CN208642454U - A kind of high-purity production of chloroacetic acid stock stirring device - Google Patents
A kind of high-purity production of chloroacetic acid stock stirring device Download PDFInfo
- Publication number
- CN208642454U CN208642454U CN201821095034.3U CN201821095034U CN208642454U CN 208642454 U CN208642454 U CN 208642454U CN 201821095034 U CN201821095034 U CN 201821095034U CN 208642454 U CN208642454 U CN 208642454U
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- China
- Prior art keywords
- vertical pivot
- stirred tank
- air inlet
- stirring rod
- paddle
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Abstract
The utility model discloses a kind of high-purity production of chloroacetic acid stock stirring devices, including stirred tank, motor and stirring rod, steam pipe is installed on the outside of the stirred tank, and steam valve is installed on steam pipe, discharge valve is installed below the stirred tank, and escape pipe is connected on the right side of stirred tank, and chuck layer is provided on the inside of stirred tank, the link block is connected with each other by ball and link slot and vertical pivot, and air inlet and snorkel are reserved on vertical pivot, the stirring rod, gas vent is offered on paddle and vertical pivot, and separation net is installed on gas vent.High-purity production of chloroacetic acid stock stirring device, contain moisture in hollow chuck layer, steam is facilitated to heat chuck layer, it is maintained in a stable range to be conducive to temperature, and chlorine is put into the material stirred by the row of exhausting-gas hole on stirring rod and paddle, improves the chlorination effect of material.
Description
Technical field
The utility model relates to monoxone technical field of processing equipment, specially a kind of high-purity production of chloroacetic acid raw material stirring
Device.
Background technique
Monoxone is the intermediate of dyestuff, medicine, pesticide, synthetic resin and other organic synthesis materials, acetic acid catalysis chlorine
Change method is to produce the most important method of monoxone both at home and abroad at present, it can be divided into batch production technique and continuous production work again
It is two kinds of skill, chloroacetic in the process it is generally necessary to use agitating device producing.
Existing agitating device is when logical chlorine, it has not been convenient to which chlorine and raw material carry out being sufficiently mixed chlorination, to drop
The low chlorination efficiency of material, and then affected indirectly chloroacetic product quality.In view of the above-mentioned problems, in original stirring
Innovative design is carried out on the basis of device.
Utility model content
The purpose of this utility model is to provide a kind of high-purity production of chloroacetic acid stock stirring devices, to solve above-mentioned background
The existing agitating device proposed in technology is when logical chlorine, it has not been convenient to and chlorine and raw material carry out being sufficiently mixed chlorination, from
And the chlorination efficiency of material is reduced, and then the problem of affected indirectly chloroacetic product quality.
To achieve the above object, the utility model provides the following technical solutions: a kind of high-purity production of chloroacetic acid raw material stirring
Device, including stirred tank, motor and stirring rod are equipped with steam pipe on the outside of the stirred tank, and are equipped with steaming on steam pipe
Steam valve door is equipped with discharge valve below the stirred tank, and is connected with escape pipe on the right side of stirred tank, and stirred tank
Inside is provided with chuck layer, and the motor is located at the top of stirred tank, and feed inlet is provided on the outside of motor, the motor
Lower section is equipped with vertical pivot, and lantern ring is connected on the outside of vertical pivot, air inlet pipe is equipped on the lantern ring, and the inside of lantern ring is fixed
There is link block, the link block is located at the inside of link slot, and ball is provided between link block and link slot, the link block
It is connected with each other by ball and link slot and vertical pivot, and is reserved with air inlet and snorkel on vertical pivot, the stirring rod is located at perpendicular
The outside of axis, and paddle is installed on stirring rod, gas vent is offered on the stirring rod, paddle and vertical pivot, and arrange
Separation net is installed on stomata.
Preferably, the lower end kettle wall of the stirred tank is hollow structure, and chuck layer is nested on the inside of stirred tank, and
Chuck layer is hollow structure.
