Drying and pyrolyzing device for acid leaching pulp liquid
Technical Field
The invention belongs to the technical field of ore resource wet smelting, and particularly relates to a drying pyrolysis device for acid leaching ore pulp liquid.
Background
In industrial production, after mineral resources such as ferronickel and the like are leached by an acid solution, the separation of nickel, iron and the like contained in a leaching solution is difficult, and the traditional processes such as evaporation, crystallization, calcination and the like are adopted, so that the process flow is complex, the equipment investment cost is high, and the energy consumption is relatively large. Compared with the traditional drying and pyrolysis equipment, the leaching solution is too complex in composition, moisture can be evaporated firstly in the drying and pyrolysis process, nitrogen oxide gas is generated through decomposition, the defects of unsmooth liquid hanging, low efficiency and the like exist in a paddle type drying machine and a roller type drying machine, a disc drying machine is used for drying solid materials with large humidity, liquid or slurry cannot be dried, and the defects that local material viscosity is too large, the materials are bonded on the disc wall and are difficult to clean, the discharging is complicated and the like exist.
Disclosure of Invention
The invention aims to solve the technical problems of complex process, difficult separation, overlarge energy consumption, low efficiency, unsmooth discharging and the like in the prior art, and provides the drying and pyrolyzing device for the acid leaching ore pulp liquid, which has high pyrolysis efficiency, relatively low energy consumption, simple discharging and stable operation.
The technical problem solved by the invention is realized by adopting the following technical scheme:
the utility model provides a dry pyrolysis device of acid leaching pulp liquid, includes the shell body, the shell body outside sets up external heating coil pipe, shell body upper end sets up the gas vent, the shell body lower extreme sets up the slag notch, suit thick liquid pyrolysis dish group on the transmission shaft in the middle of the shell body, the transmission shaft is hollow structure, thick liquid pyrolysis dish group includes thick liquid pyrolysis dish, with the supporting inlet pipe, scraper, steel brush and the auto sucking device that uses of thick liquid pyrolysis dish, inlet pipe, scraper, steel brush, auto sucking device are fixed to be set up on the shell body, are located thick liquid pyrolysis dish top, thick liquid pyrolysis dish rotates along with the transmission shaft, the inlet pipe is used for the feed of thick liquid pyrolysis dish, scraper and steel brush are used for peeling off of thick liquid pyrolysis dish material, the auto sucking device is used for absorbing the material on the thick liquid pyrolysis dish, transmission device is connected with the transmission shaft, the transmission shaft is the quill shaft, the slurry pyrolysis disc is provided with a heat source inlet and a heat source outlet, wherein the heat source inlet is communicated with heat source interfaces arranged on two sides of the joint of the transmission shaft and the slurry pyrolysis disc through a first heat source pipe, and the heat source outlet is communicated with a second heat source pipe; the second heat source pipe discharges the heat source out of the outer shell along the transmission shaft; the transmission shaft is provided with a transmission wheel which is in meshed transmission with the motor transmission device.
And a transmission shaft in the middle of the outer shell is sleeved with a plurality of layers of slurry pyrolysis disc groups from top to bottom.
And the inner lower part of the outer shell is provided with an inclined plate which is positioned below the slurry pyrolysis disc group.
The slurry pyrolysis disc is a circular ring disc, the axial inner side plate wall is higher than the outer side plate wall and comprises an upper pyrolysis disc and a lower pyrolysis disc, the inner part of the slurry pyrolysis disc is of a hollow structure, the inner cavity is provided with a flow channel type reinforcing rib plate, the outermost end of the bottom of the lower pyrolysis disc is provided with a heat source inlet, and the axial inner side plate of the upper pyrolysis disc is provided with a heat source outlet.
And a blind end is arranged on the transmission shaft above the uppermost layer of the slurry pyrolysis disc in the outer shell.
The upper end of the outer shell is provided with a temperature measuring port.
The shell body is provided with a detachable observation window.
The material suction device is a dust suction type system, and is provided with a gear device for adjusting the gap between the material suction device and the slurry pyrolysis disc up and down.
