CN208733242U - A kind of novel fluorination electrolytic cell - Google Patents
A kind of novel fluorination electrolytic cell Download PDFInfo
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- CN208733242U CN208733242U CN201821309199.6U CN201821309199U CN208733242U CN 208733242 U CN208733242 U CN 208733242U CN 201821309199 U CN201821309199 U CN 201821309199U CN 208733242 U CN208733242 U CN 208733242U
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- autoclave body
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Abstract
The utility model relates to the technical fields of the electrolytic cell of Organic Electrochemical Synthesis, more particularly to a kind of novel fluorination electrolytic cell；Including autoclave body, two groups of kettle covers, two groups of handles, multiple groups anode electrolysis plate, multiple groups catholyte plate, anode plate and cathode plate, reaction placed cavity is provided in autoclave body, autoclave body top left side is provided with and communicated with the first reaction and picks and places mouth, autoclave body top right side is provided with and communicated with the second reaction and picks and places mouth, multiple groups anode slot is provided with and communicated on anode plate, multiple groups cathode can is provided with and communicated on cathode plate, autoclave body left side wall top and right side wall top are step-like；It further include stirring motor, speed reducer, support frame, shaft coupling, stirring rod, two groups of bearings, two groups of baffles and multiple groups paddle, multiple groups paddle is uniformly connected on stirring rod lateral wall, lower bearing slot is provided on downside wall in reaction placed cavity, upper bearing (metal) slot is provided with and communicated in autoclave body side wall, output end of reducer at the top of shaft coupling and stirring rod by connecting.
Description
Technical field
The utility model relates to the technical fields of the electrolytic cell of Organic Electrochemical Synthesis, more particularly to a kind of novel fluorination
Electrolytic cell.
Background technique
It is well known that a kind of novel fluorination electrolytic cell is a kind of device for being used to prepare perfluoro-compound, in organic electrification
It learns and is widely used in a variety of applications in the field of the electrolytic cell of synthesis；Existing novel fluorination electrolytic cell includes groove body, anode conducting
Plate and cathode conductive plate are provided with electrolysis placed cavity in groove body, and are provided with and communicated with electrolysis at the top of groove body and pick and place mouth, anode conducting
Plate is located at left side in electrolysis placed cavity, and cathode conductive plate is located on the right side of electrolysis placed cavity；Existing novel fluorination electrolytic cell uses
When by raw material be put into electrolysis placed cavity in, be powered to anode conducting plate and cathode conductive plate；Existing novel fluorination
It is found in electrolytic cell use, conductive plate surface area is smaller to cause electrolytic efficiency lower；And device without mixing will lead to electrolysis not
Sufficiently.
Utility model content
In order to solve the above technical problems, the utility model provides, a kind of contact area is larger to be improved efficiency；And there is stirring
The novel fluorination electrolytic cell of device raising electrolysis degree.
