CN208320778U - A kind of small-sized reaction kettle of applied chemistry - Google Patents

A kind of small-sized reaction kettle of applied chemistry Download PDF

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Publication number
CN208320778U
CN208320778U CN201820322701.0U CN201820322701U CN208320778U CN 208320778 U CN208320778 U CN 208320778U CN 201820322701 U CN201820322701 U CN 201820322701U CN 208320778 U CN208320778 U CN 208320778U
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CN
China
Prior art keywords
autoclave body
defoaming
plate
reaction kettle
small
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201820322701.0U
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Chinese (zh)
Inventor
王敏
于姝燕
徐璐
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Inner Mongolia Medical University
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Inner Mongolia Medical University
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Filing date
Publication date
Application filed by Inner Mongolia Medical University filed Critical Inner Mongolia Medical University
Priority to CN201820322701.0U priority Critical patent/CN208320778U/en
Application granted granted Critical
Publication of CN208320778U publication Critical patent/CN208320778U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of applied chemistry small-sized reaction kettle, including autoclave body, charge pipe is installed at the top of the autoclave body, the top opening position of charge pipe is equipped with sealing flip lid by articulate;The utility model is during actually stirring, stirring rod drives solution to stir homogeneous, solution by the blocking of defoaming plate and generates impact effects during flowing at this time, solution is realized during collision to scatter, bubbles burst in the solution at this time, partial air can be discharged from exhaust tube in this way, the tapered structure in hole is defoamed simultaneously, it is easy that flow velocity can be improved due to narrowing during flowing through defoaming hole path in this way, therefore bubble surface tension is made to change under the variation of flow velocity, bubble can be allowed to rupture in advance in this way, and hangnail also may be implemented to puncture bubble, to have the function that sufficiently to defoam, total consumes energy without additional defoaming, and the baffling effect for defoaming plate also functions to certain auxiliary stirring action.

