CN208340696U - A kind of chlorination tank condensate recycling device - Google Patents

A kind of chlorination tank condensate recycling device Download PDF

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Publication number
CN208340696U
CN208340696U CN201820783104.8U CN201820783104U CN208340696U CN 208340696 U CN208340696 U CN 208340696U CN 201820783104 U CN201820783104 U CN 201820783104U CN 208340696 U CN208340696 U CN 208340696U
Authority
CN
China
Prior art keywords
gas
autoclave body
plenum chamber
kettle cover
filtering device
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201820783104.8U
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Chinese (zh)
Inventor
邓长全
余朝庆
刘群兵
邓友全
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wenchuan Xiangning Chlorate Co Ltd
Original Assignee
Wenchuan Xiangning Chlorate Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wenchuan Xiangning Chlorate Co Ltd filed Critical Wenchuan Xiangning Chlorate Co Ltd
Priority to CN201820783104.8U priority Critical patent/CN208340696U/en
Application granted granted Critical
Publication of CN208340696U publication Critical patent/CN208340696U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The utility model discloses a kind of chlorination tank condensate recycling devices, including autoclave body and kettle cover, feed inlet and exhaust outlet are equipped at the top of kettle cover, autoclave body bottom is equipped with drain pipe, feeding device is provided at feed inlet at the top of the kettle cover, exhaust ports at the top of the kettle cover are connected with gas-filtering device by exhaust pipe, safety valve is provided on exhaust pipe, plenum chamber is installed in the autoclave body, it is connected at the top of plenum chamber with exhaust pipe, condensation pipe is installed in plenum chamber, the gas-filtering device side is provided with water tank, it is connected between gas-filtering device and water tank by circulating line, circulating line one end is fixed at the top of gas-filtering device, the other end protrudes into the water level in water tank or less, the top of water tank is provided with discharge outlet.The utility model makes chlorine gas liquefaction by condensation effect, reenters in autoclave body, to reach the maximization of the utilization of resources, while can also distinguish the type that raw material has been added, and eliminates maloperation risk.

