CN208140699U - It is a kind of for measuring the device of soil available nitrogen - Google Patents

It is a kind of for measuring the device of soil available nitrogen Download PDF

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CN208140699U
CN208140699U CN201820560274.XU CN201820560274U CN208140699U CN 208140699 U CN208140699 U CN 208140699U CN 201820560274 U CN201820560274 U CN 201820560274U CN 208140699 U CN208140699 U CN 208140699U
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bottle
boric acid
reaction flask
threaded cap
acid absorption
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闫志丹
张文东
张淑敏
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Institute of Botany of CAS
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Abstract

The utility model relates to a kind of for measuring the device of soil available nitrogen comprising reaction flask, interconnecting piece, boric acid absorption bottle, the first threaded cap, liquid-feeding tube and the second threaded cap;For accommodating soil and sodium hydroxide solution in the reaction flask, reaction flask body portion is connected to by the interconnecting piece with the body portion of the boric acid absorption bottle;The bottle mouth position of the reaction flask is provided with first threaded cap with bottleneck cooperation, and is provided with the liquid-feeding tube in the middle part of first threaded cap;The bottle mouth position of the boric acid absorption bottle is provided with second threaded cap with bottleneck cooperation.The utility model is easy to operate, can improve the real reliability of experimental data, while ensure that higher experiment success rate, uses manpower and material resources sparingly.

Description

一种用于测定土壤有效氮的装置A device for measuring soil available nitrogen

技术领域technical field

本实用新型涉及一种土壤检定装置,特别是关于一种用于测定土壤有效氮的装置。The utility model relates to a soil testing device, in particular to a device for measuring soil available nitrogen.

背景技术Background technique

现有的测定装置由玻璃扩散皿和毛玻璃组成,扩散皿外室放置土壤样品,内室放置硼酸吸收液,外室边缘需涂抹阿拉伯胶,然后盖上毛玻璃,旋转数次,使皿边与毛玻璃完全粘合,再渐渐转开毛玻璃一边,沿狭缝迅速加入碱液,立即盖严,再用橡皮筋圈紧固定,轻轻摇动,随后放入恒温箱中碱解扩散。但是现有的这种装置经常出现实验失败的问题,例如:摇动时外室碱液混入内室;涂胶量掌握不好,样品污染或密闭性不好出现漏气等。The existing measuring device consists of a glass diffusion dish and frosted glass. The soil sample is placed in the outer chamber of the diffusion dish, and the boric acid absorption solution is placed in the inner chamber. The edge of the outer chamber needs to be coated with gum arabic, then covered with frosted glass, and rotated several times to make the edge of the dish and the ground glass Completely bonded, then gradually turn away the ground glass side, quickly add lye along the slit, immediately cover tightly, and then fix it tightly with a rubber band, shake it gently, and then put it in an incubator for alkaline solution diffusion. However, the existing device often has the problem of experimental failure, for example: when the outer chamber is shaken, the lye is mixed into the inner chamber;

发明内容Contents of the invention

针对上述问题,本实用新型的目的是提供一种用于测定土壤有效氮的装置,其操作简单,能提高实验数据的真实可靠性,同时保证了较高的实验成功率,节省人力物力。In view of the above problems, the purpose of this utility model is to provide a device for measuring soil available nitrogen, which is simple to operate, can improve the authenticity and reliability of experimental data, and at the same time ensure a higher success rate of the experiment and save manpower and material resources.

为实现上述目的,本实用新型采取以下技术方案:一种用于测定土壤有效氮的装置,其特征在于:该装置包括反应瓶、连接部、硼酸吸收瓶、第一螺纹盖、加液管和第二螺纹盖;所述反应瓶中用于容置土壤和氢氧化钠溶液,所述反应瓶瓶身部通过所述连接部与所述硼酸吸收瓶的瓶身部连通;位于所述反应瓶的瓶口处设置有与该瓶口配合的所述第一螺纹盖,且所述第一螺纹盖中部设置有所述加液管;位于所述硼酸吸收瓶的瓶口处设置有与该瓶口配合的所述第二螺纹盖。In order to achieve the above object, the utility model adopts the following technical solutions: a device for measuring soil available nitrogen, characterized in that: the device includes a reaction bottle, a connecting portion, a boric acid absorption bottle, a first screw cap, a liquid feeding pipe and The second screw cap; the reaction bottle is used to accommodate soil and sodium hydroxide solution, and the body of the reaction bottle communicates with the body of the boric acid absorption bottle through the connecting portion; it is located in the reaction bottle The bottle mouth of the bottle is provided with the first threaded cap that matches the bottle mouth, and the middle part of the first threaded cap is provided with the liquid feeding tube; the bottle mouth of the boric acid absorption bottle is provided with a The second threaded cap that fits the mouth.

