CN208151246U - A kind of renewable processing system for colistin sulfate - Google Patents

A kind of renewable processing system for colistin sulfate Download PDF

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Publication number
CN208151246U
CN208151246U CN201820459779.7U CN201820459779U CN208151246U CN 208151246 U CN208151246 U CN 208151246U CN 201820459779 U CN201820459779 U CN 201820459779U CN 208151246 U CN208151246 U CN 208151246U
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China
Prior art keywords
tank
valve
hydrochloric acid
acid tank
soda
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CN201820459779.7U
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Chinese (zh)
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陈青
向男君
蔡万进
洪川林
黄志强
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Livzon Group Fuzhou Fuxing Pharmaceutical Co Ltd
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Livzon Group Fuzhou Fuxing Pharmaceutical Co Ltd
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Abstract

The utility model relates to field of biological pharmacy, more particularly to a kind of renewable processing system for colistin sulfate, including filtrate tank, the first sulphuric acid tank, the second sulphuric acid tank, water tank, adsorption column, the first hydrochloric acid tank, the second hydrochloric acid tank, alkali water tank, soda water pot, desorption flow container, the first shut-off valve, the second shut-off valve, pH value detector and controller;The filtrate tank, the first sulphuric acid tank, the second sulphuric acid tank, water tank, the first hydrochloric acid tank and alkali water tank are connect with one end of the adsorption column respectively.The utility model only needs the drinking water of 40T or so that can reach soda effect, has saved a large amount of drinking water, and the soda period is also reduced to 18h by original for 24 hours, the period of resin regeneration also accordingly shortens, the utilization rate for improving equipment, reduces energy consumption cost, improves production capacity.In addition the utility model only generates the waste water less than former technology half, reduces the treating capacity of waste water, reduces the pressure of environmental protection.