Description

A kind of small-sized reaction kettle of applied chemistry
Technical field
The utility model relates to chemical fields, more particularly, to a kind of small-sized reaction kettle of applied chemistry.
Background technique
The broad understanding of reaction kettle has the container physically or chemically reacted, is designed by the structure to container and is matched with parameter It sets, realizes the mixed function for heating, evaporation, cooling and the low high speed that technique requires.
Reaction kettle is widely used in petroleum, chemical industry, rubber, pesticide, dyestuff, medicine, food, for complete vulcanization, nitrification, Pressure vessel of the technical process such as hydrogenation, hydrocarbonylation, polymerization, condensation, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.;Material Matter generally has carbon manganese steel, stainless steel, zirconium, Ni-based (Kazakhstan, Monel, inconel) alloy and other composite materials.
Easily there is the case where blister in actual use in existing reaction kettle, and air pressure inside is integrally easily caused to increase and stir The bad situation of effect, it is therefore desirable to accomplish to defoam in time.
Utility model content
The utility model is to overcome above situation insufficient, it is desirable to provide a kind of technical solution that can solve the above problem.
A kind of applied chemistry small-sized reaction kettle, including autoclave body are equipped with charge pipe, charge pipe at the top of the autoclave body Top opening position by articulate be equipped with sealing flip lid;The outer top position of autoclave body fixed peace by way of welding Equipped with horizontally disposed mounting plate, stirring motor is wherein equipped with by screw on mounting plate, the motor shaft of stirring motor passes through Through-hole at the top of mounting plate and autoclave body simultaneously extends on the inside of autoclave body, and the bottom position of motor shaft be connected with by shaft coupling it is perpendicular Straight setting agitating shaft, agitating shaft is set to the inside of autoclave body, and the bottom of agitating shaft is welded with stirring rod, is driven by stirring motor Agitating shaft rotation, to realize stirring of the stirring rod to material;Electrothermal tube, and electric heating are equipped with by screw on the inner wall of autoclave body The power supply line of pipe is pierced by from the string holes on autoclave body outer wall, and sealing is injected in string holes;The bottom discharge port of the autoclave body is welded There is discharge nozzle, and outlet valve is installed on discharge nozzle;Bleeding point, the external port of bleeding point are offered above the side wall of the autoclave body To exhaust tube is connected to, by docking aspiration pump with exhaust tube, the gas generated inside autoclave body can quickly be taken away, avoid kettle There is the case where high pressure in internal portion, so that environment under low pressure facilitates surface of material blister cracks;It is embedded on the inner wall of the autoclave body It is fixed with the plate-like defoaming plate of muti-piece, defoaming plate is arranged along the circumferentially equidistant interval of inner wall of autoclave body, and it is inclined to defoam plate Setting, defoaming plate are located at stirring rod motion profile outer fix;It is through before and after uniformly being offered on the defoaming plate to disappear Abscess, defoaming hole is in the small shape structure of import large outlet, and is uniformly machined with hangnail on the inner wall in defoaming hole, what is actually stirred In the process, stirring rod drives solution to stir homogeneous, and blocking and generation of the solution during flowing by defoaming plate at this time is hit Effect is hit, solution is realized during collision to scatter, and bubbles burst in the solution, such partial air can be from pumpings at this time It is discharged at tracheae, while defoaming the tapered structure in hole, be easy the original to narrow during flowing through defoaming hole due to path in this way Because flow velocity can be improved, therefore under the variation of flow velocity bubble surface tension is changed, bubble can be allowed to shift to an earlier date in this way Rupture, and hangnail also may be implemented to puncture bubble, and to have the function that sufficiently to defoam, total disappears without additional Bubble energy consumption, and the baffling effect for defoaming plate also functions to certain auxiliary stirring action.
As a further solution of the present invention: the outer bottom of the autoclave body is equipped with supporting leg.
As a further solution of the present invention: using integral structure between the hangnail and defoaming plate.
As a further solution of the present invention: the defoaming plate is made of ceramic material.
As a further solution of the present invention: the end port thread seal of the exhaust tube has sealing cover.
The utility model has the beneficial effects that the utility model, during actually stirring, stirring rod drives solution stirring Homogeneous, solution by the blocking of defoaming plate and generates impact effects during flowing at this time, and solution is during collision Realization is scattered, at this time bubbles burst in the solution, and such partial air can be discharged from exhaust tube, while defoaming hole in cone Shape structure is easy that flow velocity can be improved due to narrowing during flowing through defoaming hole path in this way, in flow velocity Variation under so that bubble surface tension changes, bubble can be allowed to rupture in advance in this way, and hangnail also may be implemented pair Bubble punctures, to have the function that sufficiently to defoam, total consumes energy without additional defoaming, and defoams the baffling effect of plate Fruit also functions to certain auxiliary stirring action.
The additional aspect and advantage of the utility model will be set forth in part in the description, partially will be from following description In become obvious, or recognized by the practice of the utility model.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only It is some embodiments of the utility model, for those of ordinary skill in the art, before not making the creative labor property It puts, is also possible to obtain other drawings based on these drawings.
Fig. 1 is the utility model structure diagram;
Fig. 2 is the partial structural diagram one of the utility model.
Fig. 3 is the partial structural diagram two of the utility model.
In figure: 1- autoclave body, 2- supporting leg, 3- charge pipe, 4- discharge nozzle, 5- outlet valve, 6- sealing flip lid, 7- mounting plate, 8- stirring motor, 9- shaft coupling, 10- agitating shaft, 11- stirring rod, 12- defoaming plate, 13- defoaming hole, 14- exhaust tube, 15- sealing Lid, 16- electrothermal tube, 17- hangnail.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
Please refer to Fig. 1~3, in the utility model embodiment, a kind of small-sized reaction kettle of applied chemistry, including autoclave body 1, institute The top for stating autoclave body 1 is equipped with charge pipe 3, and the top opening position of charge pipe 3 is equipped with sealing flip lid by articulate 6;The outer top position of autoclave body 1 is fixedly installed with horizontally disposed mounting plate 7 by way of welding, wherein leads on mounting plate 7 It crosses screw and stirring motor 8 is installed, the motor shaft of stirring motor 8 passes through the through-hole at 1 top of mounting plate 7 and autoclave body and extends to 1 inside of autoclave body, and the bottom position of motor shaft is connected with by shaft coupling 9 and is vertically arranged agitating shaft 10, agitating shaft 10 is set to kettle The inside of body 1, and the bottom of agitating shaft 10 is welded with stirring rod 11, drives agitating shaft 10 to rotate by stirring motor 8, thus real Existing stirring of the stirring rod 11 to material;Electrothermal tube 16, and the power supply line of electrothermal tube 16 are equipped with by screw on the inner wall of autoclave body 1 It is pierced by from the string holes on 1 outer wall of autoclave body, and is injected with sealing in string holes;The bottom discharge port of the autoclave body 1 is welded with discharge nozzle 4, and outlet valve 5 is installed on discharge nozzle 4;Bleeding point, the external port docking of bleeding point are offered above the side wall of the autoclave body 1 There is exhaust tube 14, by docking aspiration pump with exhaust tube 14, the gas generated inside autoclave body 1 can quickly be taken away, avoid There is the case where high pressure inside autoclave body 1, so that environment under low pressure facilitates surface of material blister cracks;On the inner wall of the autoclave body 1 Insertion is fixed with the plate-like defoaming plate 12 of muti-piece, and defoaming plate 12 is arranged along the circumferentially equidistant interval of inner wall of autoclave body 1, and defoams Plate 12 is inclined to set, and defoaming plate 12 is located at 11 motion profile outer fix of stirring rod;It is uniformly opened up on the defoaming plate 12 The defoaming hole 13 for having front and back through, defoaming hole 13 are in the small shape structure of import large outlet, and uniform on the inner wall in defoaming hole 13 It is machined with hangnail 17, during actually stirring, stirring rod 11 drives solution to stir homogeneous, at this time process of the solution in flowing In by defoaming plate 12 blocking and generate impact effects, solution is realized during collision scatters, at this time in the solution Bubbles burst, such partial air can be discharged from exhaust tube 14, while defoam the tapered structure in hole 13, be easy flowing in this way Flow velocity can be improved due to narrowing during through defoaming hole 13 path, bubble table is made under the variation of flow velocity Face tension changes, and bubble can be allowed to rupture in advance in this way, and hangnail 17 also may be implemented to puncture bubble, to reach To the effect sufficiently defoamed, the baffling effect that total consumes energy without additional defoaming, and defoams plate 12 also functions to certain Assist stirring action.
The outer bottom of the autoclave body 1 is equipped with supporting leg 2.
Integral structure is used between the hangnail 17 and defoaming plate 12.
The defoaming plate 12 is made of ceramic material.
The end port thread seal of the exhaust tube 14 has sealing cover 15.
The working principle of the utility model is: stirring rod 11 drives solution to stir homogeneous during actually stirring, this When solution by the blocking of defoaming plate 12 and generate impact effects during flowing, solution is realized scattered during collision It opens, at this time bubbles burst in the solution, such partial air can be discharged from exhaust tube 14, while it is tapered to defoam hole 13 Structure is easy that flow velocity can be improved due to narrowing during flowing through defoaming hole 13 path in this way, in flow velocity Variation under so that bubble surface tension changes, bubble can be allowed to rupture in advance in this way, and hangnail 17 also may be implemented Bubble is punctured, to have the function that sufficiently to defoam, total consumes energy without additional defoaming, and defoams the folding of plate 12 Stream effect also functions to certain auxiliary stirring action.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting Related claim.

