CN208641776U - Orthophosphoric acid dehydration handles special heating furnace - Google Patents

Orthophosphoric acid dehydration handles special heating furnace Download PDF

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Publication number
CN208641776U
CN208641776U CN201821325464.XU CN201821325464U CN208641776U CN 208641776 U CN208641776 U CN 208641776U CN 201821325464 U CN201821325464 U CN 201821325464U CN 208641776 U CN208641776 U CN 208641776U
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CN
China
Prior art keywords
burner hearth
shaft
phosphoric acid
rotating shaft
bearing
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Expired - Fee Related
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CN201821325464.XU
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Chinese (zh)
Inventor
陆建国
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Shifang Zhi Mou Chemical Co Ltd
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Shifang Zhi Mou Chemical Co Ltd
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Priority to CN201821325464.XU priority Critical patent/CN208641776U/en
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Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses orthophosphoric acid dehydrations to handle special heating furnace, the burner hearth including upper end opening, and bell is arranged in burner hearth upper end, and bell is detachably connected with burner hearth;Furnace body is set inside burner hearth, the opposite sides of furnace body is respectively fixedly connected with first rotating shaft, the second shaft, the axis collinear of first rotating shaft, the second shaft, and the angle of first rotating shaft, the axis of the second shaft and horizontal plane is 10~15 °, first rotating shaft is pierced by burner hearth sidewall and is connected with rotating mechanism, burner hearth inner sidewall also fixed bearing block installs second bearing on bearing block, and the second shaft is connected with second bearing;The side bottom of burner hearth also sets up thorax door, thorax door and bearing seat on the ipsilateral side wall of burner hearth.Mobility is uneven, there are laminations to solve in phosphoric acid dehydration in the prior art for the utility model, the phosphoric acid of bottom can lead to the problem of strong interference to the phosphoric acid on top, realization avoids lower part phosphoric acid from generating interference to top phosphoric acid, improves the purpose of phosphoric acid dehydration efficiency.