Description

A kind of renewable processing system for colistin sulfate
Technical field
The utility model relates to field of biological pharmacy more particularly to a kind of renewable processing systems for colistin sulfate System.
Background technique
Adsorption and desorption is the committed step in colistin sulphate production process, and the height of resin adsorption ability directly affects Quality, yield and production capacity of product etc., and the regeneration effect of resin also will have a direct impact on the adsorption capacity of resin.Logical alkali cleaning alkali It is one of most important step in resin regeneration, needs to be washed till the pH value of the resin after having led to alkali in suitable range again with water It is adsorbed.Need the drinking water of 100T or so in soda, the period of soda the amount of resin of each adsorption column 4T at present In left and right for 24 hours, still remain the soda period it is long caused by the regeneration period is long, production capacity is low;The amount of soda process consumption of potable water compared with More, energy consumption cost is high;The soda water that soda process generates is discharged into environmentally friendly pond processing as waste water, and environmental protection pressure is big.
Based on this, provides and a kind of simple easily realize, the soda period can be shortened and improve the colistin sulfate of production capacity Renewable processing system is very necessary.
Utility model content
In order to overcome the defects of the prior art described above, the technical problem to be solved by the utility model is to provide a kind of simple It easily realizes, the soda period can be shortened and improve the renewable processing system for colistin sulfate of production capacity.
In order to solve the above-mentioned technical problem, the technical solution adopted in the utility model is:It is a kind of for colistin sulfate Renewable processing system, including filtrate tank, the first sulphuric acid tank, the second sulphuric acid tank, water tank, adsorption column, the first hydrochloric acid tank, the second salt Sour tank, alkali water tank, soda water pot, desorption flow container, the first shut-off valve, the second shut-off valve, pH value detector and controller;
The filtrate tank, the first sulphuric acid tank, the second sulphuric acid tank, water tank, the first hydrochloric acid tank and alkali water tank respectively with the suction One end of attached column connects, and the other end of the adsorption column is connect with the desorption flow container, and one end of the soda water pot passes through the One shut-off valve is connect with one end of the adsorption column, and the other end of the soda water pot passes through the second shut-off valve and the adsorption column Other end connection, second hydrochloric acid tank connect with one end of the soda water pot, described in the pH value detector is mounted on The inside of soda water pot, the controller are connect with first shut-off valve, the second shut-off valve and pH value detector respectively.
In an alternative embodiment, the concentration expressed in percentage by volume of sulfuric acid is 0.5% in first sulphuric acid tank, second sulfuric acid The concentration expressed in percentage by volume of sulfuric acid is 2.8% in tank.
In an alternative embodiment, the concentration expressed in percentage by volume of hydrochloric acid is 5% in first hydrochloric acid tank, second hydrochloric acid tank The concentration expressed in percentage by volume of middle hydrochloric acid is 10%~20%, and the concentration expressed in percentage by volume of alkali is 5% in the alkali water tank.
In an alternative embodiment, the other end of the adsorption column is equipped with waste liquid outlet.
In an alternative embodiment, the renewable processing system further includes check (non-return) valve, and the check (non-return) valve is mounted on the suction Between attached column and soda water pot.
The beneficial effects of the utility model are:A kind of renewable processing system for colistin sulfate is provided, including Filtrate tank, the first sulphuric acid tank, the second sulphuric acid tank, water tank, adsorption column, the first hydrochloric acid tank, the second hydrochloric acid tank, alkali water tank, soda water Tank, desorption flow container, the first shut-off valve, the second shut-off valve, pH value detector and controller, by will be generated during resin soda Soda water collect, the pH value of soda water is adjusted to neutrality with hydrochloric acid, then be used to wash resin.It only needs so left with 40T Right drinking water can reach soda effect, therefore save a large amount of drinking water, also, the soda period is also by original It is reduced to 18h for 24 hours, thus the period of resin regeneration also accordingly shortens, and improves the utilization rate of equipment, reduces energy consumption cost, Improve production capacity.In addition the utility model only generates the waste water less than former technology half, reduces the treating capacity of waste water, reduces The pressure of environmental protection.
Detailed description of the invention
Fig. 1 show the structural representation of the renewable processing system for colistin sulfate of the utility model embodiment Figure;
Label declaration:
1- filtrate tank;
The first sulphuric acid tank of 2-;
The second sulphuric acid tank of 3-;
4- water tank;
5- adsorption column;
The first hydrochloric acid tank of 6-;The second hydrochloric acid tank of 61-;62- alkali water tank;63- soda water pot;
64- desorbs flow container;The first shut-off valve of 65-;The second shut-off valve of 66-;67-pH value detector;68- controller;69- Check (non-return) valve.
Specific embodiment
For technology contents, the objects and the effects that the utility model is described in detail, below in conjunction with embodiment and match Attached drawing is closed to be explained.
The design of the utility model most critical is:The soda water generated during resin soda is collected, salt is used The pH value of soda water is adjusted to neutrality by acid, then is used to wash resin.
It please refers to shown in Fig. 1, a kind of renewable processing system for colistin sulfate of the utility model, including filtrate Tank, the first sulphuric acid tank, the second sulphuric acid tank, water tank, adsorption column, the first hydrochloric acid tank, the second hydrochloric acid tank, alkali water tank, soda water pot, solution Imbibition tank, the first shut-off valve, the second shut-off valve, pH value detector and controller;
The filtrate tank, the first sulphuric acid tank, the second sulphuric acid tank, water tank, the first hydrochloric acid tank and alkali water tank respectively with the suction One end of attached column connects, and the other end of the adsorption column is connect with the desorption flow container, and one end of the soda water pot passes through the One shut-off valve is connect with one end of the adsorption column, and the other end of the soda water pot passes through the second shut-off valve and the adsorption column Other end connection, second hydrochloric acid tank connect with one end of the soda water pot, described in the pH value detector is mounted on The inside of soda water pot, the controller are connect with first shut-off valve, the second shut-off valve and pH value detector respectively.