The novel fluorination electrolytic cell of the utility model, including autoclave body, two groups of kettle covers, two groups of handles, multiple groups anode electrolysis plate,
Multiple groups catholyte plate, anode plate and cathode plate are provided with reaction placed cavity in autoclave body, and autoclave body top left side is provided with and communicated with
One reaction picks and places mouth, and autoclave body top right side is provided with and communicated with the second reaction and picks and places mouth, and two groups of kettle covers are respectively hinged at the first reaction
It picks and places on the right side of mouth and the second reaction picks and places on the left of mouth, two groups of handles are connected at the top of two groups of kettle covers, are connected to and are set on anode plate
It is equipped with multiple groups anode slot, multiple groups anode electrolysis board bottom portion is each passed through multiple groups anode slot and stretches in reaction placed cavity, cathode plate
On be provided with and communicated with multiple groups cathode can, multiple groups catholyte board bottom portion is each passed through multiple groups cathode can and stretches to reaction placed cavity
Interior, anode plate is located at the kettle cover bottom for being located at left side in two groups of kettle covers, and cathode plate is located at the kettle cover for being located at right side in two groups of kettle covers
Bottom, autoclave body left side wall top and right side wall top are step-like, and autoclave body side wall left end and right side are step-like, sun
Pole plate bottom and autoclave body left side wall top and kettle cover side wall left end, cathode plate bottom and autoclave body right side wall top and kettle cover top side
Wall right end；It further include stirring motor, speed reducer, support frame, shaft coupling, stirring rod, two groups of bearings, two groups of baffles and multiple groups stirring
Leaf, multiple groups paddle are uniformly connected on stirring rod lateral wall, and stirring rod is located in reaction placed cavity, react bottom side in placed cavity
Be provided with lower bearing slot on wall, be provided with and communicated with upper bearing (metal) slot in autoclave body side wall, two groups of bearings be located at upper bearing (metal) slot and
In lower bearing slot, stirring rod bottom is connected in two groups of bearings in the bearing of bottom, and two groups of bearings are passed through at the top of stirring rod
In be located at the bearing at top and stretch out at the top of autoclave body, support frame bottom is connected at the top of autoclave body, and support frame is being located at upper bearing (metal) slot just
Top, stirring motor are located at the top of autoclave body, and stirring motor output end is connect with speed reducer input terminal, and output end of reducer passes through connection
It is connect at the top of axis device and stirring rod.
The novel fluorination electrolytic cell of the utility model, further includes discharge nozzle, and discharging seal of tube connection is mounted on autoclave body bottom.
The novel fluorination electrolytic cell of the utility model is provided with and communicated with Plastic valve on discharge nozzle.
The novel fluorination electrolytic cell of the utility model, further includes four groups of supporting legs, and four groups of supporting legs are connected to autoclave body bottom
Front left side, left rear side, forward right side and right lateral side.
The novel fluorination electrolytic cell of the utility model further includes four groups of adjustable bases, difference spiral shell at the top of four groups of adjustable bases
Mounted in four groups of supporting leg bottoms.
The novel fluorination electrolytic cell of the utility model further includes transparent panel, and peep hole is provided on autoclave body rear wall, transparent
Plate is sealingly mounted in peep hole.
The novel fluorination electrolytic cell of the utility model, reaction place and are provided with erosion resistant coating on chamber inner sidewall.
The novel fluorination electrolytic cell of the utility model is provided with line slot, anode electrode and cathode electricity on two groups of kettle covers
Pole passes through two groups of line slots respectively and connect with external power supply anode and cathode.
The novel fluorination electrolytic cell of the utility model, positive pole and cathode are parallel with voltmeter.
Compared with prior art the utility model has the following beneficial effects: holding reaction raw materials by autoclave body, support device is each
Portion's component supports multiple groups anode electrolysis plate by anode plate, has gap, and multiple groups anode electrolysis board bottom portion between multiple groups anode slot
It will not contact with each other, multiple groups catholyte plate is supported by cathode plate, has gap, and multiple groups catholyte between multiple groups cathode can
Board bottom portion will not contact with each other, and be located at the kettle cover in left side in two groups of kettle covers by opening, can be by anode plate and multiple groups anode electricity
Solution plate takes out out of reaction placed cavity together, so as to carry out cleaning work to multiple groups anode electrolysis plate surface, passes through opening
It is located at the kettle cover on right side in two groups of kettle covers, cathode plate and multiple groups catholyte plate can be taken out out of reaction placed cavity together,
So as to carry out cleaning work to multiple groups catholyte plate surface, it can be convenient by two groups of handles and open two groups of kettles respectively
Lid, and two groups of kettle cover sealing covers pick and place mouth mounted in the first reaction and the second reaction picks and places mouth, can prevent former in reaction placed cavity
Material leakage；There is provided power by stirring motor drives speed reducer to be rotated, and stirring motor is the common electrical part in market, and buying back makes
Used time, which only needs to be electrically connected to specifications, can carry out using therefore details are not described herein, can reduce revolving speed by speed reducer, prevents
Only high-speed rotation causes the strenuous exercise of raw material to damage multiple groups anode electrolysis plate and multiple groups catholyte plate, passes through shaft coupling
Output end of reducer is connect by device with stirring rod top, is rotated by stirring rod and multiple groups paddle is driven to be stirred raw material,
Keep cell reaction more complete.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is autoclave body complete section schematic perspective view；
It is attached marked in the figure: 1, autoclave body；2, kettle cover；3, handle；4, anode electrolysis plate；5, catholyte plate；6, anode plate；7,
Cathode plate；8, stirring motor；9, speed reducer；10, support frame；11, shaft coupling；12, stirring rod；13, bearing；14, baffle；15,
Paddle；16, discharge nozzle；17, Plastic valve；18, supporting leg；19, adjustable base；20, transparent panel.
