is closed at one end far from through-hole (12), and kettle inner tube (4) periphery wall
On be arranged along the axial direction of the liquid separating ports (41) in several outsides in kettle inner tube (4).
5. a kind of reagent production reaction kettle according to claim 4, it is characterised in that: liquid separating port (41) opening edge
Vertical direction setting.
6. a kind of reagent production reaction kettle according to claim 4, it is characterised in that: the kettle inner tube (4) is close to kettle
One end outer peripheral surface of body (1) side wall is equipped with prism block (42), is correspondingly provided with mounting base (13) on autoclave body (1) inner sidewall,
The rib hole (131) to match with prism block (42) is equipped in the mounting base (13), the mounting base (13) is equipped with for solid
Determine the fixing piece of position between prism block (42) and rib hole (131).
7. a kind of reagent production reaction kettle according to claim 6, it is characterised in that: the mounting base (13) is cylinder
Shape and its outer peripheral surface are equipped with screw thread, and fixing piece includes being threadedly connected to the sleeve (132) of mounting base (13) outside, the sleeve
(132) inner sidewall far from autoclave body (1) side wall one end is connected to the end face of prism block (42).
8. a kind of reagent production reaction kettle according to claim 1 or claim 7, it is characterised in that: autoclave body (1) internal perisporium
On along its short transverse be equipped with horizontal treadle (14), the treadle (14) is fixed on autoclave body (1) internal perisporium at U-shaped and its both ends.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821362957.0U CN208771417U (en) | 2018-08-22 | 2018-08-22 | Reaction kettle is used in a kind of production of reagent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821362957.0U CN208771417U (en) | 2018-08-22 | 2018-08-22 | Reaction kettle is used in a kind of production of reagent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208771417U true CN208771417U (en) | 2019-04-23 |
Family
ID=66158165
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821362957.0U Expired - Fee Related CN208771417U (en) | 2018-08-22 | 2018-08-22 | Reaction kettle is used in a kind of production of reagent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208771417U (en) |
-
2018
- 2018-08-22 CN CN201821362957.0U patent/CN208771417U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190423 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |