CN208373074U - A kind of neutralization reaction kettle - Google Patents

A kind of neutralization reaction kettle Download PDF

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Publication number
CN208373074U
CN208373074U CN201820591871.9U CN201820591871U CN208373074U CN 208373074 U CN208373074 U CN 208373074U CN 201820591871 U CN201820591871 U CN 201820591871U CN 208373074 U CN208373074 U CN 208373074U
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China
Prior art keywords
reaction kettle
kettle body
conical vessel
agitating shaft
inlet tube
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CN201820591871.9U
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Chinese (zh)
Inventor
李小华
李长虹
魏娇
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LIAONING HONGHAO CHEMICAL INDUSTRY Co Ltd
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LIAONING HONGHAO CHEMICAL INDUSTRY Co Ltd
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Priority to CN201820591871.9U priority Critical patent/CN208373074U/en
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Abstract

The utility model relates to a kind of neutralization reaction kettles, including reaction kettle body, it is equipped with to cover accordingly in the reaction kettle body above the reaction kettle body and is provided with rabbling mechanism, the rabbling mechanism is driven by the driving mechanism for being set to capping top, the rabbling mechanism includes the agitating shaft for being connected to the driving mechanism, a conical vessel is connected with below agitating shaft, corresponding accommodating chamber is equipped in the conical vessel, the side wall of conical vessel and bottom are distributed with multiple recirculation holes for being communicated to the accommodating chamber;Device has a bearing on the bottom centre position of the conical vessel, a circulation inlet tube is connected on the bearing, the circulation inlet tube extends to the outside of reaction kettle body, and circulation inlet tube is connected to above the reaction kettle body by corresponding drawing liquid pump and liquid suction pipe;Corresponding stirring blade is connected on the side wall of the conical vessel.The utility model can effectively improve mixing effect, and then improve neutralization reaction efficiency and effect.

