CN208525866U - A kind of bead tube, rectifying column and rectifying plate - Google Patents

A kind of bead tube, rectifying column and rectifying plate Download PDF

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Publication number
CN208525866U
CN208525866U CN201821045269.1U CN201821045269U CN208525866U CN 208525866 U CN208525866 U CN 208525866U CN 201821045269 U CN201821045269 U CN 201821045269U CN 208525866 U CN208525866 U CN 208525866U
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China
Prior art keywords
tube
bead tube
bead
rectifying
diameter
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CN201821045269.1U
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Chinese (zh)
Inventor
应盛荣
姜战
应悦
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Dingsheng Chemical & Technology Co Ltd
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Dingsheng Chemical & Technology Co Ltd
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Abstract

The utility model is to be related to a kind of bead tube, rectifying column and rectifying plate, and wherein bead tube includes: tube body, is equipped with gaseous phase outlet in the upper end of the tube body, lower end is equipped with liquid/vapor import, and material inlet and phegma import are equipped on the side wall of the tube body;The tube body is equipped with several float chambers, and floating ball is equipped in the float chamber;The diameter of the floating ball is less than the internal diameter of float chamber.Beneficial effect is: structure is simple, and manufacturing cost is low;Using multiple floating ball cell structures for being built-in with floating ball, mass-transfer efficiency is high, can substantially reduce rectifier unit height, can be placed in interior, improve its working environment.Can be mating with micro passage reaction, form miniature chemical production device;Compensate for the deficiency of the rectifying device of micro- chemical field.Bead tube can used aloned, be also combined into a row use, can also be combined into array use;Wide adaptability;Processing capacity is changeable, is easily mastered, convenient for adjusting.

