CN208661101U - A kind of glass reaction kettle equipment of multiphase or homogeneous reaction - Google Patents
A kind of glass reaction kettle equipment of multiphase or homogeneous reaction Download PDFInfo
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- CN208661101U CN208661101U CN201820530377.1U CN201820530377U CN208661101U CN 208661101 U CN208661101 U CN 208661101U CN 201820530377 U CN201820530377 U CN 201820530377U CN 208661101 U CN208661101 U CN 208661101U
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- reaction
- reaction kettle
- kettle
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Abstract
The utility model discloses a kind of multiphase or the glass reaction kettle equipment of homogeneous reaction.Chiral process is the core process process of production, and it is the key equipment of many process units that consersion unit used, as chemical reaction, which provide the device of reaction compartment and reaction condition,.Glass reaction kettle equipment disclosed by the utility model is mainly by condenser, receiving flask, liquid phase feeder, liquid phase flow control valve, reaction kettle upper end kettle cover, reaction kettle lower end kettle cover, high frequency ultrasound pipe, reaction kettle glass chamber, blender, titanium heating tube, stirring motor, the major parts such as electric heating cover composition.The utility model device can be used for carrying out the synthesis and preparation of related nano material by reacting between solid-liquid or liquid liquid, and the application fields such as pharmacy reaction, organic reaction, inorganic reaction, fine chemistry industry reaction, Industrial Catalysis reaction, reaction efficiency is high, and input cost is low, operates flexible adjustment.
Description
Technical field
This field is novel to belong to equipment manufacturing technology field, and the glass reaction kettle for being related to a kind of multiphase or homogeneous reaction is set
It is standby.
Background technique
Solid-liquid two phase reaction refers to the reaction occurred in solid phase and liquid phase between the two, in pharmacy reaction, organic reaction, nothing
The fields such as machine reaction, fine chemistry industry, Industrial Catalysis are widely used.In addition, also there is extensive use in field of material preparation, such as
Apply the preparation of more carried catalyst in the fields such as in medicine, chemical industry plus hydrogen, new energy source fuel cell.In solid-liquid or liquid
During liquid two phase reaction, part reaction is to the dispersity of material, reaction temperature, liquid rate of addition and operation convenience
Otherwise demand with higher will bring biggish inconsistency to the product of research and development and production in performance.
Utility model content
For the portion requirements in solid-liquid or liquid-liquid diphase reaction process, the purpose of the utility model is to provide a kind of multiphases
Or the glass reaction kettle equipment of homogeneous reaction.The equipment input cost is low, high-efficient, simple to operate, and meeting has spy
The reaction requirement very required.Provided by the utility model is the glass reaction kettle equipment of a kind of multiphase or homogeneous reaction, packet
Include condenser, receiving flask, liquid phase feeder, tubulose feeder, liquid phase flow control valve, reaction kettle upper end kettle cover, under reaction kettle
Hold kettle cover, reaction kettle glass chamber, blender, titanium heating tube, stirring motor, electric heating cover.
A set of high frequency ultrasound pipe device is also equipped in reaction kettle equipment, which is conducive to the quick dissolution of powder body material
Disperse with homogenization, convenient for the quick generation of reaction.
The titanium heating tube is Dual-layer titanium heating tube, is heated in outer layer electric heating cover to reactant in reaction kettle same
When, required temperature is warming up to come supplies Quick uniform by electric heating titanium tube, temperature is solved and rises slow difficulty,
Reduce the generation of side reaction.
It is equipped with discharge gate at the top of reaction kettle, material is got using from upper end with pump, after the reaction was completed by reaction product material
It is got from upper end by metering pump, avoids the damage from bottom end opening blowing to autoclave body safety, and also save to anti-
Answer the space requirement in bottom portion.
The liquid phase feeder and tubulose feeder be can finely regulating liquid material addition and flow, solid phase charging
Device and reaction kettle body at an angle, the addition of easy solid material.
Have the function of in reaction process be condensed back, it is ensured that the solution in reaction process in reaction kettle will not be evaporated and
It reduces.Real-time online is also equipped with to the in-situ monitoring of the response parameters such as reaction temperature, pH value simultaneously.
The utility model equipment for solid-liquid two phase reaction use process is as follows: by liquid inlet opening add solvent,
And solid phase reaction material is added in reaction kettle by tubulose feeder, under the action of blender and high frequency ultrasound pipe, it will consolidate
Phase reaction object sufficiently smash with it is evenly dispersed, then adjust flow and liquid phase reacting material be added to reaction according to certain rate
In kettle, it is sufficiently mixed under the action of blender and high frequency ultrasound pipe again uniformly.It is to be mixed uniformly after, open electric jacket and titanium
Pipe heater, temperature, which is promoted the temperature to required for reacting, rapidly takes place reaction.To after the reaction was completed by by with
The booster pump abstraction reaction of reaction kettle connection generates material and gets from upper end discharge port, carries out at subsequent cooling and feed separation
Reason.The process of liquid-liquid diphase reaction is similar with the above process, and difference is that liquid material is successively added from liquid addition port.
Being characterized mainly in that in reaction kettle for the utility model is provided with high frequency ultrasound dispersal device, and it is anti-that solid may be implemented
Full and uniform the mixing of material with liquid phase material or liquid night material is answered, to realize the generation of reaction maximal efficiency.In addition, this is anti-
It answers kettle to have the ability being rapidly heated, reduces the probability that the side reaction product sensitive to reaction temperature generates, improve product
The consistency of production performance.The glass reaction kettle equipment also has the advantage that
1. the equipment operation strategies are wider, solid-liquid multiphase may be implemented or liquid liquid is equal conditioned response process.
2. the equipment is by the accurate control of temperature and the ultrasonic disperse of material, effective solution reaction process
In cause properties of product inconsistent due to the influence of reaction condition problem.
