CN208279328U - A kind of equipment that non-oxide ceramics superfine powder is prepared based on solvent thermal polymerization reaction - Google Patents
A kind of equipment that non-oxide ceramics superfine powder is prepared based on solvent thermal polymerization reaction Download PDFInfo
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- CN208279328U CN208279328U CN201820522305.2U CN201820522305U CN208279328U CN 208279328 U CN208279328 U CN 208279328U CN 201820522305 U CN201820522305 U CN 201820522305U CN 208279328 U CN208279328 U CN 208279328U
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- China
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- oxide ceramics
- superfine powder
- storehouse
- polymerization reaction
- box
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Abstract
The utility model discloses a kind of equipment for preparing non-oxide ceramics superfine powder based on solvent thermal polymerization reaction, including apparatus main body, inert gas pump is provided at the top of apparatus main body, the outer surface side of inert gas pump passes through appendix through the outer surface for the treatment of box and extends to the inside for the treatment of box, the side for the treatment of box is provided with discharge nozzle, the equipment that this kind prepares non-oxide ceramics superfine powder based on heat polymerization, increase is provided with temperature inductor and temperature indicator, temperature inductor can detect the temperature inside treatment box, and it is shown by temperature indicator, convenient for user's observation, this kind of device is provided with temperature adjustment knob simultaneously, it can make user that the heter temperature inside treatment box be adjusted by temperature adjustment knob, to keep the operation of this kind of device more convenient, increase this kind of device Working efficiency, while this kind of device is provided with universal wheel, and during using this kind of device, universal wheel can be mobile convenient for device.
Description
Technical field
The utility model relates to the equipment technical fields of ceramic ultrafine powder body, specially a kind of to be reacted based on solvent thermal polymerization
The equipment for preparing non-oxide ceramics superfine powder.
Background technique
A kind of equipment preparing non-oxide ceramics superfine powder based on solvent thermal polymerization reaction is by utilizing solvent heat
Reaction, by the organic precursor method monomer of the ceramics such as Polycarbosilane, polyborazine and zirconium carbide, hafnium carbide and tungsten carbide or mixed
The benzole soln for closing object is converted to organosilane precursor powder, then through being pyrolyzed the equipment for obtaining non-oxide ceramics superfine powder.
But the existing equipment for preparing non-oxide ceramics superfine powder based on heat polymerization, most volume is larger, no
It is easily mobile, and the temperature inside treatment box can not be detected in the course of work of production superfine powder, while cannot be right
Heter temperature inside treatment box is adjusted, and makes that this kind of equipment operation is complex and working efficiency is low.
Utility model content
The purpose of this utility model is to provide one kind to prepare non-oxide ceramics superfine powder based on solvent thermal polymerization reaction
The equipment of body, it is not easily shifted to solve to propose that volume is larger in above-mentioned background technique, the temperature inside treatment box can not be carried out
Detection, while the heter temperature inside treatment box cannot be adjusted, make this kind of equipment operation complexity and working efficiency is low
Under problem.
To achieve the above object, the utility model provides the following technical solutions: one kind is based on solvent thermal polymerization reaction preparation
The equipment of non-oxide ceramics superfine powder, including apparatus main body are provided with inert gas pump, institute at the top of described device main body
The outer surface side for stating inert gas pump passes through appendix through the outer surface for the treatment of box and extends to the inside for the treatment of box, institute
The side for stating treatment box is provided with discharge nozzle, and the interior lower section of the treatment box is provided with and is pyrolyzed storehouse, while the treatment box
Top is provided with grinding motor, and the other side of the treatment box is connected with dehvery pump, the appearance of the dehvery pump by conveying pipeline
Face is provided with exhaust filter opening, and the side of the dehvery pump is connected with hot polymerization storehouse by conveying pipeline, sets at the top of the hot polymerization storehouse
It is equipped with stirring motor, and the outer surface side in the hot polymerization storehouse is provided with commissioning pipe, the bottom of described device main body is provided with ten thousand
To wheel.
Preferably, the bottom of the grinding motor is connected with grinding block by first rotating shaft, and the grinding block passes through first
Shaft is connect with grinding motor activity.
Preferably, the bosom of the treatment box is provided with filter plate, the filter plate by welding with treatment box
It is fixed.
Preferably, the bottom of the stirring motor is connected with paddle by the second shaft.
Preferably, the inner surface in the pyrolysis storehouse, dehvery pump and hot polymerization storehouse is provided with heater.
Preferably, the inner surface side in the pyrolysis storehouse is provided with temperature inductor, sets above the temperature inductor
It is equipped with solenoid valve.
