CN209530868U - A kind of etching solution black sulfuric acid copper reaction kettle - Google Patents

A kind of etching solution black sulfuric acid copper reaction kettle Download PDF

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Publication number
CN209530868U
CN209530868U CN201920125256.3U CN201920125256U CN209530868U CN 209530868 U CN209530868 U CN 209530868U CN 201920125256 U CN201920125256 U CN 201920125256U CN 209530868 U CN209530868 U CN 209530868U
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China
Prior art keywords
tank body
sieve plate
agitating shaft
etching solution
reaction kettle
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CN201920125256.3U
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Chinese (zh)
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陈通
崔文晶
范晨君
李报
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Suzhou Huafeng Environmental Protection Technology Co Ltd
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Suzhou Huafeng Environmental Protection Technology Co Ltd
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Abstract

The utility model discloses a kind of etching solution black sulfuric acid copper reaction kettles, are related to etching solution recovery processing technical field, it is intended to which the contact area for solving stirring rod and material is smaller, stirs not uniform enough, abundant problem.Its key points of the technical solution are that including tank body, feed inlet, discharge port and being plugged in the intracorporal agitating device of tank, agitating device includes the agitating shaft being inserted into from tank body top surface, the stirring blade being connected on agitating shaft and tank body top surface is arranged in for driving the motor of agitating shaft rotation, agitating shaft is also arranged with sieve plate far from one end of motor, several gear pieces are provided on sieve plate top surface, the guiding device that the vibration device of driving sieve plate vibration is additionally provided in tank body and vibrates up and down sieve plate along the vertical direction.Under the action of guiding device and vibration device, lower vibration, the area of contacting material when gear piece increases stirring achieve the purpose that make stirring more evenly sieve plate so that the material in reaction kettle is sufficiently mixed in the vertical direction.