Preferably, the lantern ring is nested in the outside of vertical pivot, and lantern ring passes through link block, ball and link slot and vertical pivot structure
At slide construction, and vertical pivot is hollow structure.
Preferably, the air inlet pipe is the carbon steel pipe of surface patch enamel, and air inlet pipe and stirred tank be through connection, and
And the junction of air inlet pipe and stirred tank is to be welded to connect.
Preferably, air inlet equidistantly distributed annular in shape on vertical pivot, and air inlet is integrated knot with snorkel
Structure, and air inlet and snorkel constitute " T " font structure.
Preferably, the stirring rod and paddle are hollow structure, and stirring rod and paddle are integrated, and
And gas vent is evenly distributed on stirring rod and paddle.
Compared with prior art, the utility model has the beneficial effects that high-purity production of chloroacetic acid stock stirring device, side
Just chlorine is sufficiently mixed with material,
1, contain moisture in hollow chuck layer, facilitate the temperature for keeping reacting, so that being conducive to temperature maintains one
In stable range, and chlorine is put into the material stirred by the row of exhausting-gas hole on stirring rod and paddle, is improved
The chlorination effect of material；
2, air inlet pipe is stainless steel metal material, and lantern ring can be fixed, so that lantern ring be facilitated to pass through link block, rolling
Pearl and link slot and vertical pivot carry out rotational slide, avoid vertical pivot that lantern ring is driven to be moved, avoiding the occurrence of chlorine can not carry out
The case where normal perfusion；
3, chlorine is filled into the inside of material from the gas vent on stirring rod and paddle, to be conducive to chlorine and material
It carries out being sufficiently mixed chlorination, avoids the occurrence of the case where chlorine floats on surface of material, accelerate the chlorination efficiency of material.
Detailed description of the invention
Fig. 1 is the utility model overall structure diagram；
Fig. 2 is the utility model paddle and stirring rod attachment structure schematic diagram；
Fig. 3 is the utility model lantern ring and vertical pivot attachment structure schematic diagram；
Fig. 4 is the utility model air inlet structure schematic diagram.
In figure: 1, stirred tank；2, steam pipe；3, steam valve；4, discharge valve；5, escape pipe；6, chuck layer；7, electric
Machine；8, feed inlet；9, vertical pivot；10, lantern ring；11, air inlet pipe；12, link block；13, ball；14, link slot；15, air inlet；
16, snorkel；17, stirring rod；18, paddle；19, gas vent；20, separation net.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-4 is please referred to, the utility model provides a kind of technical solution: a kind of high-purity production of chloroacetic acid raw material stirring dress
It sets, including stirred tank 1, motor 7 and stirring rod 17, the outside of stirred tank 1 is equipped with steam pipe 2, and steaming is equipped on steam pipe 2
Steam valve door 3, the lower section of stirred tank 1 is equipped with discharge valve 4, and the right side of stirred tank 1 is connected with escape pipe 5, and stirred tank 1
Inside be provided with chuck layer 6, the lower end kettle wall of stirred tank 1 is hollow structure, and the inside of stirred tank 1 is nested with chuck layer 6,
And chuck layer 6 is hollow structure, facilitates steam to be filled into the hollow of stirred tank 1 and interior heats to chuck layer 6；
Motor 7 is located at the top of stirred tank 1, and the outside of motor 7 is provided with feed inlet 8, and the lower section of motor 7 is equipped with perpendicular
Axis 9, and the outside of vertical pivot 9 is connected with lantern ring 10, air inlet pipe 11 is equipped on lantern ring 10, and the inside of lantern ring 10 is fixed with connection