Description

A kind of bead tube, rectifying column and rectifying plate
Technical field
The utility model relates to chemical technology fields, more particularly, to a kind of bead tube, rectifying column and rectifying plate, especially It is a kind of bead tube, rectifying column and rectifying plate applied to micro- chemical field.
Background technique
Rectifying column is one of most important equipment in the production such as chemical industry, medicine, it can make gas (or vapour) or liquid-liquid diphase It is in close contact, achievees the purpose that interphase mass transfer and heat transfer, as the tower for being mainly used for mass transport process it may first have to make gas (vapour) liquid two-phase can come into full contact with, and to obtain high mass-transfer efficiency, while the performance of tower produces the product of whole device The everyways such as amount, quality, production capacity and the norm quota of consumption and three-protection design and environmental protection have significant impact.
The most common rectifying column is plate column and packed tower two major classes;Packed tower is divided into monomer dumped packing again and regular fills out Material;The existing general diameter of rectifying column is in DN100 or more, several meters of rectifying tower height degree to rice up to a hundred, it is bulky, manufacturing cost is high, Safety is poor, inconvenient for operation, maintenance difficult, maintenance cost are high.
In recent years, with " transport " progress of research under minute yardstick, the performance of minute yardstick fluid has obtained deeply taking off Show, micro- Chemical Engineering Technology is greatly developed as a new developing direction in Chemical waste-water, is also widely used for Scientific research and field of industrial production.But the missing of matching rectifying device limits always the development of micro- Chemical Engineering Technology, passes The trend that system rectifying column develops to microchannel rectifying column is extremely urgent.
In view of this, it is necessary to research and develop a kind of bead tube, rectifying column and rectifying plate, be particularly applied to micro- chemical field Bead tube, rectifying column and rectifying plate, to make up the deficiency in the rectifying device of micro- chemical field.
Utility model content
The utility model provides a kind of bead tube, rectifying column and rectifying plate, is specially adapted to micro- chemical field.
A kind of bead tube, rectifying column and rectifying plate of the utility model, solve the diameter of rectifying column in the prior art Greatly, the problems such as volume is big, manufacturing cost is high, safety is poor, inconvenient for operation.
The technical problem solved by the utility model is implemented by the following technical solutions:
A kind of bead tube, comprising: tube body, the upper end of the tube body be equipped with gaseous phase outlet, lower end be equipped with liquid/vapor into Mouthful, material inlet and phegma import are equipped on the side wall of the tube body;
Wherein, the tube body is equipped with several float chambers, and floating ball is equipped in the float chamber;The diameter of the floating ball Less than the internal diameter of float chamber.
Straight pipe, the internal diameter of the straight pipe are equipped between the two neighboring float chamber as a preferred technical solution, Less than the diameter of floating ball.Wherein, the straight pipe is spaced apart with float chamber, and is sequentially communicated.
The internal diameter of the straight pipe is 0.9~0.1 times of float chamber's diameter as a preferred technical solution,.
The floating ball diameter is 0.99~0.15 times of float chamber's diameter as a preferred technical solution,.
Float chamber's diameter is 0.01mm~50mm as a preferred technical solution,.Further, the float chamber is straight Diameter is 0.01mm~1mm, to be suitable for the rectifying of macro work.
The tube body is the cylinder structure or the isometrical cylinder structure of outer diameter of equal wall thickness as a preferred technical solution,.Institute State tube body using etc. wall thickness cylinder structure or outer diameter isometrical cylinder structure when, handling ease is easy to make, can pass through blowing Mode or impact style or the machine-shapings such as cutting way or etching mode.
The phegma import is positioned close at the gaseous phase outlet as a preferred technical solution,.
Rectifying material outlet is additionally provided on the tube body as a preferred technical solution,.
The liquid/vapor import is connected with rectifying still as a preferred technical solution,;The gaseous phase outlet and condenser It is connected.
The utility model also proposed a kind of rectifying column, including tower body and the essence being made of multiple above-mentioned bead tubes Distillation unit, the orderly array of the bead tube is in the tower body.
The bead tube in the rectifier unit circularizes array as a preferred technical solution,.
The rectangular array of bead tube in the rectifier unit as a preferred technical solution,.
The utility model also proposed a kind of rectifying plate, be made of including plate body and a row multiple above-mentioned bead tubes Rectifier unit, the bead tube is orderly to be arranged in the plate body.
The bead tube arranged in parallel is in the plate body as a preferred technical solution,.
The utility model has the beneficial effect that
1) structure is simple, and manufacturing cost is low;Using multiple floating ball cell structures for being built-in with floating ball, mass-transfer efficiency is high, can Rectifier unit height is substantially reduced, can be placed in interior, improves its working environment.
2) can be mating with micro passage reaction, form miniature chemical production device;The rectifying for compensating for micro- chemical field is set Standby deficiency.
3) bead tube can used aloned, be also combined into a row use, can also be combined into array use;Wide adaptability; Processing capacity is changeable, is easily mastered, convenient for adjusting.
Detailed description of the invention
It, below will be to implementation in order to illustrate more clearly of the utility model embodiment or technical solution in the prior art Scheme or attached drawing needed to be used in the description of the prior art are briefly described, it should be apparent that, the accompanying drawings in the following description Only some embodiments of the utility model are not making the creative labor for those of ordinary skill in the art Under the premise of property, it is also possible to obtain other drawings based on these drawings.