Description

A kind of etching solution black sulfuric acid copper reaction kettle
Technical field
The utility model relates to the technical fields of etching solution recovery processing, more particularly, to a kind of etching solution black sulfuric acid copper Reaction kettle.
Background technique
Reaction kettle is widely used in petroleum, chemical industry, rubber, pesticide, dyestuff, medicine, field of food.Reaction kettle is comprehensive anti- Container is answered, dispersion mixing is carried out to various materials by stirring, heating, cooling, to carry out reactive polymeric.Its structure is general It is made of autoclave body, transmission device, agitating device, heating device, cooling device, sealing device.Print the etched production in battery plate road After generate a large amount of cupric spent etching solution.Etching solution has alkalinity and acid two major classes, and the processing method of etching waste liquor mainly includes Chemical precipitation method, flocculent precipitation, solvent extraction, recycling copper, copper sulphate etc..
Existing Authorization Notice No. is that the Chinese patent of CN206868206U discloses a kind of etching solution black sulfuric acid copper equipment, Including pedestal, the top of pedestal corresponds to two sides and is mounted on support base, and reaction kettle, the bottom of reaction kettle are equipped at the top of support base Portion is equipped with discharge nozzle, is equipped with the first solenoid valve on discharge nozzle, and the junction of reaction kettle and discharge nozzle is equipped with filter screen, instead Answer kettle on control panel is installed, display screen, control button and indicator light, the inside of control panel are installed on control panel Single-chip microcontroller is installed, the side of reaction kettle is equipped with etching solution inlet pipe, second solenoid valve, reaction kettle are equipped on etching solution inlet pipe The other side water inlet pipe is installed, third solenoid valve is installed on water inlet pipe, kettle cover, the top of kettle cover are installed at the top of reaction kettle Rotating electric machine is installed, the correspondence two sides of kettle cover pass through connecting tube and connect respectively with hydrochloric acid tank and sulphuric acid tank at portion center.
Prior art among the above have the following deficiencies: using aforesaid reaction vessel stirring material when, stirring rod with The contact area of material is smaller, and not enough uniformly, sufficiently, storeroom cannot react completely, therefore be further improved for stirring.
Utility model content
The purpose of the utility model is to provide a kind of etching solution black sulfuric acid copper reaction kettles, have stirring more uniform Effect.
The above-mentioned technical purpose of the utility model has the technical scheme that
A kind of etching solution black sulfuric acid copper reaction kettle including tank body, the feed inlet that is provided with tank body top surface, is provided with tank body The discharge port of bottom surface and it is plugged in the intracorporal agitating device of tank, the agitating device includes the stirring being inserted into from tank body top surface Axis, the stirring blade being connected on agitating shaft and be arranged in tank body top surface for drive agitating shaft rotate motor, it is described to stir It mixes axis and is also arranged with sieve plate far from one end of motor, circumferential equidistant interval is provided with several gear pieces on the sieve plate top surface, described The guiding device for being additionally provided with the vibration device of driving sieve plate vibration in tank body and vibrating up and down sieve plate along the vertical direction.
By using above-mentioned technical proposal, under the action of guiding device and vibration device, sieve plate in the vertical direction under Vibration, the area of contacting material when gear piece increases stirring improve stirring so that the material in reaction kettle is sufficiently mixed uniformly Mixing efficiency, so that reaction is more complete.
The utility model is further arranged to: the vibration device includes being fixed on active of the agitating shaft far from motor one end Bevel gear and the follower lever for being rotatably connected on inner tank wall, the follower lever is connected with far from one end of tank body and active conical tooth The driven wheel of differential of cooperation is taken turns, is arranged with cam on the follower lever, the lower surface of the sieve plate is fixedly connected with guide rod, described The bottom surface of guide rod is connected with the pulley abutted with cam;
Fixed cylinder is provided on the tank body inner sidewall, the drive bevel gear and driven wheel of differential are arranged at fixed cylinder Interior, the follower lever is fixedly installed the first limit being rotatablely connected between fixed cylinder side wall from the fixed cylinder side wall place of being pierced by Ring, the agitating shaft are fixedly installed the second limit being rotatablely connected between fixed cylinder roof from the fixed cylinder roof place of being pierced by Ring.
It by using above-mentioned technical proposal, drives drive bevel gear to rotate in a circumferential direction together when agitating shaft rotates, passes through actively Bevel gear drives driven wheel of differential rotation, so that follower lever be made to rotate, fixed cam also rotates on follower lever, cam rotation Meanwhile the pulley abutted with cam face is moved along cam face, to realize the up-down vibration of sieve plate.