Block 12, air inlet pipe 11 is the carbon steel pipe of surface patch enamel, and air inlet pipe 11 and stirred tank 1 are through connection, and air inlet pipe
11 with the junction of stirred tank 1 be to be welded to connect, convenient that lantern ring 10 is fixed, and avoids vertical pivot 9 that lantern ring 10 is driven to be transported
Dynamic, lantern ring 10 is nested in the outside of vertical pivot 9, and lantern ring 10 is made up of link block 12, ball 13 and link slot 14 and vertical pivot 9 and slides
Dynamic structure, and vertical pivot 9 is hollow structure, improves the fluency of the movement of lantern ring 10, and link block 12 is located at the interior of link slot 14
Side, and ball 13 is provided between link block 12 and link slot 14, link block 12 passes through ball 13 and link slot 14 and 9 phase of vertical pivot
It connects, and is reserved with air inlet 15 and snorkel 16 on vertical pivot 9, the equidistantly distributed annular in shape on vertical pivot 9 of air inlet 15, and
Air inlet 15 is integrated with snorkel 16, and air inlet 15 and snorkel 16 constitute " T " font structure, facilitate chlorine
It is filled into vertical pivot 9 by air inlet 15 and snorkel 16, so that convenient be discharged into the material of stirring by gas vent 19；
Stirring rod 17 is located at the outside of vertical pivot 9, and paddle 18 is equipped on stirring rod 17, stirring rod 17 and paddle 18
It is hollow structure, and stirring rod 17 and paddle 18 are integrated, and uniformly divides on stirring rod 17 and paddle 18
Be furnished with gas vent 19, be conducive to chlorine be discharged into inside material carry out it is mixed chlorinated, on stirring rod 17, paddle 18 and vertical pivot 9
Gas vent 19 is offered, and separation net 20 is installed on gas vent 19.
Working principle: according to Fig. 1-4, glacial acetic acid and sulphur powder is added in stirred tank 1 by feed inlet 8 first, connect
Start the agitating device, motor 7 by vertical pivot 9 drive stirring rod 17 and paddle 18 material in stirred tank 1 is stirred
It mixes, then opens steam valve 3, so that steam is persistently injected into the hollow inner wall in 1 lower end of stirred tank out of steam pipe 2, into
And steam heats the moisture in chuck layer 6, extra steam is discharged from escape pipe 5, the moisture in chuck layer 6 facilitate by
The heating temperature of material maintains 100 degree or so, and while vertical pivot 9 is rotated, lantern ring 10 passes through link block 12, ball 13
It is rotated with link slot 14 in the outside of vertical pivot 9, while lantern ring 10 keeps steady with vertical pivot 9 by link block 12 and link slot 14
Fixed connection；
According to Fig. 1-4, when the moisture temperature in chuck layer 6 reaches to be spent 90 more, chlorine is filled with by air inlet pipe 11 at this time
Gas, chlorine are filled into snorkel 16 by the air inlet 15 on vertical pivot 9, and then a part of chlorine passes through the exhaust on vertical pivot 9
Hole 19 is discharged among the material of stirring, while another part chlorine injects in hollow stirring rod 17 and paddle 18, and injection is stirred
It mixes the chlorine in bar 17 and paddle 18 to pass through again in the material of the injection stirring of gas vent 19, facilitates chlorine directly and inside material
It is contacted, improves material and chlorine carries out mixed chlorinated efficiency, while the separation net 20 on gas vent 19 can be avoided
Material pours in hollow stirring rod 17 and paddle 18, and such a high-purity production of chloroacetic acid stock stirring device facilitates people
Use.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired
Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.