Description

A kind of chlorination tank condensate recycling device
Technical field
The utility model relates to chemical equipment technical fields, and in particular to a kind of chlorination tank condensate recycling device.
Background technique
Chlorination tank can generate a large amount of exhaust gas during the reaction, and the constituent of exhaust gas mainly includes that unreacted is complete Chlorine, HCl gas, paraffin gas molecule etc., these exhaust gas such as can bring certain pollution without processing direct emission to environment.
Existing chlorination tank is all directly to adsorb exhaust gas or spray through soda acid mostly, to achieve the purpose that vent gas treatment, And by the complete chlorine of the unreacted in chlorination reaction and newly-generated chlorine whole filtration, purification, and without recovery processing, It will cause the waste of certain resource.In addition, existing chlorination tank is usually that feed opening is arranged at the top of autoclave body, open at feed opening Spiral cover reaction raw materials are poured directly into autoclave body, since a variety of, this simple feed opening would generally be added in reaction raw materials Structure cannot directly distinguish the type that raw material has been added, and there are maloperation risks.
Summary of the invention
The purpose of this utility model is to provide a kind of chlorination tank condensate recycling device, which makes chlorine by condensation effect Gas liquefaction reenters in autoclave body, to reach the maximization of the utilization of resources, while can also distinguish the type that raw material has been added, disappear Except maloperation risk.
The purpose of this utility model is achieved through the following technical solutions: a kind of chlorination tank condensate recycling device, including Autoclave body and kettle cover, kettle cover top are equipped with feed inlet and exhaust outlet, and autoclave body bottom is equipped with drain pipe, the feed inlet at the top of the kettle cover Place is provided with feeding device, and feeding device includes feed pot, material blanking tube and multiple loading hoppers, material blanking tube be connected to feed pot and It is provided with the second control valve between the feed inlet of kettle cover, and on material blanking tube, is fixed with adjusting rod, Duo Gejia at the top of the feed pot Hopper is installed at the top of feed pot and circumferentially distributed around adjusting rod, and equal with loading hopper quantity insert is provided on the adjusting rod Slot, the interior sliding of slot are provided with cutting, and the loading hopper is hinged with hopper cover close to the side of adjusting rod, sets on the inside of hopper cover It is equipped with strut, the lower section in slot and being located at cutting, the part and the bottom of slot of the strut insertion slot are inserted into strut one end Adjustment spring is provided between face, the exhaust ports at the top of the kettle cover are connected with gas-filtering device by exhaust pipe, row It is provided with safety valve in feed channel, plenum chamber is installed in the autoclave body, is connected at the top of plenum chamber with exhaust pipe, in plenum chamber Condensation pipe is installed, refrigerant has been passed through in condensation pipe, the gas-filtering device side is provided with water tank, gas filtration dress It sets and is connect between water tank by circulating line, circulating line one end is fixed at the top of gas-filtering device, and the other end protrudes into water Water level in case is hereinafter, the top of water tank is provided with discharge outlet.
Further, the gas-filtering device includes shell and is successively set on the intracorporal active carbon of shell from top to bottom Layer, cao layers and microbe stuffing layer.
Further, vertical material baffle is provided in the feed pot, the inner cavity of feed pot is divided into more by material baffle A space corresponding with loading hopper, bottom is equipped with deflector in the feed pot, is provided in the middle part of deflector and material blanking tube The material-dropping hole of connection.
Further, the plenum chamber is mounted on the top of autoclave body inner cavity, and close to the side of exhaust pipe.
Further, the condensation pipe, which spirals, is arranged in plenum chamber, and the both ends of condensation pipe both pass through plenum chamber Side wall and autoclave body side wall.
Further, the first control valve is provided on the drain pipe.
The utility model has the beneficial effect that
1, by the way that condensation pipe is arranged in plenum chamber, the chlorine of rising liquefies afterwards to the cold, is fallen into autoclave body again into one Step reaction, to reach the maximization of the utilization of resources;
2, by setting feeding device, feeding device includes multiple loading hoppers, and it is former to can be used for being added different types of reaction Material, to avoid adding more or adding the maloperation risk of reaction raw materials less;
3, the acidity and paraffin gas molecule that chlorination reaction generates can be filtered out only in time by setting gas-filtering device Change, the safety of lifting device.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is the schematic diagram of internal structure of the utility model;
Fig. 3 is the structural schematic diagram of feeding device in the utility model;
Marked in the figure: 1- autoclave body;2- kettle cover;3- feeding device;4- drain pipe;The first control valve of 5-;6- plenum chamber;7- is cold Solidifying pipeline;8- material baffle;9- deflector;10- exhaust pipe;11- safety valve;12- gas-filtering device;13- circulating line; 14- water tank;15- discharge outlet;16- microbe stuffing layer;17- cao layers;18- active carbon layer;The second control valve of 19-;31- adds Batch can;32- loading hopper;33- hopper cover;34- strut;35- adjusting rod;36- cutting;37- sliding slot;38- adjustment spring;39- is fallen Expects pipe.
Specific embodiment
As shown in FIG. 1 to 3, chlorination tank condensate recycling device provided in this embodiment includes autoclave body 1 and is arranged in kettle The kettle cover 2 at the top of body 1, is provided with feed inlet and exhaust outlet at the top of kettle cover 2, and 1 bottom of autoclave body is provided with drain pipe 4, on drain pipe 4 It is provided with the first control valve 5.It is provided with feeding device 3 at the feed inlet at 2 top of kettle cover, feeding device 3 includes feed pot 31, material blanking tube 39 and multiple loading hoppers 32, material blanking tube 39 is connected between feed pot 31 and the feed inlet of kettle cover 2, and blanking The second control valve 19 is provided on pipe 39, the top of feed pot 31 is fixed with adjusting rod 35, and multiple loading hoppers 32, which are installed in, to be added 31 top of batch can is simultaneously circumferentially uniformly distributed around adjusting rod 35, and each correspondence of loading hopper 32 adds a kind of reaction raw materials, can avoid Now more additions or the maloperation risk for adding one or more reaction raw materials less;It is provided on the adjusting rod 35 and the number of loading hopper 32 Equal slot is measured, sliding is provided with cutting 36 in slot, and specifically, 36 two sides of cutting are provided with sliding slot 37, the inner wall of slot On be provided with and be slidably matched protrusion with sliding slot 37.The loading hopper 32 is hinged with hopper cover 33 close to the side of adjusting rod 35, material Integrally formed with strut 34, the lower section in slot and being located at cutting 36, the strut are inserted into 34 one end of strut for the inside of bucket cover 33 It is provided with adjustment spring 38 between the part of 34 insertion slots and the bottom surface table wall of slot, it is vertical to be provided in the feed pot 31 Material baffle 8,31 inner cavity of feed pot is divided into multiple separated material corresponding with loading hopper 32 spaces, the feed pot by material baffle 8 Bottom is also equipped with deflector 9 in 31, and in a ring, and the inner wall of the outer wall of deflector 9 and feed pot 31 is fixed connects for deflector 9 It connects, the middle part of deflector 9 is provided with the material-dropping hole being connected to material blanking tube 39.Cutting 36 is pressed down on, will be expected using lever principle Bucket cover 33 is tilted and is opened, and reaction raw materials are then added into corresponding loading hopper 32, and reaction raw materials enter corresponding from loading hopper 32 Separated material space, most afterwards through material blanking tube 39 enter autoclave body 1 in, unclamp cutting 36, under the action of 38 elastic force of adjustment spring, hopper Lid 33 continues to cover 32 top of loading hopper.
The exhaust ports at 2 top of kettle cover are connected with gas-filtering device 12, exhaust pipe 10 by exhaust pipe 10 On be provided with safety valve 11, plenum chamber 6 is installed, plenum chamber 6 is located at 1 inner cavity top of autoclave body, and close to exhaust in the autoclave body 1 The side of pipeline 10,6 inside turn of plenum chamber are provided with condensation pipe 7, by there is a refrigerant in condensation pipe 7, and condensation pipe 7 Both ends both pass through 1 side wall of 6 side wall of plenum chamber and autoclave body, and the chlorine and the complete chlorine of unreacted that chlorination reaction generates float up to At condensation pipe 7, chlorine liquefies to the cold, then falls after rise to 1 bottom of autoclave body and further reacts again, is greatly improved returning for chlorine Utilization rate is received, the top that remaining impurity gas then passes through plenum chamber 6 enters exhaust pipe 10 and carries out next step purification.
The gas-filtering device 12 is including shell and is successively set on the intracorporal active carbon layer 18 of shell, oxygen from top to bottom Change calcium layer 17 and microbe stuffing layer 16, sour gas, paraffin gas molecule and the impurity of floating in autoclave body 1 can be carried out It filters out, to improve the clean-up performance of gas;The side of filter device 12 is provided with water tank 14, gas-filtering device 12 and water tank It is connected between 14 by circulating line 13,13 one end of circulating line is fixed on the top of gas-filtering device 12, and the other end protrudes into Hereinafter, the top of water tank 14 is provided with discharge outlet 15, the gas after Water warfare can further improve water level in water tank 14 Its clean-up performance.
The above is only the utility model preferred embodiment, but the protection scope of the utility model is not limited to This, any transformation carried out based on technical solution provided by the utility model and inventive concept and replacement should all be covered in this reality With in novel protection scope.

