CN208302731U - A kind of chemistry solid-liquid reaction device - Google Patents

A kind of chemistry solid-liquid reaction device Download PDF

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Publication number
CN208302731U
CN208302731U CN201820730038.8U CN201820730038U CN208302731U CN 208302731 U CN208302731 U CN 208302731U CN 201820730038 U CN201820730038 U CN 201820730038U CN 208302731 U CN208302731 U CN 208302731U
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CN
China
Prior art keywords
liquid
reaction
tube
outlet
solid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201820730038.8U
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Chinese (zh)
Inventor
陶锦
文明杰
杨婷
张田雷
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shaanxi University of Technology
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Shaanxi University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shaanxi University of Technology filed Critical Shaanxi University of Technology
Priority to CN201820730038.8U priority Critical patent/CN208302731U/en
Application granted granted Critical
Publication of CN208302731U publication Critical patent/CN208302731U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The utility model discloses a kind of chemical solid-liquid reaction devices, which includes liquid inlet device and reactor;Liquid inlet device includes liquid holding bottle, the inlet at the top of liquid holding bottle and the first outlet tube set on liquid holding bottle bottom;First outlet tube is equipped with the first glass cock, and the first outlet tube also sets the glass stopper adaptation docking of pipe at its liquid outlet, and reaction tube bottom end is equipped with the second outlet tube, has glass stopper on the second outlet tube;Reactor includes reaction tube, and reaction tube top inlet and first go out liquid liquid pipe and be equipped with the second glass cock;Tube body of the reaction tube at top orientation is equipped with escape pipe, and reaction tube is equipped with the porous barrier for placing solid medicine in the tube body at the direction of bottom end.The utility model is suitable for chemical solid-liquid reaction gas collection, more efficient, and reaction in time, effectively controls reaction rate, saves reaction drug, and experimental result is even more ideal.

Description

A kind of chemistry solid-liquid reaction device
Technical field
The utility model belongs to chemical plant more particularly to a kind of chemical solid-liquid reaction device.
Background technique
Existing solid-liquid reaction device is bulky, complicated for operation.For the solid-liquid reaction of rapid reaction, existing solid-liquid Reactor efficiency is low, is unable to control reaction rate, and waste reaction reagent significantly, experimental result is unsatisfactory.
Utility model content
The purpose of this utility model is to provide a kind of chemical solid-liquid reaction devices, it is intended to solve existing in above-mentioned background technique There is the deficiency of technology.
The utility model is realized in this way a kind of chemistry solid-liquid reaction device, the reaction unit include liquid inlet device and Reactor;The liquid inlet device includes liquid holding bottle, the inlet at the top of liquid holding bottle and goes out set on the first of liquid holding bottle bottom Liquid pipe;First outlet tube is equipped with the first glass cock, and first outlet tube is additionally provided with glass at its liquid outlet Plug;
The reactor includes reaction tube, and reaction tube top inlet is adapted to pair with the glass stopper of the first outlet tube It connects, the reaction tube bottom end is equipped with the second outlet tube, and second outlet tube is equipped with the second glass cock;The reaction tube leans on Tube body at top orientation is equipped with escape pipe, and the reaction tube is equipped in the tube body at the direction of bottom end for placing solid The porous barrier of drug.
Preferably, the reaction tube is equipped with the scale for showing solid most preferably placement amount.
Preferably, the liquid inlet device further includes the glass stopper that docking is adapted to its inlet.
Compared with the prior art the shortcomings that and deficiency, the utility model has the following beneficial effects: the utility model is suitable for Chemical solid-liquid reaction prepares gas, more efficient, saves drug, and effectively control reaction rate, experimental result are even more ideal.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model chemistry solid-liquid reaction device;
Fig. 2 is structural schematic diagram of the utility model chemistry solid-liquid reaction device under disassembled form.
Specific embodiment
In order to make the purpose of the utility model, technical solutions and advantages more clearly understood, below in conjunction with attached drawing and implementation Example, the present invention will be further described in detail.It should be appreciated that specific embodiment described herein is only used to explain The utility model is not used to limit the utility model.
As shown in Figure 1 and 2, wherein Fig. 1 is the structural schematic diagram of the utility model chemistry solid-liquid reaction device;Fig. 2 is this Structural schematic diagram of the utility model chemistry solid-liquid reaction device under disassembled form.
The utility model discloses a kind of chemical solid-liquid reaction devices, which includes liquid inlet device and reactor; The liquid inlet device includes liquid holding bottle 1, the inlet at the top of liquid holding bottle and the first outlet tube 2 set on 1 bottom of liquid holding bottle; First outlet tube 2 is equipped with the first glass cock 3, and first outlet tube 2 is additionally provided with glass stopper at its liquid outlet 4;
The reactor includes reaction tube 5, and reaction tube top inlet is adapted to pair with the glass stopper of the first outlet tube 2 It connects, 5 bottom end of reaction tube is equipped with the second outlet tube 6, and second outlet tube 6 is equipped with the second glass cock 7;The reaction Tube body of the pipe 5 at top orientation is equipped with escape pipe 8, and the reaction tube 5 is equipped in the tube body at the direction of bottom end and is used for Place the porous barrier 9 of solid medicine.
In the utility model embodiment, to pass through convenient for being made full use of to solid medicine in reaction tube 5 and liquid drug Test of many times has found best graduation mark 10.
In the utility model embodiment, more specifically, the liquid inlet device further includes the glass that docking is adapted to its inlet Glass plug 11.
In the actual application of the utility model, fixed drug is added in reaction tube 5, liquid drug is added to In liquid holding bottle 1;Liquid inlet device and reactor are assembled as shown in Figure 1, liquid is added by opening glass stopper 4 in liquid holding bottle 1 Solution adjusts the first glass cock 3 control dropping liquid and is added dropwise to the speed in reaction tube 5.It is reacted during dropping liquid is added dropwise The waste liquid of generation is contained at the waste liquid storage below porous barrier, will be useless in reactor by adjusting the second glass cock 7 Drop is added in the preset beaker in underface;The gas that reaction generates then is discharged from escape pipe 8.
The utility model is suitable for complicated solid-liquid reaction and sets gas, more efficient, reacts easy to control, saves drug, experiment knot Fruit is even more ideal.
The above is only the preferred embodiment of the utility model only, is not intended to limit the utility model, all at this Made any modifications, equivalent replacements, and improvements etc., should be included in the utility model within the spirit and principle of utility model Protection scope within.