Specific embodiment
With reference to the accompanying drawings and examples, specific embodiment of the present utility model is described in further detail.Below
Embodiment is not intended to limit the scope of the present invention for illustrating the utility model.
As depicted in figs. 1 and 2, the novel fluorination electrolytic cell of the utility model, including 1, two group of autoclave body, 2, two groups of kettle cover handle
Hand 3, multiple groups anode electrolysis plate 4, multiple groups catholyte plate 5, anode plate 6 and cathode plate 7 are provided with reaction placed cavity in autoclave body,
Autoclave body top left side be provided with and communicated with the first reaction pick and place mouth, autoclave body top right side be provided with and communicated with the second reaction pick and place mouth, two
Group kettle cover is respectively hinged on the right side of the first reaction pick-and-place mouth and the second reaction picks and places mouth left side, and two groups of handles are connected to two groups
At the top of kettle cover, it is provided with and communicated with multiple groups anode slot on anode plate, multiple groups anode electrolysis board bottom portion is each passed through multiple groups anode slot and stretches
Enter to reaction placed cavity, multiple groups cathode can is provided with and communicated on cathode plate, multiple groups catholyte board bottom portion is each passed through multiple groups
Cathode can stretches in reaction placed cavity, and anode plate is located at the kettle cover bottom for being located at left side in two groups of kettle covers, and cathode plate is located at two
It is located at the kettle cover bottom on right side in group kettle cover, autoclave body left side wall top and right side wall top are step-like, and autoclave body side wall
Left end and right side are step-like, anode plate bottom and autoclave body left side wall top and kettle cover side wall left end, cathode plate bottom with
Autoclave body right side wall top and kettle cover side wall right end；It further include stirring motor 8, speed reducer 9, support frame 10, shaft coupling 11, stirring
12, two groups of bar, 13, two groups of bearing baffle 14 and multiple groups paddle 15, multiple groups paddle are uniformly connected on stirring rod lateral wall,
Stirring rod is located in reaction placed cavity, reacts in placed cavity and is provided with lower bearing slot on downside wall, is connected to and sets in autoclave body side wall
It is equipped with upper bearing (metal) slot, two groups of bearings are located in upper bearing (metal) slot and lower bearing slot, and stirring rod bottom is connected in two groups of bearings
It passes through and is located at the top of the bearing stretching autoclave body at top in two groups of bearings in the bearing of bottom, at the top of stirring rod, support frame bottom
Portion is connected at the top of autoclave body, and support frame is located at right above upper bearing (metal) slot, and stirring motor is located at the top of autoclave body, stirring motor output
End is connect with speed reducer input terminal, and output end of reducer at the top of shaft coupling and stirring rod by connecting；By holding reaction raw materials,
Each portion's component of support device supports multiple groups anode electrolysis plate by anode plate, has gap, and multiple groups anode between multiple groups anode slot
Electrolytic zinc-coated steel sheet bottom will not contact with each other, and support multiple groups catholyte plate by cathode plate, have gap between multiple groups cathode can, and more
Group catholyte board bottom portion will not contact with each other, and be located at the kettle cover in left side in two groups of kettle covers by opening, can by anode plate and
Multiple groups anode electrolysis plate takes out out of reaction placed cavity together, so as to carry out fettler to multiple groups anode electrolysis plate surface
