CN208130559U - A kind of Siraitia grosvenorii purification chromatographic column - Google Patents

A kind of Siraitia grosvenorii purification chromatographic column Download PDF

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Publication number
CN208130559U
CN208130559U CN201721897778.2U CN201721897778U CN208130559U CN 208130559 U CN208130559 U CN 208130559U CN 201721897778 U CN201721897778 U CN 201721897778U CN 208130559 U CN208130559 U CN 208130559U
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China
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chromatographic column
fixed
electric machine
drug
feed pipe
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CN201721897778.2U
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Chinese (zh)
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黄华学
刘永胜
龙伟岸
黄伟
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JIANGXI HAIFU BIOENGINEERING CO Ltd
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JIANGXI HAIFU BIOENGINEERING CO Ltd
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Abstract

The utility model discloses a kind of Siraitia grosvenoriis to purify chromatographic column,Including chromatographic column,Feed pipe,Drug-feeding tube,Drainage conduit,Solenoid valve,Flowmeter,Electric machine support,Rotary electric machine,Agitating roller,Stirrer gear,Resistance heating wire,Temperature sensor,PLC controller and sieve plate,Bottom is fixed with sieve plate in the chromatographic column,The chromatographic column top side is fixed with feed pipe,And the other side is fixed with drug-feeding tube at the top of chromatographic column,The chromatography column bottom is fixed with discharge nozzle,The feed pipe,Discharge nozzle and drug-feeding tube are respectively and fixedly provided with solenoid valve far from one end of chromatographic column,The feed pipe and drug-feeding tube surface are located at the fixation of solenoid valve side and are respectively and fixedly provided with flowmeter,The chromatographic column top center is fixed with electric machine support,This Siraitia grosvenorii purifies chromatographic column,Agitating roller rotation is driven by rotary electric machine,Stirrer gear by stirring roller surface stirs the mixed solution of mother liquor and chemicals,It is reacted convenient for mother liquor with chemicals,Improve the working efficiency of chromatographic column,It is convenient to use.