进一步,位于所述加液管上设置有阀门。Further, a valve is arranged on the liquid feeding pipe.

进一步,位于所述第一螺纹盖和第二螺纹盖内均设置有橡胶垫。Further, a rubber pad is provided inside the first threaded cap and the second threaded cap.

进一步,所述反应瓶的瓶口处以及所述硼酸吸收瓶的瓶口处均设置有与螺纹盖紧密连接的外螺纹。Further, both the mouth of the reaction bottle and the mouth of the boric acid absorption bottle are provided with external threads that are tightly connected to the screw caps.

进一步,所述反应瓶和硼酸吸收瓶均采用广口瓶。Further, both the reaction bottle and the boric acid absorption bottle are wide-mouthed bottles.

进一步,所述反应瓶的瓶底直径大于所述硼酸吸收瓶的瓶底直径。Further, the bottom diameter of the reaction bottle is larger than the bottom diameter of the boric acid absorption bottle.

进一步,所述反应瓶的瓶底直径为70cm,所述硼酸吸收瓶的瓶底直径为40cm。Further, the bottom diameter of the reaction bottle is 70cm, and the bottom diameter of the boric acid absorption bottle is 40cm.

进一步,所述连接部为圆筒型结构,且所述连接部的下部侧壁距所述反应瓶和硼酸吸收瓶的瓶底处具有距离。Further, the connecting part is a cylindrical structure, and the lower side wall of the connecting part has a distance from the bottom of the reaction bottle and the boric acid absorption bottle.

进一步,所述圆筒型的连接部直径为25mm。Further, the diameter of the cylindrical connecting portion is 25mm.

进一步,所述连接部的下部侧壁距所述反应瓶和硼酸吸收瓶的瓶底处距离为35mm。Further, the distance between the lower side wall of the connecting part and the bottom of the reaction bottle and the boric acid absorption bottle is 35mm.

本实用新型由于采取以上技术方案,其具有以下优点:1、本实用新型广口瓶连通下口距瓶底35mm,摇动及放入恒温箱时,不会将碱液流入硼酸吸收瓶。2、本实用新型采用螺纹口及胶垫结构,有效避免了污染样品漏气情况。3、本实用新型螺纹盖子上加至阀门,更方便碱液的加入。4、本实用新型操作简单,能提高实验数据的真实可靠性,同时保证了较高的实验成功率,避免反复测试,节省了时间人力物力。The utility model has the following advantages due to the adoption of the above technical scheme: 1. The utility model's wide-mouth bottle communicates with the bottom of the bottle at a distance of 35 mm from the bottom of the mouth. When shaking and putting into a constant temperature box, the lye will not flow into the boric acid absorption bottle. 2. The utility model adopts the threaded port and rubber pad structure, which effectively avoids air leakage of contaminated samples. 3. The threaded cap of the utility model is added to the valve, which is more convenient for adding lye. 4. The utility model is easy to operate, can improve the authenticity and reliability of the experimental data, and at the same time ensure a high experimental success rate, avoid repeated testing, and save time, manpower and material resources.

附图说明Description of drawings

图1是本实用新型的整体结构示意图。Fig. 1 is a schematic diagram of the overall structure of the utility model.

具体实施方式Detailed ways

在本实用新型的描述中,需要理解的是,术语“上”、“下”“内”、“外”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本实用新型和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本实用新型的限制。此外,术语“第一”、“第二”仅用于描述目的,而不能理解为指示或暗示相对重要性。下面结合附图和实施例对本实用新型进行详细的描述。In the description of the present utility model, it should be understood that the orientations or positional relationships indicated by the terms "upper", "lower", "inner", "outer", etc. are based on the orientation or positional relationships shown in the drawings, and are only for the purpose of It is convenient to describe the utility model and simplify the description, but not to indicate or imply that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus should not be construed as a limitation of the utility model. In addition, the terms "first" and "second" are used for descriptive purposes only, and should not be understood as indicating or implying relative importance. Below in conjunction with accompanying drawing and embodiment the utility model is described in detail.

