CN208688974U - A kind of Atomic Absorption Spectrometer - Google Patents

A kind of Atomic Absorption Spectrometer Download PDF

Info

Publication number
CN208688974U
CN208688974U CN201821341819.4U CN201821341819U CN208688974U CN 208688974 U CN208688974 U CN 208688974U CN 201821341819 U CN201821341819 U CN 201821341819U CN 208688974 U CN208688974 U CN 208688974U
Authority
CN
China
Prior art keywords
fixedly installed
spectrometer
cabinet
wall
generator
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201821341819.4U
Other languages
Chinese (zh)
Inventor
胡亮
杜希纯
尹海波
刘泓昱
周婷
关鹏翔
王亮
樊婕
范明珠
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangxi Forest Testing Co Ltd
Original Assignee
Jiangxi Forest Testing Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangxi Forest Testing Co Ltd filed Critical Jiangxi Forest Testing Co Ltd
Priority to CN201821341819.4U priority Critical patent/CN208688974U/en
Application granted granted Critical
Publication of CN208688974U publication Critical patent/CN208688974U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

The utility model provides a kind of Atomic Absorption Spectrometer, is related to Atomic Absorption Spectrometer technical field.The Atomic Absorption Spectrometer, including spectrometer cabinet, lamp source seat is fixedly installed at the top of the spectrometer cabinet, the bottom end of the lamp source seat is fixedly installed with lamp source body, detector is fixedly installed at the top of the spectrometer cabinet wall, the bottom of the spectrometer cabinet wall is fixedly installed with fixed plate, and the side of the fixed plate offers slit, and the inner wall of the spectrometer cabinet is fixedly installed with generator.The Atomic Absorption Spectrometer, center-pole is supported by microscope base, it is flexibly connected at center-pole and reflecting mirror Left-side center, allow reflecting mirror that adjusting reflection angle is freely rotated, the fixed block at reflecting mirror both ends is flexibly connected with adjusting rod by ball axis, and adjusting rod and threaded hole cooperate, and rotation control adjusting rod enters the length of spectrometer cabinet, then the reflection angle of reflecting mirror is controlled, it is convenient and efficient.