Description

Orthophosphoric acid dehydration handles special heating furnace
Technical field
The utility model relates to chemical fields, and in particular to orthophosphoric acid dehydration handles special heating furnace.
Background technique
Phosphoric acid or orthophosphoric acid, chemical formula H3PO4, molecular weight 97.994 is a kind of common inorganic acid, is middle strong acid.By Phosphorus pentoxide, which is dissolved in hot water, can be obtained.Orthophosphoric acid industrially uses sulfuric acid treatment apatite to obtain the final product.Phosphoric acid holds in air Easily deliquesce.Heating meeting dehydration obtains pyrophosphoric acid, and further dehydration obtains metaphosphoric acid.Phosphoric acid is mainly used for pharmacy, food, fertilizer Equal industry, including as antirust agent, food additives, dentistry and orthopaedic srugery, EDIC corrosive agent, electrolyte, scaling powder, dispersion Agent, industrial corrosion agent, the raw material and component household cleaning product of fertilizer.It also is used as chemical reagent, phosphate is all life The nutrition of form.Studying the earliest chemist of phosphoric acid is french chemist Antoine Lavoisier.1772, he did such experiment: by phosphorus It is placed on to make its burning in the bell jar of mercury sealing.Experimental result and reach a conclusion that a certain amount of phosphorus can burn Mr. Yu appearance In the air of amount;Phosphorus generates the white powder piece of anhydrous phosphorus when burning, as thin snow;The about surplus original appearance of air after burning in bottle The 80% of amount;2.5 times are nearly weighed before relatively burning after phosphorus burning;White powder piece be dissolved in water phosphoric acid.Antoine Lavoisier also confirms that phosphoric acid can It is made with concentrated nitric acid and phosphorus reaction.More than 100 years have about been spent, German chemist Li Bixi has done the experiment of many agriculture chemistry, Phosphorus and phosphoric acid are opened to the value of plant life." organic chemistry is in agricultural and physiological effect " written by Li Bixi in 1840 In, the fertility problem of soil is scientifically demonstrated, and point out effect of the phosphorus to plant.Meanwhile he has also further probed into phosphoric acid And application of the phosphate as fertilizer, enter the large-scale epoch from the production of this phosphoric acid.The production process of phosphoric acid is always by original The regional impact of material, the production of China's phosphoric acid are concentrated mainly on Yunnan, Sichuan, acid solution and are easy during the dehydration process according to glutinous Property layering, form that bottom is very viscous and Guizhou, Hubei are flowed in top, in the secondary operation of phosphoric acid, thermal dehydration is system Standby one of pyrophosphoric acid, the main method of metaphosphoric acid, however phosphoric acid dehydration device in the prior art, mostly with traditional smelting furnace For prototype, then add additional diversing flow system.Phosphorus is in relatively steady state, and which results in bottoms in phosphoric acid dehydration Viscous phosphoric acid can the preferable phosphoric acid of mobility to top generate stronger interference, influence the dehydration efficiency of top phosphoric acid.
Utility model content
The purpose of this utility model is to provide orthophosphoric acid dehydrations to handle special heating furnace, to solve phosphoric acid in the prior art In dehydration mobility it is uneven, there are lamination, the phosphoric acid of bottom can lead to the problem of strong interference to the phosphoric acid on top, Realization avoids lower part phosphoric acid from generating interference to top phosphoric acid, improves the purpose of phosphoric acid dehydration efficiency.
The utility model is achieved through the following technical solutions:
Orthophosphoric acid dehydration handles special heating furnace, the burner hearth including upper end opening, and bell, bell and furnace is arranged in burner hearth upper end Thorax is detachably connected;Furnace body is set inside the burner hearth, and the opposite sides of furnace body is respectively fixedly connected with first rotating shaft, second turn Axis, the axis collinear of the first rotating shaft, the second shaft, and the angle of first rotating shaft, the axis of the second shaft and horizontal plane is 10~15 °, the first rotating shaft is pierced by burner hearth sidewall and is connected with rotating mechanism, and the rotating mechanism is for driving first rotating shaft Along own axis, the burner hearth inner sidewall also fixed bearing block installs second bearing on bearing block, second shaft with The second bearing is connected;Expects pipe is arranged close to one end of the second shaft in the furnace body, and valve is arranged in the expects pipe;The furnace The side bottom of thorax also sets up thorax door, and the thorax door and the bearing seat are on the ipsilateral side wall of burner hearth.
For mobility in phosphoric acid dehydration in the prior art is uneven, there are laminations, the phosphoric acid of bottom can be to upper The phosphoric acid in portion leads to the problem of strong interference, and the utility model proposes orthophosphoric acid dehydrations to handle special heating furnace, and rotating mechanism is used In driving first rotating shaft rotation, first rotating shaft drives the furnace body in burner hearth to be rotated, while the second shaft is rotated therewith, Second shaft keeps stablizing under the action of bearing block and second bearing, thus by first rotating shaft, the second shaft simultaneously to furnace Body is carried, it is ensured that furnace body being capable of smooth rotation.The angle of first rotating shaft, the axis of the second shaft and horizontal plane is 10~ 15 °, therefore furnace body can also be rotated along the axis horizontal by 10~15 °.Expects pipe passes through valve for feeding and discharging Door control its shutdown, thorax door be in the prior art arbitrarily can with the door of opening and closing, metallic door preferably resistant to high temperature, For feeding.It in the utility model specific work process, is heated in burner hearth, is turned by rotating mechanism driving furnace body It is