Claims (6)
1. a kind of high-purity production of chloroacetic acid stock stirring device, including stirred tank (1), motor (7) and stirring rod (17), feature
It is: is equipped with steam pipe (2) on the outside of the stirred tank (1), and steam valve (3) are installed on steam pipe (2), it is described to stir
It mixes and is equipped with below kettle (1) discharge valve (4), and be connected with escape pipe (5) on the right side of stirred tank (1), and stirred tank (1)
Inside be provided with chuck layer (6), the motor (7) is located at the top of stirred tank (1), and be provided on the outside of motor (7) into
Material mouth (8) is equipped with vertical pivot (9) below the motor (7), and is connected with lantern ring (10), the lantern ring on the outside of vertical pivot (9)
(10) it is equipped on air inlet pipe (11), and is fixed with link block (12) on the inside of lantern ring (10), the link block (12), which is located at, to be connected
The inside of access slot (14), and ball (13) are provided between link block (12) and link slot (14), the link block (12) passes through
Ball (13) and link slot (14) and vertical pivot (9) are connected with each other, and air inlet (15) and snorkel are reserved on vertical pivot (9)
(16), the stirring rod (17) is located at the outside of vertical pivot (9), and paddle (18), the stirring are equipped on stirring rod (17)
It is offered gas vent (19) on bar (17), paddle (18) and vertical pivot (9), and separation net is installed on gas vent (19)
(20)。
2. a kind of high-purity production of chloroacetic acid stock stirring device according to claim 1, it is characterised in that: the stirred tank
(1) lower end kettle wall is hollow structure, and chuck layer (6) are nested on the inside of stirred tank (1), and chuck layer (6) is hollow
Structure.
3. a kind of high-purity production of chloroacetic acid stock stirring device according to claim 1, it is characterised in that: the lantern ring
(10) it is nested in the outside of vertical pivot (9), and lantern ring (10) passes through link block (12), ball (13) and link slot (14) and vertical pivot
(9) slide construction is constituted, and vertical pivot (9) is hollow structure.
4. a kind of high-purity production of chloroacetic acid stock stirring device according to claim 1, it is characterised in that: the air inlet pipe
(11) paste the carbon steel pipe of enamel for surface, and air inlet pipe (11) and stirred tank (1) be through connection, and air inlet pipe (11) with stir
The junction of kettle (1) is mixed to be welded to connect.
5. a kind of high-purity production of chloroacetic acid stock stirring device according to claim 1, it is characterised in that: the air inlet
(15) equidistantly distributed annular in shape on vertical pivot (9), and air inlet (15) is integrated with snorkel (16), and air inlet
Hole (15) and snorkel (16) constitute " T " font structure.
6. a kind of high-purity production of chloroacetic acid stock stirring device according to claim 1, it is characterised in that: the stirring rod
(17) and paddle (18) is hollow structure, and stirring rod (17) and paddle (18) are integrated, and stirring rod
(17) and on paddle (18) it is evenly distributed with gas vent (19).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821095034.3U CN208642454U (en) | 2018-07-11 | 2018-07-11 | A kind of high-purity production of chloroacetic acid stock stirring device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821095034.3U CN208642454U (en) | 2018-07-11 | 2018-07-11 | A kind of high-purity production of chloroacetic acid stock stirring device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208642454U true CN208642454U (en) | 2019-03-26 |
Family
ID=65784487
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821095034.3U Expired - Fee Related CN208642454U (en) | 2018-07-11 | 2018-07-11 | A kind of high-purity production of chloroacetic acid stock stirring device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208642454U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110270253A (en) * | 2019-05-09 | 2019-09-24 | 徐倩荣 | A kind of chemical industry emulsifying kettle improving emulsifying power |
| CN113845435A (en) * | 2021-10-14 | 2021-12-28 | 四川吉隆达生物科技集团有限公司 | Production process of feed-grade manganese glutamate |
-
2018
- 2018-07-11 CN CN201821095034.3U patent/CN208642454U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110270253A (en) * | 2019-05-09 | 2019-09-24 | 徐倩荣 | A kind of chemical industry emulsifying kettle improving emulsifying power |
| CN113845435A (en) * | 2021-10-14 | 2021-12-28 | 四川吉隆达生物科技集团有限公司 | Production process of feed-grade manganese glutamate |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190326 Termination date: 20200711 |