如图1所示,本实用新型提供一种用于测定土壤有效氮的装置,适用于土壤有效氮(碱解扩散法)的测定。本实用新型包括反应瓶1、连接部2、硼酸吸收瓶3、第一螺纹盖4、加液管5、阀门6和第二螺纹盖7。反应瓶1中用于容置土壤和氢氧化钠(NaOH)溶液,反应瓶1瓶身部通过连接部2与硼酸吸收瓶3的瓶身部连通。位于反应瓶1的瓶口处设置有与该瓶口配合的第一螺纹盖4,且第一螺纹盖4中部设置有加液管5,通过加液管5向反应瓶1内增加碱液,更加方便加碱液的操作;位于加液管5上设置有阀门6,以防止在不当操作时反应瓶1内的溶液流出。位于硼酸吸收瓶3的瓶口处设置有与该瓶口配合的第二螺纹盖7。As shown in Figure 1, the utility model provides a device for measuring soil available nitrogen, which is applicable to the measurement of soil available nitrogen (alkaline solution diffusion method). The utility model comprises a reaction bottle 1, a connecting part 2, a boric acid absorption bottle 3, a first threaded cap 4, a liquid feeding pipe 5, a valve 6 and a second threaded cap 7. The reaction bottle 1 is used to accommodate soil and sodium hydroxide (NaOH) solution, and the body of the reaction bottle 1 communicates with the body of the boric acid absorption bottle 3 through the connection part 2 . The bottleneck place that is positioned at reaction bottle 1 is provided with the first screw cap 4 that cooperates with this bottle mouth, and the middle part of the first screw cap 4 is provided with liquid-feeding pipe 5, increases lye in reaction bottle 1 by liquid-feeding pipe 5, The operation of adding lye is more convenient; a valve 6 is arranged on the liquid feeding pipe 5 to prevent the solution in the reaction bottle 1 from flowing out during improper operation. The bottle mouth of the boric acid absorption bottle 3 is provided with a second screw cap 7 matched with the bottle mouth.

上述实施例中,位于第一螺纹盖4和第二螺纹盖7内均设置有橡胶垫8,通过螺纹口及橡胶垫8能有效避免样品污染及漏气情况的发生。In the above embodiment, rubber pads 8 are provided inside the first threaded cap 4 and the second threaded cap 7 , and the sample contamination and air leakage can be effectively avoided through the threaded openings and the rubber pads 8 .

上述各实施例中,反应瓶1的瓶口处以及硼酸吸收瓶3的瓶口处均设置有外螺纹9,以便与螺纹盖进行紧密螺纹连接。In each of the above embodiments, the mouth of the reaction bottle 1 and the mouth of the boric acid absorption bottle 3 are provided with external threads 9 for tight screw connection with the screw cap.

上述各实施例中,反应瓶1的瓶底直径远大于硼酸吸收瓶3的瓶底直径,且反应瓶1和硼酸吸收瓶3均采用广口瓶。In each of the above embodiments, the diameter of the bottom of the reaction bottle 1 is much larger than that of the boric acid absorption bottle 3, and both the reaction bottle 1 and the boric acid absorption bottle 3 are wide-mouthed bottles.

在一个优选的实施例中,反应瓶1的瓶底直径为70cm,硼酸吸收瓶3的瓶底直径为40cm。In a preferred embodiment, the bottom diameter of the reaction bottle 1 is 70 cm, and the bottom diameter of the boric acid absorption bottle 3 is 40 cm.

上述各实施例中,连接部2为圆筒型结构,其直径优选为25mm,且连接部2的下部侧壁距反应瓶1和硼酸吸收瓶3的瓶底处具有距离,该距离优选为35mm。In above-mentioned each embodiment, connecting portion 2 is cylindrical structure, and its diameter is preferably 25mm, and the bottom side wall of connecting portion 2 has distance from the bottle bottom of reaction bottle 1 and boric acid absorption bottle 3, and this distance is preferably 35mm .