Description

A kind of Atomic Absorption Spectrometer
Technical field
The utility model relates to Atomic Absorption Spectrometer technical field, specially a kind of Atomic Absorption Spectrometer.
Background technique
Atomic absorption spectrophotometry is the specific and exclusive wavelength with element to be measured, measures atom caused by sample Absorption of the steam to radiation, to measure a kind of method of concentration of element in sample, it be based in atomizer, with flame or Element to be measured is generated atomic vapour by no flame method under high temperature action, and radiation of light source goes out the characteristic light of element to be measured, the spy Sign light is absorbed by the ground state atom of element to be measured when passing through atomizer, and transmitted light enters receiver, carry out photoelectric conversion and Record is measured the content of the element by the decrease of radiation luminous intensity, and tested concentration of element is directly proportional to absorbance value, and atom is inhaled Spectrophotometry is received because having many advantages, such as that selectivity is strong, interference is smaller, accuracy is high, analysis speed is fast becomes micro, trace One of element classics spectral method of detection is continuously improved and is developed with technical, and Atomic Absorption Spectrometer has become one As laboratory conventional analytical instruments, it is simple, cheap, easy to use, applied widely with its structure the features such as and obtain The fields such as environmental protection, medicine, health are widely applied.
When test, it may be necessary to the angle of reflecting mirror is adjusted to reach optimal reflecting effect, but existing at present In Atomic Absorption Spectrometer, reflecting mirror adjusting will not be paid attention to, and the limited angle of adjusting, precision is also not high enough, and regulative mode Also inconvenient, many puzzlements are brought to operator.
Utility model content
(1) the technical issues of solving
In view of the deficiencies of the prior art, the utility model provides a kind of Atomic Absorption Spectrometer, solves Atomic absorption The problem of it is inconvenient that spectrometer mirror angle is adjusted, and the precision of angular adjustment is not high, limited angle.
(2) technical solution
In order to achieve the above object, the utility model is achieved by the following technical programs: a kind of Atomic Absorption Spectrometer, Including spectrometer cabinet, lamp source seat is fixedly installed at the top of the spectrometer cabinet, the bottom end of the lamp source seat is fixedly mounted There is lamp source body, detector is fixedly installed at the top of the spectrometer cabinet wall, the bottom of the spectrometer cabinet wall is solid Dingan County is equipped with fixed plate, and the side of the fixed plate offers slit, and the inner wall of the spectrometer cabinet is fixedly installed with generation Device, the bottom of the generator are fixedly installed with knob, and the bottom of the generator offers feed inlet, the top of the generator Portion is fixedly installed with hood, and exhaust pipe is fixedly installed at the top of the hood, and the inside of the exhaust pipe is fixedly mounted There is ventilation fan, monochromator is fixedly installed on the left of the spectrometer cabinet wall, the right side of the spectrometer cabinet wall is solid Dingan County is equipped with microscope base, is fixedly installed with center-pole on the right side of the microscope base, and the right end of the center-pole is movably installed with reflecting mirror, The both ends of the reflecting mirror are fixedly installed with fixed block, and adjusting rod, the adjusting are movably installed on the left of the fixed block The left end of bar is fixedly installed with limited block, offers threaded hole on the left of the spectrometer cabinet wall, the generator it is interior Portion is fixedly installed with flame atomizer, and the inside of the generator is fixedly installed with graphite furnace atomizer, the generator Inside be fixedly installed with atomization unit for quartz furnace.
Preferably, the top of the lamp source seat runs through the top of spectrometer cabinet wall and extends to the outer of spectrometer cabinet Portion is fixedly installed with adjusting panel at the top of the lamp source seat.
Preferably, the central horizontal height of the fixed plate and the central horizontal height of reflecting mirror are consistent, the slit Quantity is two, and two slits are perforative through-hole, and all in horizontal position.
Preferably, shaft is fixedly installed at the center of the generator, spectrometer cabinet wall is run through in the bottom end of shaft Bottom extend to outside, the bottom end of shaft is fixedly installed with knob.
Preferably, the top of the generator and the top of spectrometer cabinet wall are offered is connected with hood Gas vent.
Preferably, it is installed at the center on the left of the center-pole and reflecting mirror using shaft activity, the adjusting rod and solid Determine block to install by spherical axis activity.
Preferably, the diameter of section of the adjusting rod and the internal diameter of threaded hole are consistent, are provided with screw thread on the adjusting rod, And match with the screw thread of threaded hole inner wall.
(3) beneficial effect
The utility model provides a kind of Atomic Absorption Spectrometer.Have it is following the utility model has the advantages that
1, the Atomic Absorption Spectrometer supports center-pole by microscope base, and activity connects at center-pole and reflecting mirror Left-side center It connects, allows reflecting mirror that adjusting reflection angle is freely rotated, the fixed block and adjusting rod at reflecting mirror both ends are connected by the activity of ball axis It connects, the rotation of reflecting mirror would not be restricted, and adjusting rod and threaded hole cooperate, and rotation control adjusting rod enters spectrometer The length of cabinet then controls the reflection angle of reflecting mirror, simply, fast, efficiently, and due to the fillet of screw progressive apart from short, Very short distance influences angle small, it is possible to the reflection angle of more accurate control reflecting mirror, to operator with To facilitate.
2, Atomic Absorption Spectrometer, by by flame atomizer, graphite furnace atomizer and atomization unit for quartz furnace It concentrating in columnar generator, three kinds of reaction tests can be done in an instrument, knob can drive generator to rotate, Third-order reaction test is successively finished, test result can compare immediately after coming out, the reference test of more two kinds of other modes More convincing as a result, the test made is more accurate, operator no longer needs time-consuming and laborious to use three instrument wheels respectively It kind tests, non-can not accomplish absolutely unanimously, to compare the meaning of reference referring to factor to other other than referring to factor like that Less.