Description

A kind of Siraitia grosvenorii purification chromatographic column
Technical field
The utility model relates to technical field, specially a kind of Siraitia grosvenorii purifies chromatographic column.
Background technique
Siraitia grosvenorii is the perennial liana of Curcurbitaceae.Its leaf is heart-shaped, dioecism, summer-flowering, seed in autumn.Chinese medicine Lung heat phlegm-fire cough, pharynx are cured mainly containing medicinal ingredients such as mogroside, a variety of amino acid and vitamins with its fruit medicine Laryngitis, tonsillitis, acute gastritis, constipation etc..It is the famous specialty in Guangxi China Guilin City.Mogroside is also known as sweet taste Element is widely used, frequently as the alternative sugar of overweight people and diabetic as sweetener due to its sugariness is high, heat is low.
With the development of modern medicine science and technology, the use of Siraitia grosvenorii is also more and more, and existing Siraitia grosvenorii is when being used as medicine The method that multi-pass crosses chromatography is purified, still, inside existing chromatographic column can not temperature control, it has not been convenient to make mother liquor and chemicals In suitable temperature, without agitating device in existing chromatographic column, can not very fast mother liquor and chemicals reaction speed, be This, it is proposed that a kind of Siraitia grosvenorii purifies chromatographic column.
Utility model content
The purpose of this utility model is to provide a kind of Siraitia grosvenoriis to purify chromatographic column, to solve to propose in above-mentioned background technique The problem of.
To achieve the above object, the utility model provides the following technical solutions:A kind of Siraitia grosvenorii purification chromatographic column, including layer Analyse column, feed pipe, drug-feeding tube, drainage conduit, solenoid valve, flowmeter, electric machine support, rotary electric machine, agitating roller, stirrer gear, resistance Heater strip, temperature sensor, PLC controller and sieve plate, bottom is fixed with sieve plate in the chromatographic column, one at the top of the chromatographic column Side is fixed with feed pipe, and the other side is fixed with drug-feeding tube at the top of chromatographic column, and the chromatography column bottom is fixed with discharge nozzle, described Feed pipe, discharge nozzle and drug-feeding tube are respectively and fixedly provided with solenoid valve, the feed pipe and drug-feeding tube surface position far from one end of chromatographic column In solenoid valve side, fixation is respectively and fixedly provided with flowmeter, and the chromatographic column top center is fixed with electric machine support, the electric machine support Inside is fixed with rotary electric machine, and the rotary electric machine output shaft is passed through and is fixedly connected at the top of chromatographic column with agitating roller top, and is turned Dynamic motor output shaft and chromatographic column are rotatablely connected by bearing, and stirrer gear is equidistantly fixed on the outside of the agitating roller;
It is fixed with resistance heating wire on the outside of the chromatographic column intermediate inner wall, the chromatography column outer wall is fixed with temperature sensing Device, and temperature sensor side is fixed with PLC controller, the temperature sensor and PLC controller input terminal are electrically connected, and PLC controller output end and resistance heating wire are electrically connected.
Preferably, the temperature sensor measurement end is located inside chromatographic column.
Preferably, the chromatographic column is equipped with the chromatographic column of heat preservation between inner and outer wall.
Preferably, the chromatographic column is made of pmma material.
Preferably, the agitating roller and stirrer gear are made of the rubber material that stability is strong and thermal conductivity is good.
Compared with prior art, the utility model has the beneficial effects that:
1, the utility model will chromatograph mother liquor by feed pipe and inject in chromatographic column, and chemicals is added by drug-feeding tube In chromatographic column, and feed pipe and drug-feeding tube top are respectively and fixedly provided with flowmeter, convenient for accurately controlling mother liquor and chemistry in chromatographic column The ratio of drug convenient for chromatography, and drives agitating roller rotation by rotary electric machine, and the stirrer gear by stirring roller surface stirs female The mixed solution of liquid and chemicals reacts with chemicals convenient for mother liquor, improves the working efficiency of chromatographic column, is easy to use.
2, the utility model detects the temperature in chromatographic column by temperature sensor, and temperature sensor passes measurement data PLC controller is passed, data are analyzed by PLC controller, when to analyze temperature in chromatographic column too low for PLC controller When, resistance heating wire's work can be controlled, the temperature in chromatographic column is improved by resistance heating wire, is in mother liquor and chemicals It is suitble to the temperature of reaction, improves the quality and speed of chromatography, and works as PLC controller and analyze in chromatographic column when the temperature is excessively high, PLC Controller can control resistance heating wire and stop working, and prevent Column temperature excessively high, chemicals is made to lose activity, and reduce and mother The reaction rate of liquid.
Detailed description of the invention
Fig. 1 is the utility model overall structure diagram;
In figure:1- chromatographic column;2- feed pipe;3- drug-feeding tube;4- discharge nozzle;5- solenoid valve;6- flowmeter;7- motor branch Frame;8- rotary electric machine;9- agitating roller;10- stirrer gear;11- resistance heating wire;12- temperature sensor;13-PLC controller;14- Sieve plate.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
Referring to Fig. 1, the utility model provides a kind of technical solution:A kind of Siraitia grosvenorii purification chromatographic column, including chromatographic column 1, feed pipe 2, drug-feeding tube 3, drainage conduit, solenoid valve 5, flowmeter 6, electric machine support 7, rotary electric machine 8, agitating roller 9, stirrer gear 10, resistance heating wire 11, temperature sensor 12, PLC controller 13 and sieve plate 14, bottom is fixed with sieve plate in the chromatographic column 1 14,1 top side of chromatographic column is fixed with feed pipe 2, and the 1 top other side of chromatographic column is fixed with drug-feeding tube 3, the chromatography 1 bottom of column is fixed with discharge nozzle 4, and the feed pipe 2, discharge nozzle 4 and drug-feeding tube 3 are respectively and fixedly provided with electricity far from one end of chromatographic column 1 Magnet valve 5, the feed pipe 2 and 3 surface of drug-feeding tube are located at the fixation of 5 side of solenoid valve and are respectively and fixedly provided with flowmeter 6, the chromatographic column 1 Top center is fixed with electric machine support 7, and rotary electric machine 8,8 output shaft of rotary electric machine are fixed with inside the electric machine support 7 Across the top of chromatographic column 1 be fixedly connected at the top of agitating roller 9, and 8 output shaft of rotary electric machine and chromatographic column 1 pass through bearing rotation company It connects, 9 outside of agitating roller is equidistantly fixed with stirrer gear 10;
Resistance heating wire 11 is fixed on the outside of 1 intermediate inner wall of chromatographic column, 1 outer wall of chromatographic column is fixed with temperature biography Sensor 12, and 12 side of temperature sensor is fixed with PLC controller 13, the temperature sensor 12 is inputted with PLC controller 13 End is electrically connected, and 13 output end of PLC controller and resistance heating wire 11 are electrically connected.
12 measurement end of temperature sensor is located inside chromatographic column 1.
The chromatographic column 1 is equipped with the chromatographic column of heat preservation between inner and outer wall.
The chromatographic column 1 is made of pmma material.
The agitating roller 9 and stirrer gear 10 are made of the rubber material that stability is strong and thermal conductivity is good.
Working principle:Mother liquor will be chromatographed by feed pipe 2 to inject in chromatographic column 1, and chemicals will be added by drug-feeding tube 3 Chromatograph in 1 column, and feed pipe 2 and 3 top of drug-feeding tube are respectively and fixedly provided with flowmeter 6, convenient for accurately control chromatographic column 1 in mother liquor with The ratio of chemicals convenient for chromatography, and drives agitating roller 9 to rotate, passes through the stirring on 9 surface of agitating roller by rotary electric machine 8 Tooth 10 stirs the mixed solution of mother liquor and chemicals, reacts convenient for mother liquor with chemicals, improves the work effect of chromatographic column 1 Rate is easy to use, and detects the temperature in chromatographic column 1 by temperature sensor 12, and temperature sensor 12 passes measurement data PLC controller 13 is passed, data are analyzed by PLC controller 13, when PLC controller 13 analyzes temperature in chromatographic column 1 When spending low, can control resistance heating wire 11 work, by resistance heating wire 11 improve chromatographic column 1 in temperature, make mother liquor and Chemicals is in the temperature for being suitble to reaction, improves the quality and speed of chromatography, and when PLC controller 13 analyzes chromatographic column 1 Inside when the temperature is excessively high, PLC controller 13 can control resistance heating wire 11 and stop working, and prevent 1 temperature of chromatographic column excessively high, make chemistry Drug loses activity, and reduces the reaction rate with mother liquor.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment Intrinsic element.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art, It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.