Fig. 1 is the utility model: a kind of the first structural schematic diagram of bead tube;
Fig. 2 is the utility model: a kind of second of structural schematic diagram of bead tube;
Fig. 3 a is a kind of the utility model: structural schematic diagram of the rectangular array of rectifying column;
Fig. 3 b is a kind of the utility model: structural schematic diagram of the annular array of rectifying column;
Fig. 4 is the utility model: a kind of structural schematic diagram of rectifying plate.
Specific embodiment
In order to be easy to understand the technical means, creative features, achievement of purpose, and effectiveness of the utility model, under Face combines and is specifically illustrating, and the utility model is further described.
Embodiment 1
Shown in referring to Fig.1, a kind of bead tube, comprising: tube body 1 is equipped with gaseous phase outlet 11 in the upper end of tube body 1, and lower end is set There is liquid/vapor import 12, material inlet 13 and phegma import 14 are equipped on the side wall of tube body 1;Wherein, it is set on tube body 1 There are several float chambers 2, floating ball 3 is equipped in float chamber 2;The diameter of floating ball 3 is less than the internal diameter of float chamber 2.
Above-mentioned tubular body can wait the cylinder structure of wall thickness or the isometrical cylinder structure of outer diameter.When the pipe of the wall thickness such as tube body use When type structure or the isometrical cylinder structure of outer diameter, handling ease is easy to make, by blowing mode or impact style or can cut Cut the machine-shapings such as mode or etching mode.The cylinder structure of the wall thickness such as the use of tube body 1 in the present embodiment.It can be one It is body formula or split knockdown.
Straight pipe 4 is equipped in the present embodiment between two neighboring float chamber 2, the internal diameter of straight pipe 4 is less than the straight of floating ball 3 Diameter, wherein straight pipe 4 is spaced apart with float chamber 2, and is sequentially communicated.Of course, straight pipe 4 and float chamber 2 are spaced apart Mode can be 12 → 1 sections of float chamber, 2 → 1 sections of the float chamber of straight pipe 4 → 1 straight pipe 4, or continuous 2 or 2 → 1 sections of multiple float chambers straight pipe 4 → 2 or 2 → 1 sections of multiple float chambers straight pipe 4, setting in this way can To improve material distillation process number in limited height.Further, it can also be not provided between two neighboring float chamber 2 Straight pipe 4 can reduce the height of this bead tube in this way.
The internal diameter of the straight pipe 4 of the utility model is 0.9~0.1 times of 2 diameter of float chamber, and 3 diameter of floating ball is float chamber 2 0.99~0.15 times of diameter.Floating ball 3 can only float in float chamber 2 in this way, by 2 inner wall of float chamber, 3 body surface face of floating ball, The gas-liquid two-phase of 4 inner wall of straight pipe contacts, and carries out the high-efficient of mass-and heat-transfer amount.
2 diameter of float chamber of the utility model is 0.01mm~50mm.Further, 2 diameter of float chamber be 0.01mm~ 1mm, to be suitable for the rectifying of macro work.Since the rectifying of micro- chemical field does not need very big flow, the utility model The diameter of the float chamber 2 of design is not necessarily in 10MM or more.
The phegma import 14 of the utility model is positioned close at gaseous phase outlet 11, and rectifying material is additionally provided on tube body 1 Outlet 15.Liquid/vapor import 12 is connected with rectifying still;Gaseous phase outlet 11 is connected with condenser.
Specifically, in use, liquid/vapor import 12 and the rectifying still phase of the bead tube lower end of the utility model Even;Gaseous phase outlet 11 is connected with condenser, and the gas phase come out from rectifying still sequentially passes through float chamber 2, straight pipe 4, due to floating Floating ball 3 is equipped in ball room 2, gas phase is in contact with 2 inner wall of float chamber, 3 body surface face of floating ball, 4 inner wall of straight pipe, carries out mass transfer biography Heat realizes rectifying separation.Gas phase after separation is entered in condenser by gaseous phase outlet 11 to be condensed, condensed liquid A part is turned again to by phegma import 14 and carries out abundant rectifying in bead tube, to realize more preferable, more accurate rectifying point From.
Embodiment 2
Referring to shown in Fig. 2, unlike the first embodiment, the tube body 1 of the utility model cylinder structure isometrical using outer diameter When, handling ease, float chamber 2 can be formed with etching mode.
Embodiment 3
Referring to Fig. 3 a, shown in 3b, the utility model also proposed a kind of rectifying column, including tower body 100 and by multiple The rectifier unit 200 that the bead tube 10 stated forms, the orderly array of bead tube is in tower body 100.
Wherein, the bead tube 10 in rectifier unit 200 circularizes array (such as Fig. 3 a) or rectangular array (such as Fig. 3 b). Above-mentioned array manner can be selected according to the different structure of rectifying column.
Embodiment 4
Referring to shown in Fig. 4, the utility model also proposed a kind of rectifying plate, including plate body 300 and a row are by multiple The rectifier unit 200 that the bead tube 10 stated forms, bead tube 20 is orderly to be arranged in plate body 300.Wherein, bead tube 10 is simultaneously Townhouse is distributed in plate body 300.
The basic principles and main features of the present invention and the advantages of the present invention have been shown and described above.Current row The technical staff of industry is described in above embodiments and description it should be appreciated that the present utility model is not limited to the above embodiments Only illustrate the principles of the present invention, on the premise of not departing from the spirit and scope of the utility model, the utility model is also It will have various changes and improvements, these various changes and improvements fall within the scope of the claimed invention.The utility model Claimed range is defined by the appending claims and its equivalent thereof.