综上所述,本实用新型在使用时,首先把称取好的土壤样品平铺放置于反应瓶1的底部,吸收瓶3内放置定量的硼酸吸收液,然后将两个橡胶垫8分别装入对应的第一螺纹盖4和第二螺纹盖7中,旋紧反应瓶1和吸收瓶3,拧开阀门6,加入一定体积的碱液,关闭阀门6,轻轻摇动,随后放入恒温箱中碱解扩散。本实用新型可以有效避免样品污染及漏气情况的发生,操作简单,提高实验数据的真实可靠性,同时保证了较高的实验成功率,避免反复测试,节省了时间人力物力。In summary, when the utility model is in use, the soil sample that has been weighed is placed on the bottom of the reaction bottle 1, and quantitative boric acid absorption liquid is placed in the absorption bottle 3, and then the two rubber pads 8 are respectively packed. Put it into the corresponding first threaded cap 4 and the second threaded cap 7, tighten the reaction bottle 1 and the absorption bottle 3, unscrew the valve 6, add a certain volume of lye, close the valve 6, shake it gently, and then put it into a constant temperature Alkaline solution diffusion in the box. The utility model can effectively avoid the occurrence of sample pollution and air leakage, is simple to operate, improves the authenticity and reliability of experimental data, ensures a high experimental success rate, avoids repeated testing, and saves time, manpower and material resources.

上述各实施例仅用于说明本实用新型,各部件的结构、尺寸、设置位置及形状都是可以有所变化的,在本实用新型技术方案的基础上,凡根据本实用新型原理对个别部件进行的改进和等同变换,均不应排除在本实用新型的保护范围之外。The above-mentioned embodiments are only used to illustrate the utility model, and the structure, size, location and shape of each component can be changed. On the basis of the technical solution of the utility model, all individual components can The improvements and equivalent transformations should not be excluded from the protection scope of the present utility model.

Claims (10)

1. a kind of for measuring the device of soil available nitrogen, it is characterised in that:The device includes reaction flask, interconnecting piece, boric acid suction Receive bottle, the first threaded cap, liquid-feeding tube and the second threaded cap;For accommodating soil and sodium hydroxide solution in the reaction flask, institute Reaction flask body portion is stated to be connected to by the interconnecting piece with the body portion of the boric acid absorption bottle;Positioned at the bottleneck of the reaction flask Place is provided with first threaded cap with bottleneck cooperation, and is provided with the liquid-feeding tube in the middle part of first threaded cap;Position The bottle mouth position of the boric acid absorption bottle is provided with second threaded cap with bottleneck cooperation.
2. device as described in claim 1, it is characterised in that:Valve is provided on the liquid-feeding tube.
3. device as described in claim 1, it is characterised in that:It is provided in first threaded cap and the second threaded cap Rubber pad.
4. such as any one of claims 1 to 3 described device, it is characterised in that:The bottle mouth position of the reaction flask and the boric acid The bottle mouth position of absorption bottle is provided with and the close-connected external screw thread of threaded cap.
5. such as any one of claims 1 to 3 described device, it is characterised in that:The reaction flask and boric acid absorption bottle are all made of extensively Mouth bottle.
6. such as any one of claims 1 to 3 described device, it is characterised in that:The bottom of bottle diameter of the reaction flask is greater than the boron The bottom of bottle diameter of sour absorption bottle.
7. device as claimed in claim 6, it is characterised in that:The bottom of bottle diameter of the reaction flask is 70cm, and the boric acid absorbs The bottom of bottle diameter of bottle is 40cm.
8. such as any one of claims 1 to 3 described device, it is characterised in that:The interconnecting piece is cylinder type, and the company There is distance at bottom of bottle of the lower sides of socket part away from the reaction flask and boric acid absorption bottle.
9. device as claimed in claim 8, it is characterised in that:The interconnecting piece diameter of the cylinder type is 25mm.
10. device as claimed in claim 8, it is characterised in that:The lower sides of the interconnecting piece are away from the reaction flask and boric acid Distance is 35mm at the bottom of bottle of absorption bottle.
CN201820560274.XU 2018-04-19 2018-04-19 It is a kind of for measuring the device of soil available nitrogen Active CN208140699U (en)

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