Detailed description of the invention
FIG. 1 is a schematic structural view of the utility model;
Fig. 2 is the partial enlargement diagram of A portion structure in Fig. 1;
Fig. 3 is the structural schematic diagram of the utility model generator.
In figure: 1 spectrometer cabinet, 2 lamp source seats, 3 lamp source bodies, 4 detectors, 5 fixed plates, 6 slits, 7 generators, 8 knobs, 9 feed inlets, 10 hoods, 11 exhaust pipes, 12 ventilation fans, 13 monochromators, 14 microscope bases, 15 center-poles, 16 reflecting mirrors, 17 are fixed Block, 18 adjusting rods, 19 limited blocks, 20 threaded holes, 21 flame atomizers, 22 graphite furnace atomizers, 23 quartzy furnace atomization Device.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
The utility model embodiment provides a kind of Atomic Absorption Spectrometer, as shown in Figure 1-3, include spectrometer cabinet 1, light The top of spectrometer cabinet 1 is fixedly installed with lamp source seat 2, top and extension of the top of lamp source seat 2 through 1 inner wall of spectrometer cabinet To the outside of spectrometer cabinet 1, the top of lamp source seat 2 is fixedly installed with adjusting panel, and the bottom end of lamp source seat 2 is fixedly installed with lamp Source body 3 is fixedly installed with detector 4 at the top of 1 inner wall of spectrometer cabinet, and the bottom of 1 inner wall of spectrometer cabinet is fixedly installed with Fixed plate 5, the side of fixed plate 5 offer slit 6, and the central horizontal height of fixed plate 5 and the central horizontal of reflecting mirror 16 are high Degree is consistent, and the quantity of slit 6 is two, and two slits 6 are perforative through-hole, and all in horizontal position, spectrometer cabinet 1 Inner wall is fixedly installed with generator 7, and the bottom of generator 7 is fixedly installed with knob 8, is fixedly installed at the center of generator 7 The bottom end of shaft, shaft extends to outside through the bottom of 1 inner wall of spectrometer cabinet, and the bottom end of shaft is fixedly installed with knob 8, The bottom of generator 7 offers feed inlet 9, and the top of generator 7 is fixedly installed with hood 10, the top of generator 7 and light The top of 1 inner wall of spectrometer cabinet offers the gas vent being connected with hood 10, and the top of hood 10 is fixedly installed with Exhaust pipe 11, the inside of exhaust pipe 11 are fixedly installed with ventilation fan 12, are fixedly installed with monochrome on the left of 1 inner wall of spectrometer cabinet Instrument 13 is fixedly installed with microscope base 14 on the right side of 1 inner wall of spectrometer cabinet, and the right side of microscope base 14 is fixedly installed with center-pole 15, in The right end of core bar 15 is movably installed with reflecting mirror 16, and the both ends of reflecting mirror 16 are fixedly installed with fixed block 17, fixed block 17 Left side is movably installed with adjusting rod 18, is installed at the center in 16 left side of center-pole 15 and reflecting mirror using shaft activity, adjusting rod 18 are installed by spherical axis activity with fixed block 17, and the left end of adjusting rod 18 is fixedly installed with limited block 19, in spectrometer cabinet 1 Threaded hole 20 is offered on the left of wall, the diameter of section of adjusting rod 18 is consistent with the internal diameter of threaded hole 20, is arranged on adjusting rod 18 There is screw thread, and match with the screw thread of 20 inner wall of threaded hole, center-pole 15, center-pole 15 and reflecting mirror 16 are supported by microscope base 14 It is flexibly connected at Left-side center, allows reflecting mirror 16 that adjusting reflection angle, the fixed block 17 at 16 both ends of reflecting mirror is freely rotated It is flexibly connected with adjusting rod 18 by ball axis, the rotation of reflecting mirror 16 would not be restricted, adjusting rod 18 and 20 phase of threaded hole Mutually cooperation, rotation control adjusting rod 18 enter the length of spectrometer cabinet 1, then control the reflection angle of reflecting mirror 16, simply, Fast, efficiently, and due to the fillet of screw it is progressive apart from short, very short distance on angle influence it is small, it is possible to it is more accurate Control reflecting mirror 16 reflection angle, brought convenience to operator, the inside of generator 7 is fixedly installed with flame atomization Device 21, the inside of generator 7 are fixedly installed with graphite furnace atomizer 22, and it is former that the inside of generator 7 is fixedly installed with quartzy furnace Sonization device 23, by the way that flame atomizer 21, graphite furnace atomizer 22 and atomization unit for quartz furnace 23 are concentrated on cylindrical shape Generator 7 in, three kinds of reaction tests can be done in an instrument, knob 9 can drive generator 7 to rotate, and successively finish Third-order reaction test, test result can compare immediately after coming out, and more reference test results of two kinds of other modes make Test it is more accurate, it is more convincing, operator no longer need it is time-consuming and laborious tested by turns using three instruments respectively, It can not accomplish absolutely unanimously, to compare having little significance for reference referring to factor to others are non-other than referring to factor like that.
The electric elements occurred in this article are electrically connected with extraneous main controller and 220V alternating current, and main controller can be meter Calculation machine etc. plays the conventionally known equipment of control.
Working principle: in use, being put into substance to be tested in generator 7 by feed inlet 9, microscope base 14 supports center-pole 15, it is flexibly connected at center-pole 15 and 16 Left-side center of reflecting mirror, allows reflecting mirror 16 that adjusting reflection angle is freely rotated, instead The fixed block 17 for penetrating 16 both ends of mirror is flexibly connected with adjusting rod 18 by ball axis, and the rotation of reflecting mirror 16 would not be restricted, Adjusting rod 18 and threaded hole 20 cooperate, and rotation control adjusting rod 18 enters the length of spectrometer cabinet 1, then control reflection The reflection angle of mirror 16, and due to the fillet of screw it is progressive apart from short, very short distance on angle influence it is small, it is possible to more It is accurately controlled the reflection angle of reflecting mirror 16,16 angle of reflecting mirror opens reaction test after mixing up, and drives and occurs by knob 8 Device 7 rotates, and keeps test substance successively anti-in flame atomizer 21, graphite furnace atomizer 22 and atomization unit for quartz furnace 23 It should test, three kinds of test results are put together after the completion of test and are compared, finally obtain test result the most accurate.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment Intrinsic element.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art, It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.