Compared with prior art, the utility model has the beneficial effects that this kind, which is based on heat polymerization, prepares non-oxidized substance
The equipment of ceramic ultrafine powder body, increase are provided with temperature inductor and temperature indicator, and temperature inductor can be to treatment box inside
Temperature detected, and shown, observed convenient for user, while this kind of device is provided with temperature by temperature indicator
Knob can make user that the heter temperature inside treatment box be adjusted by temperature adjustment knob, to make this kind of device
It operates more convenient, increases the working efficiency of this kind of device, while this kind of device is provided with universal wheel, filled using this kind
During setting, universal wheel can be mobile convenient for device.
Detailed description of the invention
FIG. 1 is a schematic structural view of the utility model；
Fig. 2 is the utility model schematic diagram of internal structure；
Fig. 3 is the utility model collection cabinet structural schematic diagram.
In figure: 1, apparatus main body, 2, treatment box, 3, appendix, 4, inert gas pump, 5, grinding motor, 6, conveying pipeline, 7,
Dehvery pump, 8, stirring motor, 9, universal wheel, 10, hot polymerization storehouse, 11, commissioning pipe, 12, heater, 13, first rotating shaft, 14, grinding
Block, the 15, second shaft, 16, paddle, 17, filter plate, 18, solenoid valve, 19, temperature inductor, 20, temperature indicator, 21, temperature
Spend knob, 22, exhaust filter opening, 23, discharge nozzle.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Please refer to Fig. 1-3, the utility model provides a kind of technical solution: one kind is prepared non-oxygen based on solvent thermal polymerization reaction
The equipment of compound ceramic ultrafine powder body, including apparatus main body 1, battery 2, driving motor 3, vacuum pump 4, water inlet pipe 5, heat dissipation filter
Hole 6, heat-dissipating storehouse 7, support column 8, vacuum tube 9, vacuum pump 10, exhaust pipe 11, station 12, temperature indicator 13, start button
14, radiate button 15, universal wheel 16, radiating motor 17, first rotating shaft 18, radiating vane 19, heater 20, rotation sample bin
21, graphite target 22, electron gun 23, metallic target 24, outlet pipe 25, temperature inductor 26, the second shaft 27, described device main body 1
Top be provided with inert gas pump 4, the outer surface side of inert gas pump 4 is by appendix 3 through treatment box 2
Outer surface and the inside for extending to treatment box 2, the side of the treatment box 2 is provided with discharge nozzle 23, and the treatment box 2 is interior
Lower section is provided with pyrolysis storehouse 24, while the top of the treatment box 2 is provided with grinding motor 5, and the other side of the treatment box 2 is logical
It crosses conveying pipeline 6 and is connected with dehvery pump 7, the outer surface of the dehvery pump 7 is provided with exhaust filter opening 22, and the one of the dehvery pump 7
Side is connected with hot polymerization storehouse 10 by conveying pipeline 6, and the top in the hot polymerization storehouse 10 is provided with stirring motor 8, and the hot polymerization storehouse 10
Outer surface side be provided with commissioning pipe 11, the bottom of described device main body 1 is provided with universal wheel 9.
Preferably, the bottom of the grinding motor 5 is connected with grinding block 14 by first rotating shaft 13, and the grinding block 14 is logical
Cross first rotating shaft 13 with grinding motor 5 is flexibly connected, grinding motor 5 can by first rotating shaft 13 drive grinding block 14 to raw material into
Row grinding.
Preferably, the bosom of the treatment box 2 is provided with filter plate 17, the filter plate 17 by welding with place
Reason case 2 is fixed, and filter plate 17 can screen the raw material after grinding.
Preferably, the bottom of the stirring motor 8 is connected with paddle 16 by the second shaft 15, and paddle 16 can
The raw material in hot polymerization storehouse 10 is stirred by stirring motor 8 and the second shaft 15.
Preferably, the inner surface in the pyrolysis storehouse 24, dehvery pump 7 and hot polymerization storehouse 10 is provided with heater 12, heater
12 can heat raw material, convenient for raw material drying and carry out heat polymerization.
Preferably, the inner surface side in the pyrolysis storehouse 24 is provided with temperature inductor 19, the temperature inductor 19
Top is provided with solenoid valve 18, and temperature inductor 19 can detect the temperature inside pyrolysis case 24, and solenoid valve 18 can make to sieve
Raw material after choosing enters pyrolysis storehouse 24 and carries out high temperature pyrolysis.