Description

A kind of neutralization reaction kettle
Technical field
The utility model relates to a kind of reaction kettle, in particular to a kind of neutralization reaction kettles.
Background technique
It include three chemical units, i.e. rectification cell, post-processing unit and refined unit in boric-10 acid production process.Essence Evaporating unit is that the complex compound rich in boron -10 is obtained through Chemical Exchange rectifying;Post-processing unit is through chemical process by complex compound solution From and be converted into boric acid;Refined unit is to be esterified clarification matter to obtain finished product boric-10 acid.Richness caused by rectification cell The complex compound of boracic -10 needs after entering post-processing unit by hydrolysis and neutralization reaction, hydrolysis and neutralization reaction It is carried out in corresponding reaction kettle respectively.During neutralization reaction, material is carried out sufficiently, during stirring in place directly affects With the efficiency and effect of reaction.Neutralization reaction kettle employed in existing boric acid production process is all conventional neutralization reaction kettle, Its mixing plant generally comprises agitating shaft and stirring blade, and mixing effect is relatively low, causes the efficiency of neutralization reaction lower, is Ensure to react in place, the reaction time have to be extended.Therefore, design is a can effectively improve mixing effect, it is ensured that quickly mixing Material, the neutralization reaction kettle for effectively improving neutralization reaction efficiency and effect is the research purpose of the utility model.
Utility model content
In view of the above-mentioned problems of the prior art, the neutralization is anti-the utility model lies in that providing a kind of neutralization reaction kettle Kettle is answered to can effectively solve the problem that the above-mentioned problems of the prior art.
The technical solution of the utility model is:
A kind of neutralization reaction kettle, including reaction kettle body, the reaction kettle body top is equipped with to be covered accordingly, in the capping Equipped with corresponding feed inlet, the feed inlet is equipped with corresponding material inlet valve, and corresponding discharging is equipped with below the reaction kettle body Mouthful, the discharge port is equipped with corresponding discharge valve, and the outside of the reaction kettle body is equipped with corresponding heating jacket, the heating The two sides of collet are respectively equipped with corresponding hot gas inlet port and hot gas outlet, are provided with rabbling mechanism in the reaction kettle body, The rabbling mechanism is driven by the driving mechanism for being set to capping top, and the rabbling mechanism includes to be connected to the driving The agitating shaft of mechanism is connected with multiple corresponding agitating plates above the agitating shaft, is connected with a taper below agitating shaft Container, the conical vessel is interior to be equipped with corresponding accommodating chamber, and the side wall of conical vessel and bottom are distributed with multiple be communicated to The recirculation hole of the accommodating chamber;Device has a bearing on the bottom centre position of the conical vessel, is connected on the bearing One circulation inlet tube, the circulation inlet tube extend to the outside of reaction kettle body, circulation inlet tube by corresponding drawing liquid pump and Liquid suction pipe is connected to above the reaction kettle body;Corresponding stirring blade is connected on the side wall of the conical vessel.
The driving mechanism includes driving motor and the reduction gearbox for being connected to the driving motor, and the agitating shaft is connected to The output shaft of the reduction gearbox.
The conical vessel is secured to the lower section of the agitating shaft by welding manner.
The advantages of the utility model:
Multiple corresponding agitating plates are connected with above the agitating shaft of the utility model, are connected with a taper below agitating shaft Container is connected with corresponding stirring blade on the side wall of conical vessel.Conventional reactor is played by agitating plate and stirring blade Possessed mixing function.On this basis, it is equipped with corresponding accommodating chamber in the conical vessel of the utility model, conical vessel Side wall and bottom are distributed with multiple recirculation holes for being communicated to the accommodating chamber, device on the bottom centre position of conical vessel There is a bearing, a circulation inlet tube is connected on bearing, circulation inlet tube extends to the outside of reaction kettle body, and circulation inlet tube is logical It crosses corresponding drawing liquid pump and liquid suction pipe is connected to above reaction kettle body.When conical vessel is rotated with agitating shaft, feed liquor is recycled Manage motionless, Matter Transfer is taken out the accommodating chamber in conical vessel by drawing liquid pump movement, the taper being rotated then along recirculation hole Container is thrown away, and effectively in the whipping process of material, is made the circulation of material, is most importantly generated rolling to the material in stirring Effect, greatly improves mixing effect, it is ensured that quick mixed material effectively improves neutralization reaction efficiency and effect.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model.
Specific embodiment
In order to facilitate the understanding of those skilled in the art, existing make structure of the embodiment combination attached drawing to the utility model into one Step detailed description:
With reference to Fig. 1, a kind of neutralization reaction kettle, including reaction kettle body 1 is equipped with corresponding capping above the reaction kettle body 1 2, the capping 2 is equipped with corresponding feed inlet, and the feed inlet is equipped with corresponding material inlet valve 3,1 lower section of reaction kettle body Equipped with corresponding discharge port, the discharge port is equipped with corresponding discharge valve 4, and the outside of the reaction kettle body 1 is equipped with corresponding Heating jacket 5, the two sides of the heating jacket 5 are respectively equipped with corresponding hot gas inlet port 6 and hot gas outlet 7, the reaction Rabbling mechanism 8 is provided in autoclave body 1, the rabbling mechanism 8 is driven by the driving mechanism 9 for being set to 2 top of capping, described Rabbling mechanism 8 includes the agitating shaft 81 for being connected to the driving mechanism 9, and the top of the agitating shaft 81 is connected with multiple corresponding Agitating plate 82, the lower section of agitating shaft 81 are connected with a conical vessel 83, are equipped with corresponding accommodating chamber 10 in the conical vessel 83, The side wall of conical vessel 83 and bottom are distributed with multiple recirculation holes 11 for being communicated to the accommodating chamber 10;The conical vessel Device has a bearing 12 on 83 bottom centre position, is connected with a circulation inlet tube 13 on the bearing 12, it is described recycle into Liquid pipe 13 extends to the outside of reaction kettle body 1, and circulation inlet tube 13 is connected to institute by corresponding drawing liquid pump 14 and liquid suction pipe 15 State 1 top of reaction kettle body;Corresponding stirring blade 84 is connected on the side wall of the conical vessel 83.
The driving mechanism 9 includes driving motor 91 and the reduction gearbox 92 for being connected to the driving motor 91, the stirring Axis 81 is connected to the output shaft of the reduction gearbox 92.The conical vessel 83 is secured to the agitating shaft 81 by welding manner Lower section.
Play mixing function possessed by conventional reactor by agitating plate 82 and stirring blade 84, conical vessel 83 with Agitating shaft 81 rotate when, circulation inlet tube 13 it is motionless, drawing liquid pump 14 movement Matter Transfer is taken out to the appearance in conical vessel 83 It receives chamber 10, is thrown away then along the conical vessel 83 that recirculation hole 11 is rotated, effectively in the whipping process of material, make material Circulation most importantly generates rolling effect to the material in stirring, greatly improves mixing effect, it is ensured that quick mixture Material, effectively improves neutralization reaction efficiency and effect.
The above is only the preferred embodiment of the present invention, it is all done according to present utility model application the scope of the patents it is equal Deng variation and modification, the covering scope of the utility model all should belong to.