Claims (15)

1. a kind of bead tube, comprising: tube body, the upper end of the tube body be equipped with gaseous phase outlet, lower end be equipped with liquid/vapor into Mouthful, material inlet and phegma import are equipped on the side wall of the tube body;
It is characterized in that, the tube body is equipped with several float chambers, floating ball is equipped in the float chamber;The floating ball it is straight Diameter is less than the internal diameter of float chamber.
2. a kind of bead tube according to claim 1, which is characterized in that be equipped with straight tube between the two neighboring float chamber Section, the internal diameter of the straight pipe are less than the diameter of floating ball.
3. a kind of bead tube according to claim 2, which is characterized in that the straight pipe is spaced apart with float chamber, and It is sequentially communicated.
4. a kind of bead tube according to claim 2, which is characterized in that the internal diameter of the straight pipe is float chamber's diameter 0.9~0.1 times.
5. a kind of bead tube according to claim 1, which is characterized in that the floating ball diameter is the 0.99 of float chamber's diameter ~0.15 times.
6. a kind of bead tube according to claim 1, which is characterized in that float chamber's diameter is 0.01mm~50mm.
7. a kind of bead tube according to claim 1, which is characterized in that the tube body is the cylinder structure or outer of equal wall thickness The isometrical cylinder structure of diameter.
8. a kind of bead tube according to claim 1, which is characterized in that the phegma import is positioned close to the gas Phase exit.
9. a kind of bead tube according to claim 1, which is characterized in that be additionally provided with rectifying material outlet on the tube body.
10. a kind of bead tube according to claim 1, which is characterized in that the liquid/vapor import and rectifying still phase Even;The gaseous phase outlet is connected with condenser.
11. a kind of rectifying column, which is characterized in that including tower body and by multiple as claim 1-10 any one right is wanted The rectifier unit for asking the bead tube to form, the orderly array of the bead tube is in the tower body.
12. a kind of rectifying column according to claim 11, which is characterized in that the bead tube in the rectifier unit circularizes Array.
13. a kind of rectifying column according to claim 11, which is characterized in that the bead tube in the rectifier unit is rectangular Array.
14. a kind of rectifying plate, including plate body and a row as multiple as described in claim 1-10 any one claim The rectifier unit of bead tube composition, the bead tube is orderly to be arranged in the plate body.
15. a kind of rectifying plate according to claim 14, which is characterized in that the bead tube arranged in parallel is in the plate body It is interior.
CN201821045269.1U 2018-07-03 2018-07-03 A kind of bead tube, rectifying column and rectifying plate Active CN208525866U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821045269.1U CN208525866U (en) 2018-07-03 2018-07-03 A kind of bead tube, rectifying column and rectifying plate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821045269.1U CN208525866U (en) 2018-07-03 2018-07-03 A kind of bead tube, rectifying column and rectifying plate

Publications (1)

Publication Number Publication Date
CN208525866U true CN208525866U (en) 2019-02-22

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Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108579116A (en) * 2018-07-03 2018-09-28 衢州市鼎盛化工科技有限公司 A kind of bead tube, rectifying column and rectifying plate

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108579116A (en) * 2018-07-03 2018-09-28 衢州市鼎盛化工科技有限公司 A kind of bead tube, rectifying column and rectifying plate

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