CN208420463U - A kind of automatic sampling device during chemical industry synthesis - Google Patents

A kind of automatic sampling device during chemical industry synthesis Download PDF

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Publication number
CN208420463U
CN208420463U CN201821151725.0U CN201821151725U CN208420463U CN 208420463 U CN208420463 U CN 208420463U CN 201821151725 U CN201821151725 U CN 201821151725U CN 208420463 U CN208420463 U CN 208420463U
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CN
China
Prior art keywords
sampling room
sampling
room
chemical industry
glass tube
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Expired - Fee Related
Application number
CN201821151725.0U
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Chinese (zh)
Inventor
孙维军
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Lanzhou New Vanke Instrument Equipment Co Ltd
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Lanzhou New Vanke Instrument Equipment Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
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Priority to CN201821151725.0U priority Critical patent/CN208420463U/en
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Publication of CN208420463U publication Critical patent/CN208420463U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses the automatic sampling devices during a kind of chemical industry synthesis, including sampling room, the bottom of the sampling room is communicated with setting-out pipe, the inside of the sampling room is equipped with heating tape, the side of the sampling room is equipped with support plate, aspiration pump is fixedly installed at the top of the support plate, the output end of the aspiration pump is connected to sampling room, the other side of the sampling room is equipped with glass tube and pressure gauge, the pressure gauge is located at the top of glass tube, and the bottom of the glass tube is connected to the bottom of sampling room.The utility model cleans the inside of sampling room adequately, prevent influence of the residue to inspection result, pass through setting heating tape and temperature sensor, make sampling room after the washing and can dry the moisture inside sampling room, and sampling room is internally heated, make the equalized temperature of the temperature and reaction kettle inside sampling room, to prevent the measurement result because of temperature difference to compound.