Make, is located at the kettle cover on right side in two groups of kettle covers by opening, cathode plate and multiple groups catholyte plate can be put from reaction together
Intracavitary taking-up is set, so as to carry out cleaning work to multiple groups catholyte plate surface, can be convenient difference by two groups of handles
Two groups of kettle covers are opened, and two groups of kettle cover sealing covers pick and place mouth mounted in the first reaction and the second reaction picks and places mouth, can prevent from reacting
Raw material leaks in placed cavity；There is provided power by stirring motor drives speed reducer to be rotated, and stirring motor is the common electricity in market
Device, only needing to be electrically connected to specifications when buying back use can carry out using therefore details are not described herein, can be with by speed reducer
Revolving speed is reduced, prevents high-speed rotation from the strenuous exercise of raw material being caused to cause to damage to multiple groups anode electrolysis plate and multiple groups catholyte plate
It is bad, output end of reducer is connect with stirring rod top by shaft coupling, is rotated by stirring rod and drives multiple groups paddle to original
Material is stirred, and keeps cell reaction more complete.
The novel fluorination electrolytic cell of the utility model further includes discharge nozzle 16, and discharging seal of tube connection is mounted on autoclave body bottom
Portion；The product after electrolysis can be discharged by discharge nozzle.
The novel fluorination electrolytic cell of the utility model is provided with and communicated with Plastic valve 17 on discharge nozzle；By being closed plastics
Valve prevents raw material from leaking, and opens Plastic valve and product is discharged, and is that plastic material prevents corrosion of the raw material to valve by valve.
The novel fluorination electrolytic cell of the utility model, further includes four groups of supporting legs 18, and four groups of supporting legs are connected to autoclave body bottom
Front left side, left rear side, forward right side and the right lateral side in portion；Autoclave body can be supported by four groups of supporting legs, for the bottom of the tube that discharges
Space is provided.
The novel fluorination electrolytic cell of the utility model further includes four groups of adjustable bases 19, difference at the top of four groups of adjustable bases
It is screwed on four groups of supporting leg bottoms；By the height of the adjustable four groups of supporting legs of four groups of adjustable bases, autoclave body is made to be adjusted to horizontal position,
Facilitate the amount of raw material in observing response placed cavity.
The novel fluorination electrolytic cell of the utility model further includes transparent panel 20, peep hole is provided on autoclave body rear wall, thoroughly
Isotropic disk is sealingly mounted in peep hole；It can be with working condition in observing response placed cavity by transparent panel.
The novel fluorination electrolytic cell of the utility model, reaction place and are provided with erosion resistant coating on chamber inner sidewall；Pass through erosion resistant coating
It can prevent raw material from extending the service life of autoclave body to the corrosion of autoclave body.
The novel fluorination electrolytic cell of the utility model is provided with line slot, anode electrode and cathode electricity on two groups of kettle covers
Pole passes through two groups of line slots respectively and connect with external power supply anode and cathode；By two groups of line slots can be convenient anode electrode and
Cathode electrode is connect with positive pole and cathode.
The novel fluorination electrolytic cell of the utility model, positive pole and cathode are parallel with voltmeter；It can be with by voltmeter
It shows decomposition voltage, when voltage is bigger than normal or less than normal, so that voltage is in proper range by adjusting power supply, improve electrolytic efficiency.