The utility model is further arranged to: the guiding device includes two cunnings being symmetrically distributed on tank body inner sidewall Slot, the circumference side last week of the sieve plate, there are two the guide pads cooperated with sliding slot inlay card to equidistant interval connection.
By using above-mentioned technical proposal, due to the cooperation of guide pad and sliding slot, so that sieve plate makees one along vertical direction Fixed up-down vibration, sieve plate, which is not likely to produce, to rotate in a circumferential direction.More soft material, such as rubber pad can be used in guide pad.
The utility model is further arranged to: also circumferentially equidistant on the sieve plate bottom surface to be arranged at intervals with several gear pieces.
By using above-mentioned technical proposal, the area of contacting material when gear piece increases stirring, further such that reacting Material in kettle is sufficiently mixed uniformly, and raising is stirred efficiency, so that reaction is more complete.
The utility model is further arranged to: being arranged with several casings along agitating shaft length direction on the agitating shaft, often There are two stirring blade, the cross sectional shape of the stirring blade is T-shaped for circumferential equidistant interval connection in one described sleeve pipe.
By using above-mentioned technical proposal, since the cross-sectional shape of stirring blade is T-type, increase stirring blade rotation warp The region crossed, to increase the area of stirring blade contacting material, so that more materials are flowed by stirring blade two sides Power, achieve the effect that stir evenly.Agitating shaft length direction is provided with several stirring blades, so that each region in tank body Material is all stirred, and keeps material stirring uniform.In addition, the stirring blade high stability of T-type, extends the use of stirring blade Service life.
The utility model is further arranged to: the stirring blade in upper and lower two neighboring described sleeve pipe is interspersed.
By using above-mentioned technical proposal, the stirring blade on upper and lower adjacent two casings is interspersed, so that material stream By motive force when moving different location, further such that stirring evenly.
The utility model is further arranged to: being set on the stirring blade along the length direction equidistant interval of stirring blade It is equipped with several pillars.
By using above-mentioned technical proposal, the area of stirring blade contacting material is further increased, so that material stirring is more Add uniformly.
The utility model is further arranged to: adjacent pillar is interspersed on the same stirring blade.
By using above-mentioned technical proposal, so that material by the power flowed to different directions, futher stirs uniformly.
In conclusion the advantageous effects of the utility model are as follows:
1. passing through the setting of sieve plate and gear piece, under the action of guiding device and vibration device, sieve plate is in the vertical direction Lower vibration, the area of contacting material when gear piece increases stirring, so that the material in reaction kettle is sufficiently mixed uniformly, raising is stirred Mixing efficiency is mixed, so that reaction is more complete;
2. passing through the setting of T-type stirring blade, increases the region that stirring blade rotation is passed through, connect to increase stirring blade The area for touching material, so that material stirring is more uniform.
Detailed description of the invention
Fig. 1 is the overall structure diagram of the utility model embodiment.
Fig. 2 is the partial cutaway schematic view for showing reaction kettle internal structure;
Fig. 3 is the partial cutaway schematic view for showing vibration device internal structure;
Fig. 4 is the partial schematic diagram for showing stirring blade structure.
In figure, 1, tank body;11, feed inlet;12, discharge port;13, sliding slot;2, motor;3, agitating shaft;31, casing;4, it stirs Mix blade;41, pillar;42, bottom plate;43, plate;5, sieve plate;51, gear piece;52, guide rod;521, pulley;53, guide pad;6, Drive bevel gear;61, the second stop collar;7, driven wheel of differential;71, the first stop collar;8, follower lever;81, cam;9, fixed Cylinder.
Specific embodiment
The utility model is described in further detail below in conjunction with attached drawing.
It referring to Fig.1, is a kind of etching solution black sulfuric acid copper reaction kettle disclosed by the utility model, including tank made of enamel Body 1,1 top surface of tank body are provided with circular feed inlet 11, are hinged with cover board on feed inlet 11.Cover board is opened, it can be from feed inlet 11 are added reaction mass into tank body 1.1 bottom surface of tank body is provided with discharge port 12, and discharge port 12 is by valve control discharge port 12 Opening and closing.