Claims (7)

1. a kind of Atomic Absorption Spectrometer, including spectrometer cabinet (1), it is characterised in that: the top of the spectrometer cabinet (1) It is fixedly installed with lamp source seat (2), the bottom end of the lamp source seat (2) is fixedly installed with lamp source body (3), the spectrometer cabinet (1) It being fixedly installed at the top of inner wall detector (4), the bottom of spectrometer cabinet (1) inner wall is fixedly installed with fixed plate (5), The side of the fixed plate (5) offers slit (6), and the inner wall of the spectrometer cabinet (1) is fixedly installed with generator (7), The bottom of the generator (7) is fixedly installed with knob (8), and the bottom of the generator (7) offers feed inlet (9), described It is fixedly installed at the top of generator (7) hood (10), is fixedly installed with exhaust pipe (11) at the top of the hood (10), The inside of the exhaust pipe (11) is fixedly installed with ventilation fan (12), and the left side of spectrometer cabinet (1) inner wall is fixedly mounted Have monochromator (13), is fixedly installed with microscope base (14) on the right side of spectrometer cabinet (1) inner wall, the right side of the microscope base (14) It is fixedly installed with center-pole (15), the right end of the center-pole (15) is movably installed with reflecting mirror (16), the reflecting mirror (16) Both ends be fixedly installed with fixed block (17), be movably installed with adjusting rod (18), the tune on the left of the fixed block (17) The left end of pole (18) is fixedly installed with limited block (19), offers threaded hole on the left of spectrometer cabinet (1) inner wall (20), the inside of the generator (7) is fixedly installed with flame atomizer (21), the fixed peace in the inside of the generator (7) Equipped with graphite furnace atomizer (22), the inside of the generator (7) is fixedly installed with atomization unit for quartz furnace (23).
2. a kind of Atomic Absorption Spectrometer according to claim 1, it is characterised in that: passed through at the top of the lamp source seat (2) It wears the top of spectrometer cabinet (1) inner wall and extends to the outside of spectrometer cabinet (1), the top of the lamp source seat (2) is fixed Adjusting panel is installed.
3. a kind of Atomic Absorption Spectrometer according to claim 1, it is characterised in that: the middle edema with the heart involved of the fixed plate (5) Flat height is consistent with the central horizontal height of reflecting mirror (16), and the quantity of the slit (6) is two, two slits (6) For perforative through-hole, and all in horizontal position.
4. a kind of Atomic Absorption Spectrometer according to claim 1, it is characterised in that: at the center of the generator (7) It is fixedly installed with shaft, the bottom end of shaft extends to outside through the bottom of spectrometer cabinet (1) inner wall, and the bottom end of shaft is fixed Knob (8) are installed.
5. a kind of Atomic Absorption Spectrometer according to claim 1, it is characterised in that: the top of the generator (7) and The top of spectrometer cabinet (1) inner wall offers the gas vent being connected with hood (10).
6. a kind of Atomic Absorption Spectrometer according to claim 1, it is characterised in that: the center-pole (15) and reflecting mirror (16) it is installed at the center on the left of using shaft activity, the adjusting rod (18) and fixed block (17) are pacified by spherical axis activity Dress.
7. a kind of Atomic Absorption Spectrometer according to claim 1, it is characterised in that: the section of the adjusting rod (18) is straight Diameter is consistent with the internal diameter of threaded hole (20), and screw thread, and the screw thread with threaded hole (20) inner wall are provided on the adjusting rod (18) Match.
CN201821341819.4U 2018-08-20 2018-08-20 A kind of Atomic Absorption Spectrometer Expired - Fee Related CN208688974U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821341819.4U CN208688974U (en) 2018-08-20 2018-08-20 A kind of Atomic Absorption Spectrometer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821341819.4U CN208688974U (en) 2018-08-20 2018-08-20 A kind of Atomic Absorption Spectrometer