Claims (6)

1. a kind of chlorination tank condensate recycling device, including autoclave body and kettle cover, kettle cover top is equipped with feed inlet and exhaust outlet, autoclave body bottom Portion is equipped with drain pipe, it is characterised in that: feeding device is provided at the feed inlet at the top of the kettle cover, feeding device includes charging Tank, material blanking tube and multiple loading hoppers, material blanking tube are connected between feed pot and the feed inlet of kettle cover, and are provided on material blanking tube Second control valve, the feed pot top are fixed with adjusting rod, and multiple loading hoppers are installed at the top of feed pot and around adjusting rod It is circumferentially distributed, the slot equal with loading hopper quantity is provided on the adjusting rod, sliding is provided with cutting, the charging in slot It struggles against and is hinged with hopper cover close to the side of adjusting rod, strut is provided on the inside of hopper cover, strut one end is inserted into slot and position Adjustment spring, the kettle cover top are provided between the lower section of cutting, the part of the strut insertion slot and the bottom surface of slot The exhaust ports in portion are connected with gas-filtering device by exhaust pipe, are provided with safety valve on exhaust pipe, in the autoclave body Plenum chamber is installed, is connected at the top of plenum chamber with exhaust pipe, condensation pipe is installed in plenum chamber, has been passed through in condensation pipe Refrigerant, the gas-filtering device side are provided with water tank, are connected, are followed by circulating line between gas-filtering device and water tank Endless tube road one end is fixed at the top of gas-filtering device, and the water level that the other end protrudes into water tank is hereinafter, the top of water tank is set It is equipped with discharge outlet.
2. chlorination tank condensate recycling device according to claim 1, it is characterised in that: the gas-filtering device includes shell Body and it is successively set on the intracorporal active carbon layer of shell, cao layers and microbe stuffing layer from top to bottom.
3. chlorination tank condensate recycling device according to claim 1, it is characterised in that: it is vertical to be provided in the feed pot Material baffle, the inner cavity of feed pot is divided into multiple spaces corresponding with loading hopper by material baffle, and bottom is pacified in the feed pot Equipped with deflector, the material-dropping hole being connected to material blanking tube is provided in the middle part of deflector.
4. chlorination tank condensate recycling device according to claim 1, it is characterised in that: the plenum chamber is mounted in autoclave body The top of chamber, and close to the side of exhaust pipe.
5. chlorination tank condensate recycling device according to claim 4, it is characterised in that: the condensation pipe, which spirals to be arranged, to exist In plenum chamber, and the both ends of condensation pipe both pass through plenum chamber side wall and autoclave body side wall.
6. chlorination tank condensate recycling device according to claim 1, it is characterised in that: be provided with first on the drain pipe Control valve.
CN201820783104.8U 2018-05-24 2018-05-24 A kind of chlorination tank condensate recycling device Expired - Fee Related CN208340696U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820783104.8U CN208340696U (en) 2018-05-24 2018-05-24 A kind of chlorination tank condensate recycling device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820783104.8U CN208340696U (en) 2018-05-24 2018-05-24 A kind of chlorination tank condensate recycling device

Publications (1)

Publication Number Publication Date
CN208340696U true CN208340696U (en) 2019-01-08

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820783104.8U Expired - Fee Related CN208340696U (en) 2018-05-24 2018-05-24 A kind of chlorination tank condensate recycling device

Country Status (1)

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CN (1) CN208340696U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114853682A (en) * 2022-06-10 2022-08-05 江苏中渊化学品有限公司 Production equipment and method of bulk drug intermediate 4, 6-dichloro-5-fluoropyrimidine

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114853682A (en) * 2022-06-10 2022-08-05 江苏中渊化学品有限公司 Production equipment and method of bulk drug intermediate 4, 6-dichloro-5-fluoropyrimidine

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190108

Termination date: 20200524

CF01 Termination of patent right due to non-payment of annual fee