The lower end of the transmission shaft is provided with a rotary joint, and a heat source enters the transmission shaft through the rotary joint.
The inlet pipe is a straight pipe, and a plurality of discharge holes are axially distributed at the bottom of the pipe wall above the slurry pyrolysis disc.
The invention has the beneficial effects that: compared with the traditional equipment for drying liquid materials, the equipment has a vertical structure, is small in spatial arrangement, increases the contact surface area of the materials, improves the drying and pyrolysis efficiency, and reduces the energy consumption to some extent; secondly, innovation is carried out on the basis of a traditional disc dryer, an outer jacket type and disc hollow inner cavity double-heating system is adopted, the pyrolysis speed of the slurry is increased, meanwhile, the slurry pyrolysis disc can intermittently rotate, other auxiliary components such as a scraper and a steel brush do not rotate, the number of rotating components is small, the operation stability of the equipment is good, and the power consumption is low; moreover, dry materials adopt a dust collection mode, and compared with a scraper chute structure, the material discharging is simple and thorough.
Drawings
FIG. 1 is a schematic view of a housing of the present invention;
FIG. 2 is a top view of the interior of the present invention;
FIG. 3 is a schematic top view of the structure of a slurry pyrolysis tray of the present invention;
FIG. 4 is a cross-sectional view of the present invention;
FIG. 5 is a structural sectional view of a slurry pyrolysis disc of the present invention.
Detailed Description
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described in detail with reference to the attached drawings:
as shown in fig. 1, fig. 2, fig. 3, fig. 4 and fig. 5, the drying and pyrolyzing device for acid leaching ore pulp liquid comprises an outer shell 15, an external heating coil 1 is arranged outside the outer shell 15, a detachable observation window 4 is arranged on the outer shell 15, and a feeding pipe 13, a scraper 12, a steel brush 10 and a material sucking device 8 are convenient to observe and detach. The upper end of the outer shell 15 is provided with an exhaust port 3 and a temperature measuring port 2, and the exhaust port 3 of the outer shell is connected with a fan and used for pumping out moisture, nitrogen oxide and other gases evaporated in the drying and pyrolysis process. The lower end of one side of the outer shell 15 is provided with a slag outlet 5, the lower part of the other side of the outer shell 15 is provided with an inclined plate 14, the inclined plate 14 is positioned in the outer shell 15 below the slurry pyrolysis disc group, and the inclined plate 14 is convenient for collecting solid materials scattered from the slurry pyrolysis disc 9 and discharging from the slag outlet 5. A transmission shaft 17 in the middle of the outer shell 15 is sleeved with a plurality of layers of slurry pyrolysis disc groups from top to bottom. A blind end is arranged on the transmission shaft above the slurry pyrolysis disc 9 at the uppermost layer in the outer shell 15, so as to prevent a heat source from passing a shortcut. The transmission shaft 17 has a hollow structure. The slurry pyrolysis disc set comprises a slurry pyrolysis disc 9, a feeding pipe 13, a scraper 12, a steel brush 10, a material sucking device 8 and a transmission device 7, wherein the feeding pipe is matched with the slurry pyrolysis disc 9, and a spring is arranged between the scraper 12, the steel brush 10 and an outer shell 15. Wherein inhale material device 8 and be dust absorption formula system, through outside suction with dry material through inhaling the material pipe and collect outside material storehouse, inhale material device 8 simultaneously and be equipped with the gear device and be used for adjusting from top to bottom and the clearance of thick liquid pyrolysis dish 9. The steel brush 10 is a roller type needle brush, which is convenient for secondary stripping of materials which are not thoroughly scraped. As shown in fig. 4, the slurry pyrolysis disc 9 is a circular disc, and is formed by welding an upper pyrolysis disc and a lower pyrolysis disc, the inner part of the slurry pyrolysis disc is of a hollow structure, and a flow channel type reinforcing rib plate 16 is welded in an inner cavity of the slurry pyrolysis disc, so that a heat source can conveniently flow according to a specified path without short cut. The central part of the slurry pyrolysis disc 9 is of a hollow structure, and the axial inner side plate wall is higher than the axial outer side plate wall, so that dry materials are prevented from extruding out of the slurry pyrolysis disc 9 