Referring to Fig.1 with Fig. 4, agitating device is additionally provided in tank body 1, agitating device includes agitating shaft 3, motor 2 and connection Stirring blade 4 on agitating shaft 3.The top surface of tank body 1 is arranged in motor 2, for driving agitating shaft 3 to rotate in a circumferential direction.Agitating shaft 3 It is connected to the driving end of motor 2 and protrudes into tank body 1, in the present embodiment, the casing of four circular tube shapeds is arranged on agitating shaft 3 31.It is equipped with bolt on casing 31, casing 31 is fixed on agitating shaft 3 by bolt.Two are welded on a piece casing 31 to stir Blade 4 is mixed, stirring blade 4 is each perpendicular to the axially placed of agitating shaft 3, and 4 equidistant interval of stirring blade is distributed in the two of casing 31 Side.The cross sectional shape of stirring blade 4 is T-type, and stirring blade 4 includes a bottom plate 42 and the plate 43 perpendicular to bottom plate 42, is inserted Plate 43 is arranged along the length direction of bottom plate 42, and plate 43 is located at the centre of bottom plate 42 and length is equal with bottom plate 42.Same root set The placement direction of two plates 43 of the stirring blade 4 on pipe 31 is opposite.Stirring blade 4 on upper and lower adjacent two casings 31 It is interspersed.Stirring blade 4 is designed it is T-shaped, increase stirring blade 4 rotate when and material contact area, promote material again It is uniformly mixed in reaction kettle, improves stirring efficiency.Several pillars are welded with along the length direction of stirring blade 4 on bottom plate 42 41, pillar 41 is also connected on plate 43, and the pillar 41 on bottom plate 42 is interspersed with the pillar 41 on plate 43, further Increase stirring blade 4 rotate when and material contact area.
Referring to Fig. 2 and Fig. 3, the one end of agitating shaft 3 far from motor 2 also movable sleeve is equipped with sieve plate 5, and sieve plate 5 is rounded and sieves Several through-holes are distributed in 5 surface of plate.It is circumferentially equidistant on 5 top and bottom of sieve plate to be arranged at intervals with several gear pieces 51, gear piece 51 Section it is triangular in shape.Be additionally provided in tank body 1 driving sieve plate 5 vibrate vibration device and make sieve plate 5 along the vertical direction on The guiding device of lower vibration.Vibration device includes the drive bevel gear 6 being fixed on agitating shaft 3 and is rotatably connected on tank body 1 The follower lever 8 of inner wall, drive bevel gear 6 are located at the end of agitating shaft 3.Follower lever 8 is connected with and active far from one end of tank body 1 The driven wheel of differential 7 that bevel gear 6 cooperates is connected with fixed cylinder 9 by the bar of two rectangles on 1 inner sidewall of tank body, and fixed cylinder 9 is in It is rectangular-shaped.Drive bevel gear 6 and driven wheel of differential 7 are arranged at fixed cylinder 9, in order to enable drive bevel gear 6 always with it is driven Bevel gear 7 keeps engagement, and follower lever 8 is fixedly installed the first rounded limit of a section from the 9 side wall place of being pierced by of fixed cylinder Ring 71 is rotatablely connected between 9 side wall of first stop collar 71 and fixed cylinder, and agitating shaft 3 is fixedly installed from the 9 roof place of being pierced by of fixed cylinder There is the second stop collar 61 that a section is rounded, is rotatablely connected between 9 roof of the second stop collar 61 and fixed cylinder.Follower lever 8 On be arranged with cam 81, drive drive bevel gear 6 to rotate in a circumferential direction together when agitating shaft 3 rotates, by drive bevel gear 6 drive from Dynamic bevel gear 7 rotates, so that follower lever 8 be made to rotate, fixed cam 81 also rotates on follower lever 8.The lower surface of sieve plate 5 is fixed It is welded with guide rod 52, guide rod 52 is cylindrical.The bottom surface of guide rod 52 is connected with pulley 521, and pulley 521 is abutted with cam 81, convex While 81 rotation of wheel, the pulley 521 abutted with 81 surface of cam is moved along 81 surface of cam, to realize the upper of sieve plate 5 Lower vibration.
Referring to Fig. 2 and Fig. 3, guiding device includes two sliding slots 13 being symmetrically distributed on 1 inner sidewall of tank body, sliding slot 13 Rectangular in cross-section, there are two the guide pad 53 with the cooperation of 13 inlay card of sliding slot, two guide pads 53 for connection on the circumference side of sieve plate 5 About the central symmetry of sieve plate 5, when the lower vibration in the vertical direction of sieve plate 5, guide pad 53 is also moved up and down in sliding slot 13 And without departing from sliding slot 13, so that sieve plate 5 is not likely to produce and rotates in a circumferential direction.More soft material can be used in guide pad 53, Such as rubber.
The implementation principle of the present embodiment are as follows: open cover board, reaction mass is added into tank body 1 from feed inlet 11, then shut Cover board.
Start motor 2, the generation of agitating shaft 3 rotates in a circumferential direction, and since the cross-sectional shape of stirring blade 4 is T-type, increases stirring The region that the rotation of blade 4 is passed through, to increase the area of 4 contacting material of stirring blade, so that the material stirring in tank body 1 is more equal It is even.
It drives drive bevel gear 6 to rotate in a circumferential direction together when agitating shaft 3 rotates, is driven by drive bevel gear 6 from mantle tooth 7 rotation of wheel, so that follower lever 8 be made to rotate, fixed cam 81 also rotates on follower lever 8.While cam 81 rotates, with cam The pulley 521 that 81 surfaces abut is moved along 81 surface of cam, to realize the up-down vibration of sieve plate 5.Sieve plate 5 is in vertical direction It vibrates up and down, the area of 5 contacting material of sieve plate, promotes the flowing of material when gear piece 51 increases stirring, so that in reaction kettle Interior material is sufficiently mixed uniformly, and raising is stirred efficiency, so that reaction is more complete.
The embodiment of present embodiment is the preferred embodiment of the utility model, and not limitation is originally practical new according to this The protection scope of type, therefore: the equivalence changes that all structures, shape, principle according to the utility model are done should all be covered by practical Within novel protection scope.