The novel fluorination electrolytic cell of the utility model holds reaction raw materials by autoclave body, support device is each at work
Portion's component supports multiple groups anode electrolysis plate by anode plate, has gap, and multiple groups anode electrolysis board bottom portion between multiple groups anode slot
It will not contact with each other, multiple groups catholyte plate is supported by cathode plate, has gap, and multiple groups catholyte between multiple groups cathode can
Board bottom portion will not contact with each other, and be located at the kettle cover in left side in two groups of kettle covers by opening, can be by anode plate and multiple groups anode electricity
Solution plate takes out out of reaction placed cavity together, so as to carry out cleaning work to multiple groups anode electrolysis plate surface, passes through opening
It is located at the kettle cover on right side in two groups of kettle covers, cathode plate and multiple groups catholyte plate can be taken out out of reaction placed cavity together,
So as to carry out cleaning work to multiple groups catholyte plate surface, it can be convenient by two groups of handles and open two groups of kettles respectively
Lid, and two groups of kettle cover sealing covers pick and place mouth mounted in the first reaction and the second reaction picks and places mouth, can prevent former in reaction placed cavity
Material leakage；There is provided power by stirring motor drives speed reducer to be rotated, and stirring motor is the common electrical part in market, and buying back makes
Used time, which only needs to be electrically connected to specifications, can carry out using therefore details are not described herein, can reduce revolving speed by speed reducer, prevents
Only high-speed rotation causes the strenuous exercise of raw material to damage multiple groups anode electrolysis plate and multiple groups catholyte plate, passes through shaft coupling
Output end of reducer is connect by device with stirring rod top, is rotated by stirring rod and multiple groups paddle is driven to be stirred raw material,
Keep cell reaction more complete；The product after electrolysis can be discharged by discharge nozzle；Prevent raw material from leaking by being closed Plastic valve,
It opens Plastic valve and product is discharged, be that plastic material prevents corrosion of the raw material to valve by valve；It can be with by four groups of supporting legs
Autoclave body is supported, provides space for discharging bottom of the tube；By the height of the adjustable four groups of supporting legs of four groups of adjustable bases, make
Autoclave body is adjusted to horizontal position, facilitates the amount of raw material in observing response placed cavity；It can be in observing response placed cavity by transparent panel
Working condition；It can prevent raw material from extending the service life of autoclave body to the corrosion of autoclave body by erosion resistant coating；Pass through two groups of line slots
It can be convenient anode electrode and cathode electrode connect with positive pole and cathode；Decomposition voltage can be shown by voltmeter, when
When voltage is bigger than normal or less than normal, so that voltage is in proper range by adjusting power supply, improve electrolytic efficiency.
The above is only the preferred embodiment of the utility model, it is noted that for the common skill of the art
For art personnel, without deviating from the technical principle of the utility model, several improvements and modifications can also be made, these change
It also should be regarded as the protection scope of the utility model into modification.
Claims (9)
1. a kind of novel fluorination electrolytic cell, which is characterized in that including autoclave body (1), two groups of kettle covers (2), two groups of handles (3), multiple groups
Anode electrolysis plate (4), multiple groups catholyte plate (5), anode plate (6) and cathode plate (7), autoclave body (1) is interior to be provided with reaction placement
Chamber, autoclave body (1) top left side are provided with and communicated with the first reaction and pick and place mouth, and autoclave body (1) top right side is provided with and communicated with the second reaction
Mouth is picked and placed, two groups of kettle covers (2) are respectively hinged on the right side of the first reaction pick-and-place mouth and the second reaction picks and places mouth left side, two groups of handles
(3) it is connected at the top of two groups of kettle covers (2), is provided with and communicated with multiple groups anode slot, multiple groups anode electrolysis plate on anode plate (6)
(4) bottom is each passed through multiple groups anode slot and stretches in reaction placed cavity, and cathode plate is provided with and communicated with multiple groups cathode can on (7),
Multiple groups catholyte plate (5) bottom is each passed through multiple groups cathode can and stretches in reaction placed cavity, and anode plate (6) is located at two groups of kettles