dynamic, furnace body along and horizontal plane angle be 10~15 ° axis rotated so that the liquid phosphoric acid of furnace interior is by whipping, Under the influence of centrifugal force, liquid constantly carry out whipping with mix so that the phosphoric acid of poor fluidity and good fluidity Phosphoric acid can always in the mixed process, entire thermal dehydration process remain at phosphoric acid solution more uniformly in the state of It carries out, to solve in phosphoric acid dehydration in the prior art, layering is serious, upper flow is good, lower flow is poor, on Phosphoric acid dehydration efficiency low problem in portion's realizes and lower part phosphoric acid is avoided to generate interference to top phosphoric acid, improves phosphoric acid dehydration effect The purpose of rate.In the utility model, the angle of first rotating shaft, the axis of the second shaft and horizontal plane is 10~15 ° and needs strictly Control, angle is too small, is difficult to for product being quickly discharged by expects pipe after the completion of dehydration, and angle is excessive, and centrifugal force is dry by gravity It disturbs greatly, whipping mixed effect is poor, and the effect for causing the utility model to improve efficiency is unobvious.
Several jacks are arranged in the roof of the furnace, and several protrusions, the protrusion and the jack is arranged in the bell bottom Match, lifting lug is set at the top of the bell.It is carried out detachably between burner hearth and bell by the jack and protrusion that are mutually matched Connection.Lifting lug is for slinging bell.
The burner hearth lateral wall fixed mounting plate, the mounting plate is for installing rotating mechanism.Mounting plate is rotating mechanism Installation station is provided, while carrying out carrying and stress.
The rotating mechanism is stepper motor.
The position that the first rotating shaft passes through burner hearth sidewall is arranged first bearing, is fixed on furnace on the outside of the first bearing In thorax side wall.The stability in first rotating shaft rotation process is improved by first bearing.
The utility model compared with prior art, has the following advantages and benefits:
The utility model orthophosphoric acid dehydration handles special heating furnace, and entire thermal dehydration process remains at phosphoric acid solution More uniformly in the state of carry out, thus solve be layered in phosphoric acid dehydration in the prior art serious, upper flow is good, Lower flow is poor, the low problem of top phosphoric acid dehydration efficiency, realizes and lower part phosphoric acid is avoided to generate interference to top phosphoric acid, Improve the purpose of phosphoric acid dehydration efficiency.
Detailed description of the invention
Attached drawing described herein is used to provide to further understand the utility model embodiment, constitutes the one of the application Part does not constitute the restriction to the utility model embodiment.In the accompanying drawings:
Fig. 1 is the structural schematic diagram of the utility model specific embodiment.
Label and corresponding parts title in attached drawing:
1- burner hearth, 2- bell, 3- furnace body, 4- first rotating shaft, the second shaft of 5-, 6- rotating mechanism, 7- bearing block, 8- second Bearing, 9- expects pipe, 10- valve, 11- thorax door, 12- jack, 13- protrusion, 14- lifting lug, 15- mounting plate, 16- first bearing.
Specific embodiment
For the purpose of this utility model, technical solution and advantage is more clearly understood, below with reference to embodiment and attached drawing, The utility model is described in further detail, and the exemplary embodiment and its explanation of the utility model are only used for explaining this Utility model is not intended to limit the scope of the present invention.
Embodiment 1:
Orthophosphoric acid dehydration as shown in Figure 1 handles special heating furnace, the burner hearth 1 including upper end opening, the setting of 1 upper end of burner hearth Bell 2, bell 2 are detachably connected with burner hearth 1;Furnace body 3 is set inside the burner hearth 1, and the opposite sides of furnace body 3 is fixed respectively to be connected Connect first rotating shaft 4, the second shaft 5, the axis collinear of the first rotating shaft 4, the second shaft 5, and first rotating shaft 4, the second shaft 5 Axis and the angle of horizontal plane be 12 °, the first rotating shaft 4 is pierced by 1 side wall of burner hearth and is connected with rotating mechanism 6, the rotation Rotation mechanism 6 is for driving first rotating shaft 4 along own axis, 1 inner sidewall of burner hearth also fixed bearing block 7, on bearing block 7 Second bearing 8 is installed, second shaft 5 is connected with the second bearing 8;The furnace body 3 is set close to one end of the second shaft 5 Expects pipe 9 is set, valve 10 is set in the expects pipe 9;The side bottom of the burner hearth 1 also sets up thorax door 11, the thorax door 11 and institute Bearing block 7 is stated to be located on the ipsilateral side wall of burner hearth 1.
Embodiment 2:
Orthophosphoric acid dehydration processing special heating furnace as shown in Figure 1 is set at the top of the burner hearth 1 on the basis of embodiment 1 Several jacks 12 are set, 2 bottom of the bell setting several raised 13, described raised 13 matches with the jack 12, the furnace Lifting lug 14 is set at the top of lid 2.The 1 lateral wall fixed mounting plate 15 of burner hearth, the mounting plate 15 is for installing rotating mechanism 6. The rotating mechanism 6 is stepper motor.The position that the first rotating shaft 4 passes through 1 side wall of burner hearth is arranged first bearing 16, and described the The outside of one bearing 16 is fixed in 1 side wall of burner hearth.
Above-described specific embodiment, to the purpose of this utility model, technical scheme and beneficial effects carried out into One step is described in detail, it should be understood that being not used to limit the foregoing is merely specific embodiment of the present utility model Determine the protection scope of the utility model, within the spirit and principle of the utility model, any modification for being made equally is replaced It changes, improve, should be included within the scope of protection of this utility model.