Claims (8)

1. a kind of etching solution black sulfuric acid copper reaction kettle, including tank body (1), the feed inlet (11) that is provided with tank body (1) top surface, open The agitating device for being located at the discharge port (12) of tank body (1) bottom surface and being plugged in tank body (1), the agitating device include from tank The agitating shaft (3) of body (1) top surface insertion, the stirring blade (4) being connected on agitating shaft (3) and setting are in tank body (1) top surface Motor (2) for driving agitating shaft (3) to rotate, it is characterised in that: the agitating shaft (3) also covers far from the one end of motor (2) Equipped with sieve plate (5), circumferential equidistant interval is provided with several gear pieces (51) on sieve plate (5) top surface, is also set in the tank body (1) The guiding device for being equipped with the vibration device of driving sieve plate (5) vibration and vibrating up and down sieve plate (5) along the vertical direction.
2. a kind of etching solution black sulfuric acid copper reaction kettle according to claim 1, it is characterised in that: the vibration device packet Include be fixed on agitating shaft (3) far from motor (2) one end drive bevel gear (6) and be rotatably connected on tank body (1) inner wall from Lever (8), the follower lever (8) are connected with the driven wheel of differential with drive bevel gear (6) cooperation far from the one end of tank body (1) (7), it is arranged with cam (81) on the follower lever (8), the lower surface of the sieve plate (5) is fixedly connected with guide rod (52), described The bottom surface of guide rod (52) is connected with the pulley (521) abutted with cam (81);
It is provided with fixed cylinder (9) on tank body (1) inner sidewall, the drive bevel gear (6) and driven wheel of differential (7) are respectively provided with In fixed cylinder (9), the follower lever (8) is fixedly installed between fixed cylinder (9) side wall from fixed cylinder (9) side wall place of being pierced by The first stop collar (71) of rotation connection, the agitating shaft (3) is fixedly installed from fixed cylinder (9) roof place of being pierced by and fixed cylinder (9) the second stop collar (61) being rotatablely connected between roof.
3. a kind of etching solution black sulfuric acid copper reaction kettle according to claim 2, it is characterised in that: the guiding device packet Include two sliding slots (13) being symmetrically distributed on tank body (1) inner sidewall, circumference side last week of the sieve plate (5) is to equidistant interval There are two the guide pads (53) with the cooperation of sliding slot (13) inlay card for connection.
4. a kind of etching solution black sulfuric acid copper reaction kettle according to claim 1, it is characterised in that: sieve plate (5) bottom It is also circumferentially equidistant on face to be arranged at intervals with several gear pieces (51).
5. a kind of etching solution black sulfuric acid copper reaction kettle according to claim 1, it is characterised in that: the agitating shaft (3) On be arranged with several casings (31) along agitating shaft (3) length direction, circumferential equidistant interval is connected on each described sleeve pipe (31) The cross sectional shape of two stirring blades (4), the stirring blade (4) is T-shaped.
6. a kind of etching solution black sulfuric acid copper reaction kettle according to claim 5, it is characterised in that: upper and lower two neighboring Stirring blade (4) in described sleeve pipe (31) is interspersed.
7. a kind of etching solution black sulfuric acid copper reaction kettle according to claim 6, it is characterised in that: the stirring blade (4) the length direction equidistant interval of stirring blade (4) is provided with several pillars (41) on.
8. a kind of etching solution black sulfuric acid copper reaction kettle according to claim 7, it is characterised in that: the same paddle Adjacent pillar (41) is interspersed on piece (4).
CN201920125256.3U 2019-01-24 2019-01-24 A kind of etching solution black sulfuric acid copper reaction kettle Active CN209530868U (en)

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CN201920125256.3U CN209530868U (en) 2019-01-24 2019-01-24 A kind of etching solution black sulfuric acid copper reaction kettle

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116809003A (en) * 2023-08-29 2023-09-29 江苏科伦多食品配料有限公司 Efficient neutralization equipment for potassium citrate production
CN117259196A (en) * 2023-09-25 2023-12-22 四川沃耐稀新材料科技有限公司 Lanthanum chloride cooling crystallization screening plant

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116809003A (en) * 2023-08-29 2023-09-29 江苏科伦多食品配料有限公司 Efficient neutralization equipment for potassium citrate production
CN117259196A (en) * 2023-09-25 2023-12-22 四川沃耐稀新材料科技有限公司 Lanthanum chloride cooling crystallization screening plant
CN117259196B (en) * 2023-09-25 2024-02-06 四川沃耐稀新材料科技有限公司 Lanthanum chloride cooling crystallization screening plant

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