Claims (3)

1. a kind of neutralization reaction kettle, including reaction kettle body, the reaction kettle body top is equipped with corresponding capping, sets in the capping There is corresponding feed inlet, the feed inlet is equipped with corresponding material inlet valve, is equipped with corresponding discharge port below the reaction kettle body, The discharge port is equipped with corresponding discharge valve, and the outside of the reaction kettle body is equipped with corresponding heating jacket, the heating folder The two sides of set are respectively equipped with corresponding hot gas inlet port and hot gas outlet, are provided with rabbling mechanism in the reaction kettle body, institute It states rabbling mechanism to be driven by the driving mechanism for being set to capping top, it is characterised in that: the rabbling mechanism includes connection To the agitating shaft of the driving mechanism, multiple corresponding agitating plates are connected with above the agitating shaft, the lower section of agitating shaft is solid It is connected to a conical vessel, is equipped with corresponding accommodating chamber in the conical vessel, the side wall of conical vessel and bottom are distributed with Multiple recirculation holes for being communicated to the accommodating chamber;Device has a bearing, the axis on the bottom centre position of the conical vessel It holds and is connected with a circulation inlet tube, the circulation inlet tube extends to the outside of reaction kettle body, and circulation inlet tube passes through corresponding Drawing liquid pump and liquid suction pipe be connected to above the reaction kettle body;Corresponding paddle is connected on the side wall of the conical vessel Piece.
2. a kind of neutralization reaction kettle according to claim 1, it is characterised in that: the driving mechanism include driving motor and It is connected to the reduction gearbox of the driving motor, the agitating shaft is connected to the output shaft of the reduction gearbox.
3. a kind of neutralization reaction kettle according to claim 1, it is characterised in that: the conical vessel is solid by welding manner It is connected to the lower section of the agitating shaft.
CN201820591871.9U 2018-04-24 2018-04-24 A kind of neutralization reaction kettle Active CN208373074U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820591871.9U CN208373074U (en) 2018-04-24 2018-04-24 A kind of neutralization reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820591871.9U CN208373074U (en) 2018-04-24 2018-04-24 A kind of neutralization reaction kettle

Publications (1)

Publication Number Publication Date
CN208373074U true CN208373074U (en) 2019-01-15

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CN201820591871.9U Active CN208373074U (en) 2018-04-24 2018-04-24 A kind of neutralization reaction kettle

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117920117A (en) * 2024-03-25 2024-04-26 福建常青新能源科技有限公司 Equipment is used in production of ternary precursor

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117920117A (en) * 2024-03-25 2024-04-26 福建常青新能源科技有限公司 Equipment is used in production of ternary precursor

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