Claims (3)

1. a kind of chemistry solid-liquid reaction device, which is characterized in that the reaction unit includes liquid inlet device and reactor;The feed liquor Device includes liquid holding bottle, the inlet at the top of liquid holding bottle and the first outlet tube set on liquid holding bottle bottom;Described first goes out Liquid pipe is equipped with the first glass cock, and first outlet tube is additionally provided with glass stopper at its liquid outlet;
The reactor includes reaction tube, and reaction tube top inlet is adapted to docking, institute with the glass stopper of the first outlet tube Reaction tube bottom end is stated equipped with the second outlet tube, second outlet tube is equipped with the second glass cock;The reaction tube leans on top Tube body at direction is equipped with escape pipe, and the reaction tube is equipped in the tube body at the direction of bottom end for placing solid medicine Porous barrier.
2. chemistry solid-liquid reaction device as described in claim 1, which is characterized in that the reaction tube is equipped with solid for showing The scale of body most preferably placement amount.
3. chemistry solid-liquid reaction device as claimed in claim 2, which is characterized in that the liquid inlet device further includes and its inlet It is adapted to the glass stopper of docking.
CN201820730038.8U 2018-05-16 2018-05-16 A kind of chemistry solid-liquid reaction device Expired - Fee Related CN208302731U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820730038.8U CN208302731U (en) 2018-05-16 2018-05-16 A kind of chemistry solid-liquid reaction device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820730038.8U CN208302731U (en) 2018-05-16 2018-05-16 A kind of chemistry solid-liquid reaction device

Publications (1)

Publication Number Publication Date
CN208302731U true CN208302731U (en) 2019-01-01

Family

ID=64712676

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820730038.8U Expired - Fee Related CN208302731U (en) 2018-05-16 2018-05-16 A kind of chemistry solid-liquid reaction device

Country Status (1)

Country Link
CN (1) CN208302731U (en)

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GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190101

Termination date: 20190516