Claims (5)

1. orthophosphoric acid dehydration handles special heating furnace, which is characterized in that the burner hearth (1) including upper end opening, burner hearth (1) upper end are set It sets bell (2), bell (2) is detachably connected with burner hearth (1);Furnace body (3) are set inside the burner hearth (1), furnace body (3) it is opposite Two sides are respectively fixedly connected with first rotating shaft (4), the second shaft (5), and the first rotating shaft (4), the axis of the second shaft (5) are total Line, and the angle of first rotating shaft (4), the axis of the second shaft (5) and horizontal plane is 10~15 °, the first rotating shaft (4) is pierced by Burner hearth (1) side wall is simultaneously connected with rotating mechanism (6), and the rotating mechanism (6) is for driving first rotating shaft (4) to turn along own axes It moves, burner hearth (1) inner sidewall also fixed bearing block (7), second bearing (8) is installed on bearing block (7), second shaft (5) it is connected with the second bearing (8);Expects pipe (9) are arranged close to the one end of the second shaft (5) in the furnace body (3), the expects pipe (9) valve (10) are set on;The side bottom of the burner hearth (1) is also set up thorax door (11), the thorax door (11) and the bearing Seat (7) is located on the ipsilateral side wall of burner hearth (1).
2. orthophosphoric acid dehydration according to claim 1 handles special heating furnace, which is characterized in that at the top of the burner hearth (1) It is arranged several jacks (12), bell (2) the bottom setting is several raised (13), the protrusion (13) and the jack (12) phase Lifting lug (14) are arranged in matching, bell (2) top.
3. orthophosphoric acid dehydration according to claim 1 handles special heating furnace, which is characterized in that on the outside of the burner hearth (1) Wall fixed mounting plate (15), the mounting plate (15) is for installing rotating mechanism (6).
4. orthophosphoric acid dehydration according to claim 1 handles special heating furnace, which is characterized in that the rotating mechanism (6) For stepper motor.
5. orthophosphoric acid dehydration according to claim 1 handles special heating furnace, which is characterized in that the first rotating shaft (4) Position across burner hearth (1) side wall is arranged first bearing (16), and burner hearth (1) side wall is fixed on the outside of the first bearing (16) It is interior.
CN201821325464.XU 2018-08-15 2018-08-15 Orthophosphoric acid dehydration handles special heating furnace Expired - Fee Related CN208641776U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821325464.XU CN208641776U (en) 2018-08-15 2018-08-15 Orthophosphoric acid dehydration handles special heating furnace

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821325464.XU CN208641776U (en) 2018-08-15 2018-08-15 Orthophosphoric acid dehydration handles special heating furnace

Publications (1)

Publication Number Publication Date
CN208641776U true CN208641776U (en) 2019-03-26

Family

ID=65790191

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821325464.XU Expired - Fee Related CN208641776U (en) 2018-08-15 2018-08-15 Orthophosphoric acid dehydration handles special heating furnace

Country Status (1)

Country Link
CN (1) CN208641776U (en)

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190326

Termination date: 20190815

CF01 Termination of patent right due to non-payment of annual fee