3. the equipment is not easy to plug convenient for cleaning, safe operation, simple and convenient.
Detailed description of the invention
Fig. 1 is the glass reaction kettle overall structure diagram of the utility model；
Fig. 2 is the glass reaction kettle kettle cover structural schematic diagram of the utility model；
Fig. 3 is the titanium heating tube (left side) and high frequency ultrasound pipe (right side) schematic diagram of the utility model；
Fig. 4 solid-phase material adder structural schematic diagram.
In figures 1-4, condenser (1), receiving flask (2), liquid phase feeder (3), liquid phase flow control valve (4), reaction kettle
Upper end kettle cover (5), reaction kettle lower end kettle cover (6), high frequency ultrasound pipe (7), reaction kettle glass chamber (8), blender (9), titanium adds
Mouth (14) are added dropwise in heat pipe (10), stirring motor (11), electric heating cover (12), temperature sensing mouth (13), liquid phase, and high frequency ultrasound pipe is put
It sets mouth (15), solid-phase material adding mouth (16), exhaust outlet (17), discharge port (18), stirring port (19), condensate port (20), titanium adds
Heat pipe mouth (21), pH value test mouth (22), solid phase feeder (23)
Specific embodiment:
The utility model equipment for solid-liquid two phase reaction use process is as follows: by liquid inlet opening add solvent,
And solid phase reaction material is added in reaction kettle by tubulose feeder, under the action of blender and high frequency ultrasound pipe, it will consolidate
Phase reaction object sufficiently smash with it is evenly dispersed, then adjust flow and liquid phase reacting material be added to reaction according to certain rate
In kettle, it is sufficiently mixed under the action of blender and high frequency ultrasound pipe again uniformly.It is to be mixed uniformly after, open electric jacket and titanium
Pipe heater, temperature, which is promoted the temperature to required for reacting, rapidly takes place reaction.To after the reaction was completed by by with
The booster pump abstraction reaction of reaction kettle connection generates material and gets from upper end discharge port, carries out at subsequent cooling and feed separation
Reason.The process of liquid-liquid diphase reaction is similar with the above process, and difference is that liquid material is successively added from liquid addition port.
The utility model is described in detail in 1-4 and specific embodiment with reference to the accompanying drawing.The utility model is one
The glass reaction kettle equipment of kind multiphase or homogeneous reaction is added in reaction kettle body (8) by liquid phase feeder (3) first,
Start to stir under the action of the agitating paddle (9) that motor (11) drives, solid matter then is added by solid phase feeder (23), beats
High frequency ultrasound pipe (7) are opened, in ultrasound with after dispersion under the synergistic effect of stirring and uniformly mixed material, are opened electric heating cover (12)
Begin to warm up, while opening titanium heating tube (10), temperature is promoted rapidly to reaction and set temperature and keep stable, avoid due to
Slowly heating bring side reaction occurs.In reaction process, the steam of generation within the condenser (1) after circulating cooling again
It flows into and participates in reaction in glass reaction kettle (8).After the completion of end reaction, the material after reaction is covered from reaction kettle by pumping
It brings out material mouth (18) to get, carries out refrigerated separation recycling into subsequent cooling device.
Claims (5)
1. the glass reaction kettle equipment of a kind of multiphase or homogeneous reaction, characterized by comprising: condenser, receiving flask, liquid phase
Feeder, tubulose feeder, liquid phase flow control valve, reaction kettle upper end kettle cover, reaction kettle lower end kettle cover, reaction kettle glass cavity
Body, blender, titanium heating tube, stirring motor, electric heating cover.
2. the glass reaction kettle equipment of a kind of multiphase according to claim 1 or homogeneous reaction, it is characterised in that: anti-
It answers and is also equipped with a set of high frequency ultrasound pipe device in kettle equipment.
3. the glass reaction kettle equipment of a kind of multiphase according to claim 1 or homogeneous reaction, it is characterised in that: described
Titanium heating tube is Dual-layer titanium heating tube, while outer layer electric heating cover heats reactant in reaction kettle, is added by electricity
Hot titanium tube carrys out supplies Quick uniform and is warming up to required temperature.
4. the glass reaction kettle equipment of a kind of multiphase according to claim 1 or homogeneous reaction, it is characterised in that: reaction
Kettle top portion is equipped with discharge gate, gets material using from upper end with pump, reaction product material is passed through meter from upper end after the reaction was completed
Amount pump is got.
5. the glass reaction kettle equipment of a kind of multiphase according to claim 1 or homogeneous reaction, it is characterised in that: described
Liquid phase feeder and tubulose feeder be can finely regulating liquid material addition and flow, solid phase feeder and reaction kettle body
At an angle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820530377.1U CN208661101U (en) | 2018-04-13 | 2018-04-13 | A kind of glass reaction kettle equipment of multiphase or homogeneous reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820530377.1U CN208661101U (en) | 2018-04-13 | 2018-04-13 | A kind of glass reaction kettle equipment of multiphase or homogeneous reaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208661101U true CN208661101U (en) | 2019-03-29 |
Family
ID=65822365
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820530377.1U Active CN208661101U (en) | 2018-04-13 | 2018-04-13 | A kind of glass reaction kettle equipment of multiphase or homogeneous reaction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208661101U (en) |
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2018
- 2018-04-13 CN CN201820530377.1U patent/CN208661101U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20230827 Address after: No. 988, Keji Road, high tech Industrial Development Zone, Kunming, Yunnan 650000 Patentee after: Yunnan Precious Metals Laboratory Co.,Ltd. Address before: No. 988 Keji Road, Wuhua District, Kunming City, Yunnan Province, 650106 Patentee before: SINO-PRECIOUS METALS HOLDING CO.,LTD. |