It covering in (2) and is located at kettle cover (2) bottom in left side, cathode plate (7) is located at kettle cover (2) bottom for being located at right side in two groups of kettle covers (2),
Autoclave body (1) left side wall top and right side wall top be it is step-like, and autoclave body (1) side wall left end and right side be it is step-like,
Anode plate (6) bottom and autoclave body (1) left side wall top and kettle cover (2) side wall left end, cathode plate (7) bottom and autoclave body (1) are right
Side wall top and kettle cover (2) side wall right end；It further include stirring motor (8), speed reducer (9), support frame (10), shaft coupling
(11), stirring rod (12), two groups of bearings (13), two groups of baffles (14) and multiple groups paddle (15), multiple groups paddle (15) are uniform
It is connected on stirring rod (12) lateral wall, stirring rod (12) is located in reaction placed cavity, reacts in placed cavity and is arranged on downside wall
There is lower bearing slot, upper bearing (metal) slot is provided with and communicated in autoclave body (1) side wall, two groups of bearings (13) are located at upper bearing (metal) slot under
In bearing groove, stirring rod (12) bottom is connected in two groups of bearings (13) in the bearing (13) of bottom, stirring rod (12) top
Portion, which passes through, to be located at the top of bearing (13) stretching autoclave body (1) at top in two groups of bearings (13), and support frame (10) bottom is connected to kettle
At the top of body (1), and support frame (10) is located at right above upper bearing (metal) slot, and stirring motor (8) is located at the top of autoclave body (1), stirring motor
(8) output end is connect with speed reducer (9) input terminal, and speed reducer (9) output end passes through shaft coupling (11) and stirring rod (12) top
Connection.
2. novel fluorination electrolytic cell as described in claim 1, which is characterized in that further include discharge nozzle (16), discharge nozzle (16)
Sealing connection is mounted on autoclave body (1) bottom.
3. novel fluorination electrolytic cell as claimed in claim 2, which is characterized in that discharge nozzle is provided with and communicated with plastic valve on (16)
Door (17).
4. novel fluorination electrolytic cell as claimed in claim 3, which is characterized in that further include four groups of supporting legs (18), four groups of supporting legs
(18) front left side, left rear side, forward right side and the right lateral side of autoclave body (1) bottom are connected to.
5. novel fluorination electrolytic cell as claimed in claim 4, which is characterized in that it further include four groups of adjustable bases (19), four groups
It is screwed on four groups of supporting leg (18) bottoms respectively at the top of adjustable base (19).
6. novel fluorination electrolytic cell as claimed in claim 5, which is characterized in that further include transparent panel (20), autoclave body (1) rear side
Peep hole is provided on wall, transparent panel (20) is sealingly mounted in peep hole.
7. novel fluorination electrolytic cell as claimed in claim 6, which is characterized in that reaction places and is provided with anti-corrosion on chamber inner sidewall
Layer.
8. novel fluorination electrolytic cell as claimed in claim 7, which is characterized in that it is provided with line slot on two groups of kettle covers (2),
Anode electrode and cathode electrode pass through two groups of line slots respectively and connect with external power supply anode and cathode.
9. novel fluorination electrolytic cell as claimed in claim 8, which is characterized in that positive pole and cathode are parallel with voltmeter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821309199.6U CN208733242U (en) | 2018-08-14 | 2018-08-14 | A kind of novel fluorination electrolytic cell |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821309199.6U CN208733242U (en) | 2018-08-14 | 2018-08-14 | A kind of novel fluorination electrolytic cell |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208733242U true CN208733242U (en) | 2019-04-12 |
Family
ID=66029503
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821309199.6U Expired - Fee Related CN208733242U (en) | 2018-08-14 | 2018-08-14 | A kind of novel fluorination electrolytic cell |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208733242U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110777392A (en) * | 2019-12-03 | 2020-02-11 | 陈雨 | Stirring type fluorination electrolytic tank |
-
2018
- 2018-08-14 CN CN201821309199.6U patent/CN208733242U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110777392A (en) * | 2019-12-03 | 2020-02-11 | 陈雨 | Stirring type fluorination electrolytic tank |
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190412 Termination date: 20190814 |
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| CF01 | Termination of patent right due to non-payment of annual fee |