As can be seen from the above description, the beneficial effects of the utility model are:By being washed what is generated during resin soda Buck collects, and the pH value of soda water is adjusted to neutrality with hydrochloric acid, then be used to wash resin.It is only needed in this way with 40T's or so Drinking water can reach soda effect, therefore save a large amount of drinking water, also, the soda period is also by original drop for 24 hours As low as 18h, thus the period of resin regeneration also accordingly shortens, and improves the utilization rate of equipment, reduces energy consumption cost, improves Production capacity.In addition the utility model only generates the waste water less than former technology half, reduces the treating capacity of waste water, reduces environmental protection Pressure.
Further, the concentration expressed in percentage by volume of sulfuric acid is 0.5% in first sulphuric acid tank, sulphur in second sulphuric acid tank The concentration expressed in percentage by volume of acid is 2.8%.
As can be seen from the above description, being carried out using the sulfuric acid that the concentration expressed in percentage by volume in the first sulphuric acid tank is 0.5% to filtrate Pre- to elute operation, the sulfuric acid that the concentration expressed in percentage by volume in the second sulphuric acid tank is 2.8% carries out formal elution operation, reduction to filtrate Total dosage of sulfuric acid, the reduction of desalination amount of resin also accordingly reduce acid used in resin regeneration process in desorption process The dosage of alkali and drinking water, desorption production cycle foreshorten to 22h from original 28h, improve production capacity.
Further, the concentration expressed in percentage by volume of hydrochloric acid is 5% in first hydrochloric acid tank, hydrochloric acid in second hydrochloric acid tank Concentration expressed in percentage by volume be 10%~20%, the concentration expressed in percentage by volume of alkali is 5% in the alkali water tank.
As can be seen from the above description, hydrochloric acid in the first hydrochloric acid tank is to carry out the logical sour operation of adsorption column, in the second hydrochloric acid tank Hydrochloric acid the pH value of soda water is adjusted to neutrality.
Further, the other end of the adsorption column is equipped with waste liquid outlet.
As can be seen from the above description, waste liquid outlet is to the waste liquid after elution is discharged.
Further, the renewable processing system further includes check (non-return) valve, the check (non-return) valve be mounted on the adsorption column and Between soda water pot.
As can be seen from the above description, check (non-return) valve can prevent the soda water in soda water pot from flowing back, system operation ensure that Stability.
It please refers to shown in Fig. 1, the embodiments of the present invention one are:A kind of renewable processing system for colistin sulfate System, including filtrate tank 1, the first sulphuric acid tank 2, the second sulphuric acid tank 3, water tank 4, adsorption column 5, the first hydrochloric acid tank 6, the second hydrochloric acid tank 61, alkali water tank 62, soda water pot 63, desorption flow container 64, the first shut-off valve 65, the second shut-off valve 66, pH value detector 67 and control Device 68 processed;
The filtrate tank 1, the first sulphuric acid tank 2, the second sulphuric acid tank 3, water tank 4, the first hydrochloric acid tank 6 and alkali water tank 62 respectively with One end of the adsorption column 5 connects, and the other end of the adsorption column 5 is connect with the desorption flow container 64, the soda water pot 63 One end connect with one end of the adsorption column 5 by the first shut-off valve 65, the other end of the soda water pot 63 passes through second Shut-off valve 66 is connect with the other end of the adsorption column 5, and second hydrochloric acid tank 61 is connect with one end of the soda water pot 63, The pH value detector 67 is mounted on the inside of the soda water pot 63, the controller 68 respectively with first shut-off valve 65, the second shut-off valve 66 and pH value detector 67 connect.
It please refers to shown in Fig. 1, the embodiments of the present invention two are:A kind of renewable processing system for colistin sulfate System, including filtrate tank 1, the first sulphuric acid tank 2, the second sulphuric acid tank 3, water tank 4, adsorption column 5, the first hydrochloric acid tank 6, the second hydrochloric acid tank 61, alkali water tank 62, soda water pot 63, desorption flow container 64, the first shut-off valve 65, the second shut-off valve 66, pH value detector 67 and control Device 68 processed;
The filtrate tank 1, the first sulphuric acid tank 2, the second sulphuric acid tank 3, water tank 4, the first hydrochloric acid tank 6 and alkali water tank 62 respectively with One end of the adsorption column 5 connects, and the other end of the adsorption column 5 is connect with the desorption flow container 64, the soda water pot 63 One end connect with one end of the adsorption column 5 by the first shut-off valve 65, the other end of the soda water pot 63 passes through second Shut-off valve 66 is connect with the other end of the adsorption column 5, and second hydrochloric acid tank 61 is connect with one end of the soda water pot 63, The pH value detector 67 is mounted on the inside of the soda water pot 63, the controller 68 respectively with first shut-off valve 65, the second shut-off valve 66 and pH value detector 67 connect.The other end of the other end of the soda water pot 63 and the adsorption column 5 Between equipped with the basin of 1 60T be configured to temporarily store soda water.
The concentration expressed in percentage by volume of sulfuric acid is 0.5% in first sulphuric acid tank 2, the body of sulfuric acid in second sulphuric acid tank 3 Product percentage concentration is 2.8%.The concentration expressed in percentage by volume of hydrochloric acid is 5% in first hydrochloric acid tank 6, in second hydrochloric acid tank 61 The concentration expressed in percentage by volume of hydrochloric acid is 10%~20%, and the concentration expressed in percentage by volume of alkali is 5% in the alkali water tank 62.The adsorption column 5 other end is equipped with waste liquid outlet.The renewable processing system further includes check (non-return) valve 69, and the check (non-return) valve 69 is mounted on described Between adsorption column 5 and soda water pot 63.
In conclusion a kind of renewable processing system for colistin sulfate provided by the utility model, including filtrate Tank, the first sulphuric acid tank, the second sulphuric acid tank, water tank, adsorption column, the first hydrochloric acid tank, the second hydrochloric acid tank, alkali water tank, soda water pot, solution Imbibition tank, the first shut-off valve, the second shut-off valve, pH value detector and controller, by being washed what is generated during resin soda Buck collects, and the pH value of soda water is adjusted to neutrality with hydrochloric acid, then be used to wash resin.It is only needed in this way with 40T's or so Drinking water can reach soda effect, therefore save a large amount of drinking water, also, the soda period is also by original drop for 24 hours As low as 18h, thus the period of resin regeneration also accordingly shortens, and improves the utilization rate of equipment, reduces energy consumption cost, improves Production capacity.In addition the utility model only generates the waste water less than former technology half, reduces the treating capacity of waste water, reduces environmental protection Pressure.
The above description is only the embodiments of the present invention, and therefore it does not limit the scope of the patent of the utility model, all Equivalents made based on the specification and figures of the utility model are applied directly or indirectly in relevant technology neck Domain is also included in the patent protection scope of the utility model.