Publications (1)

Publication Number Publication Date
CN208688974U true CN208688974U (en) 2019-04-02

Family

ID=65885892

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821341819.4U Expired - Fee Related CN208688974U (en) 2018-08-20 2018-08-20 A kind of Atomic Absorption Spectrometer

Country Status (1)

Country Link
CN (1) CN208688974U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110823362A (en) * 2019-09-10 2020-02-21 李东华 High beam detection system and detection method thereof
CN110823363A (en) * 2019-09-10 2020-02-21 李东华 Automobile light detection system and detection method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110823362A (en) * 2019-09-10 2020-02-21 李东华 High beam detection system and detection method thereof
CN110823363A (en) * 2019-09-10 2020-02-21 李东华 Automobile light detection system and detection method thereof

Similar Documents

Publication Publication Date Title
CN105277503B (en) Multicomponent gas while detection means and method based on two amounts son cascade laser spectrum
CN208688974U (en) A kind of Atomic Absorption Spectrometer
CN107328727B (en) Flue gas analysis device and method based on ultraviolet difference technology
Fox Jr Stable internal standard flame photometer for potassium and sodium analyses
CN105606562B (en) A kind of near-infrared diffusing reflection automatically corrects probe
CN104596639B (en) Far-field three-dimensional strength representation device for semiconductor light source
CN209215215U (en) Adjustable laser analysis equipment
CN203881653U (en) Automatic analyzer for free silicon dioxide in dust
CN206292158U (en) A kind of Multifunction infrared spectrometer sample holder
CN203490167U (en) Sample gas absorption cell for Fourier infrared spectrum detection device
Mohamed et al. Laser Fraunhofer diffraction studies of aerosol droplet size in atomic spectrochemical analysis
Rains et al. Automatic correction system for light scatter in atomic fluorescence spectrometry
Christmann et al. Automated instrument for absorption-corrected molecular fluorescence measurements by the cell shift method
JPS61195331A (en) Method and device for optimizing operation parameter of meter for analysis
CN108731809A (en) Atomic absorption spectrometer and system
Michel et al. A novel method of wavelength modulation for atomic spectrometry—some preliminary experiments
CN108120677B (en) Centering leveling device for infrared spectrometer observation and sample rotating method
CN209264723U (en) A kind of heat-transferring printing paper coating banner uniformity on-line measuring device
CN209417028U (en) A kind of liquid food illuminance detecting device
CN101845951B (en) Method for quickly analyzing components of drilling liquid by using ultrasonic molecular beams
CN208297349U (en) The mercury detector of high measurement accuracy
Werner et al. Establishment of optimum conditions for ICP atomic emission spectrometry (AES)
Torsi et al. Absolute analysis in electrothermal atomization atomic absorption spectroscopy—an atomization system for confining all the atoms injected in the opti
CN215678104U (en) Multi-axis positioning device for laser Raman spectrometer
CN103940512A (en) Polarization calibrating method and device for direct current Zeeman atomic absorption of two detectors

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190402

Termination date: 20210820