Claims (5)

1. a kind of applied chemistry small-sized reaction kettle, including autoclave body, charge pipe is installed at the top of the autoclave body, charge pipe Top opening position is equipped with sealing flip lid by articulate;The outer top position of autoclave body is fixedly mounted by way of welding There is horizontally disposed mounting plate, stirring motor is wherein equipped with by screw on mounting plate, the motor shaft of stirring motor passes through peace Through-hole at the top of loading board and autoclave body simultaneously extends on the inside of autoclave body, and the bottom position of motor shaft is connected with vertically by shaft coupling Agitating shaft is set, and agitating shaft is set to the inside of autoclave body, and the bottom of agitating shaft is welded with stirring rod, is stirred by stirring motor drive Axis rotation is mixed, electrothermal tube is equipped with by screw on the inner wall of autoclave body, and the power supply line of electrothermal tube is from the string holes on autoclave body outer wall It is pierced by, and is injected with sealing in string holes;The bottom discharge port of the autoclave body is welded with discharge nozzle, and discharging is equipped on discharge nozzle Valve;Offer bleeding point above the side wall of the autoclave body, the external port of bleeding point is to being connected to exhaust tube, which is characterized in that described Insertion is fixed with the plate-like defoaming plate of muti-piece on the inner wall of autoclave body, and defoaming plate is set along the circumferentially equidistant interval of inner wall of autoclave body It sets, and defoams plate and be inclined to set, defoaming plate is located at stirring rod motion profile outer fix;It is uniformly opened up on the defoaming plate The defoaming hole for having front and back through, defoaming hole are in the small shape structure of import large outlet, and are uniformly machined on the inner wall in defoaming hole Hangnail.
2. the small-sized reaction kettle of applied chemistry according to claim 1, which is characterized in that the outer bottom of the autoclave body is installed There is supporting leg.
3. the small-sized reaction kettle of applied chemistry according to claim 1, which is characterized in that between the hangnail and defoaming plate Using integral structure.
4. the small-sized reaction kettle of applied chemistry according to claim 1, which is characterized in that the defoaming plate is using ceramic material Matter is made.
5. the small-sized reaction kettle of applied chemistry according to claim 1, which is characterized in that the end port spiral shell of the exhaust tube Line is sealed with sealing cover.
CN201820322701.0U 2018-02-28 2018-02-28 A kind of small-sized reaction kettle of applied chemistry Expired - Fee Related CN208320778U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820322701.0U CN208320778U (en) 2018-02-28 2018-02-28 A kind of small-sized reaction kettle of applied chemistry

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820322701.0U CN208320778U (en) 2018-02-28 2018-02-28 A kind of small-sized reaction kettle of applied chemistry

Publications (1)

Publication Number Publication Date
CN208320778U true CN208320778U (en) 2019-01-04

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Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112834444A (en) * 2019-11-22 2021-05-25 财团法人工业技术研究院 Residual poison detection device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112834444A (en) * 2019-11-22 2021-05-25 财团法人工业技术研究院 Residual poison detection device

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190104

Termination date: 20200228