Claims (5)

1. a kind of renewable processing system for colistin sulfate, which is characterized in that including filtrate tank, the first sulphuric acid tank, Two sulphuric acid tanks, water tank, adsorption column, the first hydrochloric acid tank, the second hydrochloric acid tank, alkali water tank, soda water pot, desorption flow container, the first cut-off Valve, the second shut-off valve, pH value detector and controller;
The filtrate tank, the first sulphuric acid tank, the second sulphuric acid tank, water tank, the first hydrochloric acid tank and alkali water tank respectively with the adsorption column One end connection, the other end of the adsorption column connect with the desorption flow container, and one end of the soda water pot is by first section Only valve is connect with one end of the adsorption column, and the other end of the soda water pot is another by the second shut-off valve and the adsorption column One end connection, second hydrochloric acid tank are connect with one end of the soda water pot, and the pH value detector is mounted on the soda The inside of water pot, the controller are connect with first shut-off valve, the second shut-off valve and pH value detector respectively.
2. the renewable processing system according to claim 1 for colistin sulfate, which is characterized in that first sulphur The concentration expressed in percentage by volume of sulfuric acid is 0.5% in sour tank, and the concentration expressed in percentage by volume of sulfuric acid is 2.8% in second sulphuric acid tank.
3. the renewable processing system according to claim 1 for colistin sulfate, which is characterized in that first salt The concentration expressed in percentage by volume of hydrochloric acid is 5% in sour tank, and the concentration expressed in percentage by volume of hydrochloric acid is 10%~20% in second hydrochloric acid tank, The concentration expressed in percentage by volume of alkali is 5% in the alkali water tank.
4. the renewable processing system according to claim 1 for colistin sulfate, which is characterized in that the adsorption column The other end be equipped with waste liquid outlet.
5. the renewable processing system according to claim 1 for colistin sulfate, which is characterized in that described renewable Processing system further includes check (non-return) valve, and the check (non-return) valve is mounted between the adsorption column and soda water pot.
CN201820459779.7U 2018-04-03 2018-04-03 A kind of renewable processing system for colistin sulfate Active CN208151246U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820459779.7U CN208151246U (en) 2018-04-03 2018-04-03 A kind of renewable processing system for colistin sulfate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820459779.7U CN208151246U (en) 2018-04-03 2018-04-03 A kind of renewable processing system for colistin sulfate

Publications (1)

Publication Number Publication Date
CN208151246U true CN208151246U (en) 2018-11-27

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Application Number Title Priority Date Filing Date
CN201820459779.7U Active CN208151246U (en) 2018-04-03 2018-04-03 A kind of renewable processing system for colistin sulfate

Country Status (1)

Country Link
CN (1) CN208151246U (en)

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