from the inner side under the action of the scraper 12. The lower pyrolysis disc hollow edge surpasss the upper pyrolysis disc hollow edge, is convenient for carry out bolted connection with 4 channel-section steels that support in lower pyrolysis disc bottom and equipartition and fixes thick liquids pyrolysis disc 9, and the channel-section steel is fixed with bolted connection with transmission shaft 17 respectively again. The second heat source tube 11 is arranged in the channel steel for supporting. The outermost end of the bottom of the lower pyrolysis disc is provided with a heat source inlet, and the axial inner side plate of the upper pyrolysis disc is provided with a heat source outlet. Wherein, the heat source inlet is communicated with heat source interfaces arranged at two sides of the joint of the transmission shaft 17 and the slurry pyrolysis disc 9 through a first heat source pipe 18, and the heat source outlet is communicated with a second heat source pipe 11; the second heat source pipe 11 is connected with the heat source outlet of the slurry pyrolysis disc 9 through threads or welded, and a movable joint is arranged on the second heat source pipe 11, so that the second heat source pipe is convenient to overhaul and disassemble. All the second heat source tubes 11 discharge the heat source out of the outer shell 15 along the channel steel on the transmission shaft 17, and the connection point of all the second heat source tubes 11 and the transmission shaft 17 is higher than the blind end of the middle transmission shaft 17, so that the heat source can return to the heat source system from the end of the transmission shaft 17. The first heat source pipe 18, the second heat source pipe 11 and the slurry pyrolysis disc 9 rotate together with the transmission shaft 17. The transmission shaft 17 is provided with a transmission wheel which is in meshed transmission with the motor transmission device. The lower end of the transmission shaft 17 is provided with a rotary joint 6, and a heat source enters the transmission shaft 17 through the rotary joint 6. The length of a material suction pipe of the material suction device 8 is equal to the radius of the annular disc, the material inlet pipe 13 is a straight pipe, a plurality of material outlet holes are distributed at the bottom of the pipe wall above the slurry pyrolysis disc 9 along the axial direction, and the material inlet pipe 13 has enough distance from the steel brush to keep the material drying time as long as possible.
The specific implementation process of the invention comprises the following steps: acid leaching slurry is uniformly distributed to slurry pyrolysis discs 9 of each layer of slurry pyrolysis disc set through a feeding pipe 13, the liquid distribution thickness is 3-5mm, meanwhile, a part of heat sources enter an external heating coil pipe 1 through a heat source inlet to be heated, a part of heat sources enter the slurry pyrolysis discs 9 layer by layer through a first heat source pipe 18 through a rotary joint 6 at the lower end of a hollow transmission shaft, liquid is filled in the inner cavities of the slurry pyrolysis discs 9 according to a flow channel, and then flows back to a second heat source pipe 11 communicated with a heat source outlet through a branch pipe, and the second heat source pipe 11 returns to a heat source heating system from the rotary joint at the upper end of the hollow transmission shaft. And the temperature of the heat source is adjusted through the temperature feedback of the temperature measuring port 2 in the middle process. The acid leaching ore pulp on the pulp pyrolysis disc 9 is firstly evaporated and then decomposed under the action of a heat source, and the generated water vapor and gas are pumped away by an external fan from the exhaust port 3 at the top. After the materials are pyrolyzed and dried through the observation hole 4 after a certain time, the slurry pyrolysis disc 9 is rotated by starting the motor, and in the rotating process, the materials are contacted with the scraper 12 and the steel brush 10 to be made into powdery materials. In the process, the scraper 12 and the steel brush 10 are provided with springs, so that the gap can be automatically adjusted up and down, and the scraper and the steel brush cannot be clamped with materials. The gear of the material suction device 8 is adjusted again to tightly contact the material suction pipe with the slurry pyrolysis disc 9, and the material suction device 8 is started to intensively recycle the materials to an external material bin. After all the materials in each layer are recovered, the process is repeated. The starting of the motor can be manually operated, and the automatic operation can also be realized by controlling the time.