Description

A kind of automatic sampling device during chemical industry synthesis
Technical field
The utility model relates to the automatic sampling dresses during sampler technical field more particularly to a kind of chemical industry synthesis It sets.
Background technique
Sampling refers to the process of extracts individual or sample from totality, namely to the overall process tested or observed, Divide random sampling and nonrandom sampling two types, the former refers to the sampling side in accordance with randomization sample drawn from totality Method, it is without any subjectivity, including simple random sampling, systematic sampling, chester sampling and stratified sampling.
There are some more mature samplers in chemical industry synthesis at present, it when in use, will be in sampler Probe tube be placed in material, be sampled, general sampler after sampling, after a period of time carry out next time Sampling, but is easy remaining chemicals among probe tube and sampling room, and during being sampled sampling room and reaction kettle it Between temperature change differ greatly, be easy to cause measurement result inaccurate.
Summary of the invention
Purpose of the utility model is to solve disadvantages existing in the prior art, and a kind of chemical industry synthesis mistake proposed Automatic sampling device in journey.
To achieve the goals above, the utility model adopts the technical scheme that
A kind of automatic sampling device during chemical industry synthesis, including sampling room, the bottom of the sampling room, which is communicated with, puts Sample pipe, the inside of the sampling room are equipped with heating tape, and the side of the sampling room is equipped with support plate, the top of the support plate Portion is fixedly installed with aspiration pump, and the output end of the aspiration pump is connected to sampling room, and the other side of the sampling room is equipped with glass Pipe and pressure gauge, the pressure gauge are located at the top of glass tube, and the bottom of the glass tube is connected to the bottom of sampling room, described Temperature sensor, motor and water injection hole are provided at the top of sampling room, the motor between temperature sensor and water injection hole, For the temperature sensor completely through the top of sampling room, the inside of the water injection hole is equipped with rubber stopper, the output of the motor End is connected with spinner handle, and for the spinner handle completely through the top of sampling room, the surface of the spinner handle is equipped with paddle, the paddle Positioned at the inside of sampling room, the side of the sampling room is communicated with probe tube, is communicated with back between the probe tube and setting-out pipe The side of flow tube, the probe tube is equipped with drainpipe.
Preferably, the setting-out pipe, probe tube, return pipe, drainpipe surface be equipped with valve.
Preferably, the quantity of the paddle is three, and three paddles are with the centre symmetry line of spinner handle circumferentially battle array Column arrangement.
Preferably, the glass tube is L shape, and the top of glass tube seals, and the surface of glass tube is equipped with graduation mark.
Preferably, the model WZP-187 of the temperature sensor.
Compared with prior art, the utility model has the beneficial effects that
It by setting motor, spinner handle, paddle and water injection hole in the utility model, incite somebody to action sampling room can after sampling Cleaning solution is sufficiently merged with remaining compound, then is excluded from drainpipe, thus clean the inside of sampling room adequately, Influence of the residue to inspection result is prevented, by setting heating tape and temperature sensor, makes sampling room after the washing can be with The moisture inside sampling room is dried, and sampling room is internally heated, makes the temperature of the temperature and reaction kettle inside sampling room Balance, to prevent the measurement result because of temperature difference to compound.
Detailed description of the invention
Fig. 1 be the utility model proposes a kind of chemical industry synthesis during automatic sampling device structural schematic diagram;
Fig. 2 be the utility model proposes a kind of chemical industry synthesis during automatic sampling device top view.
In figure: 1 sampling room, 2 setting-out pipes, 3 heating tapes, 4 glass tubes, 5 support plates, 6 aspiration pumps, 7 temperature sensors, 8 electricity Machine, 9 water injection holes, 10 pressure gauges, 11 spinner handles, 12 paddles, 13 probe tubes, 14 return pipes, 15 drainpipes.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.
Referring to Fig.1-2, the automatic sampling device during a kind of chemical industry synthesis, including sampling room 1, the bottom of sampling room 1 It is communicated with setting-out pipe 2, the inside of sampling room 1 is equipped with heating tape 3, and the side of sampling room 1 is equipped with support plate 5, support plate 5 Top is fixedly installed with aspiration pump 6, and the output end of aspiration pump 6 is connected to sampling room 1, and the other side of sampling room 1 is equipped with glass tube 4 With pressure gauge 10, glass tube 4 is L shape, and the top of glass tube 4 seals, and the surface of glass tube 4 is equipped with graduation mark, pressure gauge 10 Positioned at the top of glass tube 4, the bottom of glass tube 4 is connected to the bottom of sampling room 1, and the top of sampling room 1 is provided with temperature biography Sensor 7, motor 8 and water injection hole 9, motor 8 is between temperature sensor 7 and water injection hole 9, and temperature sensor 7 is completely through taking The inside at the top of specimen chamber 1, the model WZP-187 of temperature sensor 7, water injection hole 9 is equipped with rubber stopper, the output end of motor 8 It is connected with spinner handle 11, for spinner handle 11 completely through the top of sampling room 1, the surface of spinner handle 11 is equipped with paddle 12, and paddle 12 In the inside of sampling room 1, the quantity of paddle 12 is three, and three paddles 12 with the centre symmetry line of spinner handle 11 circumferentially Array arrangement, the side of sampling room 1 are communicated with probe tube 13, return pipe 14 are communicated between probe tube 13 and setting-out pipe 2, sample The side of pipe 13 be equipped with drainpipe 15, setting-out pipe 2, probe tube 13, return pipe 14, drainpipe 15 surface be equipped with valve, lead to Cross setting motor 8, spinner handle 11, paddle 12 and water injection hole 9, make sampling room 1 after sampling can by cleaning solution with it is remaining Compound sufficiently merges, then excludes from drainpipe 15, so that the inside of sampling room 1 be made adequately to be cleaned, prevents residue Influence to inspection result makes sampling room 1 that can dry sampling after the washing by setting heating tape 3 and temperature sensor 7 Moisture inside room 1, and sampling room 1 is internally heated, make the equalized temperature of the temperature and reaction kettle inside sampling room 1, To prevent the measurement result because of temperature difference to compound.
Working principle: when being sampled, sampling room 1 first is begun to warm up using heating tape 3, is made inside sampling room 1 Temperature it is consistent with the temperature of reaction kettle, start aspiration pump 6, close drainpipe 15 on valve, compound is drawn into sampling Among room 1, then from the outflow of setting-out pipe 2, after sampling, valve on probe tube 13 is closed, opens the valve on drainpipe 15, Cleaning solution is injected from water injection hole 9, starts motor 8, motor 8 drives paddle 12 to rotate by spinner handle 11, thus to sampling room 1 Inside is adequately cleaned, and opens the valve on drainpipe 15, waste liquid is excluded, and is reused heating tape 3 and is carried out to sampling room 1 The cleaning solution of 1 internal residual of sampling room is dried in heating.
The preferable specific embodiment of the above, only the utility model, but the protection scope of the utility model is not It is confined to this, anyone skilled in the art is within the technical scope disclosed by the utility model, practical according to this Novel technical solution and its utility model design are subject to equivalent substitution or change, should all cover the protection model in the utility model Within enclosing.