Working principle: when using this kind of device, each position of device should be checked first, it is ensured that each position member of device
It just can be used after part is intact, when in use, first by apparatus main body 1 by the mobile place for needing work of universal wheel, and
Apparatus main body 1 is connected to external power supply, the organic precursor monomer of non-oxide ceramics is dissolved in toluene and by commissioning pipe 11
Hot polymerization storehouse 10 is put into, starts stirring motor 8 and drives paddle 16 to be stirred raw material by the second shaft 15, simultaneously
Heater 12 is heated when stirring raw material, so that raw material is carried out heat polymerization and is generated polymer, dehvery pump 7 can pass through conveying
Pipe 6 and heater 12 can be conveyed to the polymer of generation and are dried processing, and the dry gas generated can pass through exhaust
Filter opening 22 is discharged, and the polymer after making drying is purer, and the polymer after drying at this time enters in treatment box 2, grinding electricity
Machine 5 can grind it by first rotating shaft 13 and grinding block 14, the polymer after grinding by filter plate 17 screen after by
Solenoid valve 18 enters in pyrolysis storehouse 24, and starting inert gas pump 4, inert gas is delivered to by inert gas pump 4 by appendix 3
It is pyrolyzed in storehouse 24, while user can be examined by the temperature in temperature inductor 19 and 20 pairs of temperature indicator pyrolysis storehouses 24
It surveys and observes, and the temperature for being pyrolyzed heater 12 in storehouse 24 by 21 pairs of temperature adjustment knob is adjusted, to make polymer lazy
High temperature pyrolysis is carried out under the protection of property gas, non-oxide ceramics superfine powder can be obtained, user is finally by discharge nozzle
23 discharge powders.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired
Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.
Claims (6)
1. a kind of equipment that non-oxide ceramics superfine powder is prepared based on solvent thermal polymerization reaction, including apparatus main body (1),
It is characterized in that: being provided with inert gas pump (4), the outer surface one of the inert gas pump (4) at the top of described device main body (1)
Side passes through appendix (3) through the outer surface for the treatment of box (2) and extends to the inside for the treatment of box (2), the treatment box (2)
Side is provided with discharge nozzle (23), and the interior lower section of the treatment box (2) is provided with pyrolysis storehouse (24), while the treatment box
(2) grinding motor (5) is provided at the top of, the other side of the treatment box (2) is connected with dehvery pump (7) by conveying pipeline (6),
The outer surface of the dehvery pump (7) is provided with exhaust filter opening (22), and the side of the dehvery pump (7) is connected by conveying pipeline (6)
It is connected to hot polymerization storehouse (10), is provided with stirring motor (8) at the top of the hot polymerization storehouse (10), and the outer surface in the hot polymerization storehouse (10)
Side is provided with commissioning pipe (11), and the bottom of described device main body (1) is provided with universal wheel (9).
A kind of setting for non-oxide ceramics superfine powder is prepared based on solvent thermal polymerization reaction 2. according to claim 1
It is standby, it is characterised in that: the bottom of grinding motor (5) is connected with grinding block (14), the grinding by first rotating shaft (13)
Block (14) is flexibly connected by first rotating shaft (13) with grinding motor (5).
A kind of setting for non-oxide ceramics superfine powder is prepared based on solvent thermal polymerization reaction 3. according to claim 1
It is standby, it is characterised in that: the bosom of the treatment box (2) is provided with filter plate (17), the side that the filter plate (17) passes through welding
Formula is fixed with treatment box (2).
A kind of setting for non-oxide ceramics superfine powder is prepared based on solvent thermal polymerization reaction 4. according to claim 1
It is standby, it is characterised in that: the bottom of the stirring motor (8) is connected with paddle (16) by the second shaft (15).
A kind of setting for non-oxide ceramics superfine powder is prepared based on solvent thermal polymerization reaction 5. according to claim 1
It is standby, it is characterised in that: the inner surface of pyrolysis storehouse (24), dehvery pump (7) and hot polymerization storehouse (10) is provided with heater (12).
A kind of setting for non-oxide ceramics superfine powder is prepared based on solvent thermal polymerization reaction 6. according to claim 1
It is standby, it is characterised in that: the inner surface side of pyrolysis storehouse (24) is provided with temperature inductor (19), the temperature inductor
(19) solenoid valve (18) are provided with above.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820522305.2U CN208279328U (en) | 2018-04-13 | 2018-04-13 | A kind of equipment that non-oxide ceramics superfine powder is prepared based on solvent thermal polymerization reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820522305.2U CN208279328U (en) | 2018-04-13 | 2018-04-13 | A kind of equipment that non-oxide ceramics superfine powder is prepared based on solvent thermal polymerization reaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208279328U true CN208279328U (en) | 2018-12-25 |
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ID=64749094
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820522305.2U Expired - Fee Related CN208279328U (en) | 2018-04-13 | 2018-04-13 | A kind of equipment that non-oxide ceramics superfine powder is prepared based on solvent thermal polymerization reaction |
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| Country | Link |
|---|---|
| CN (1) | CN208279328U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113527136A (en) * | 2021-08-19 | 2021-10-22 | 浙江迪邦化工有限公司 | System and process for producing paranitroaniline diazonium salt |
-
2018
- 2018-04-13 CN CN201820522305.2U patent/CN208279328U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113527136A (en) * | 2021-08-19 | 2021-10-22 | 浙江迪邦化工有限公司 | System and process for producing paranitroaniline diazonium salt |
| CN113527136B (en) * | 2021-08-19 | 2023-08-04 | 浙江迪邦化工有限公司 | System and process for producing diazonium salt of p-nitroaniline |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20181225 Termination date: 20210413 |