Claims (5)

1. the automatic sampling device during a kind of chemical industry synthesis, including sampling room (1), which is characterized in that the sampling room (1) Bottom be communicated with setting-out pipe (2), the inside of the sampling room (1) is equipped with heating tape (3), the side of the sampling room (1) It is equipped with support plate (5), is fixedly installed with aspiration pump (6) at the top of the support plate (5), the output end of the aspiration pump (6) It is connected to sampling room (1), the other side of the sampling room (1) is equipped with glass tube (4) and pressure gauge (10), the pressure gauge (10) Positioned at the top of glass tube (4), the bottom of the glass tube (4) is connected to the bottom of sampling room (1), the sampling room (1) Top is provided with temperature sensor (7), motor (8) and water injection hole (9), and the motor (8) is located at temperature sensor (7) and water filling Between hole (9), for the temperature sensor (7) completely through the top of sampling room (1), the inside of the water injection hole (9) is equipped with rubber The output end of rubber plug, the motor (8) is connected with spinner handle (11), top of the spinner handle (11) completely through sampling room (1), institute The surface for stating spinner handle (11) is equipped with paddle (12), and the paddle (12) is located at the inside of sampling room (1), the sampling room (1) side is communicated with probe tube (13), is communicated with return pipe (14) between the probe tube (13) and setting-out pipe (2), described The side of probe tube (13) is equipped with drainpipe (15).
2. the automatic sampling device during a kind of chemical industry synthesis according to claim 1, which is characterized in that the setting-out Pipe (2), probe tube (13), return pipe (14), drainpipe (15) surface be equipped with valve.
3. the automatic sampling device during a kind of chemical industry synthesis according to claim 1, which is characterized in that the stirring The quantity of leaf (12) is three, and three paddles (12) with the centre symmetry line of spinner handle (11), circumferentially arrange by array.
4. the automatic sampling device during a kind of chemical industry synthesis according to claim 1, which is characterized in that the glass Managing (4) is L shape, and the top of glass tube (4) seals, and the surface of glass tube (4) is equipped with graduation mark.
5. the automatic sampling device during a kind of chemical industry synthesis according to claim 1, which is characterized in that the temperature The model WZP-187 of sensor (7).
CN201821151725.0U 2018-07-20 2018-07-20 A kind of automatic sampling device during chemical industry synthesis Expired - Fee Related CN208420463U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821151725.0U CN208420463U (en) 2018-07-20 2018-07-20 A kind of automatic sampling device during chemical industry synthesis

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821151725.0U CN208420463U (en) 2018-07-20 2018-07-20 A kind of automatic sampling device during chemical industry synthesis

Publications (1)

Publication Number Publication Date
CN208420463U true CN208420463U (en) 2019-01-22

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113252381A (en) * 2021-05-27 2021-08-13 大连海事大学 Dissolution sampling device for large-area surface
CN117309494A (en) * 2023-10-16 2023-12-29 山东瑞泰玻璃绝缘子有限公司 Sampling device for testing softening point of glass insulator

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113252381A (en) * 2021-05-27 2021-08-13 大连海事大学 Dissolution sampling device for large-area surface
CN117309494A (en) * 2023-10-16 2023-12-29 山东瑞泰玻璃绝缘子有限公司 Sampling device for testing softening point of glass insulator
CN117309494B (en) * 2023-10-16 2024-03-29 山东瑞泰玻璃绝缘子有限公司 Sampling device for testing softening point of glass insulator

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190122

Termination date: 20190720