Claims (5)

1. a kind of Siraitia grosvenorii purifies chromatographic column, including chromatographic column(1), feed pipe(2), drug-feeding tube(3), drainage conduit, solenoid valve (5), flowmeter(6), electric machine support(7), rotary electric machine(8), agitating roller(9), stirrer gear(10), resistance heating wire(11), temperature Spend sensor(12), PLC controller(13)And sieve plate(14), it is characterised in that:The chromatographic column(1)Interior bottom is fixed with sieve plate (14), the chromatographic column(1)Top side is fixed with feed pipe(2), and chromatographic column(1)The top other side is fixed with drug-feeding tube (3), the chromatographic column(1)Bottom is fixed with discharge nozzle(4), the feed pipe(2), discharge nozzle(4)And drug-feeding tube(3)Far from layer Analyse column(1)One end be respectively and fixedly provided with solenoid valve(5), the feed pipe(2)And drug-feeding tube(3)Surface is located at solenoid valve(5)Side Fixation is respectively and fixedly provided with flowmeter(6), the chromatographic column(1)Top center is fixed with electric machine support(7), the electric machine support(7) Inside is fixed with rotary electric machine(8), the rotary electric machine(8)Output shaft passes through chromatographic column(1)Top and agitating roller(9)Top is solid Fixed connection, and rotary electric machine(8)Output shaft and chromatographic column(1)It is rotatablely connected by bearing, the agitating roller(9)Outside is equidistantly solid Surely there is stirrer gear(10);
The chromatographic column(1)Resistance heating wire is fixed on the outside of intermediate inner wall(11), the chromatographic column(1)Outer wall is fixed with temperature Sensor(12), and temperature sensor(12)Side is fixed with PLC controller(13), the temperature sensor(12)It is controlled with PLC Device processed(13)Input terminal is electrically connected, and PLC controller(13)Output end and resistance heating wire(11)It is electrically connected.
2. a kind of Siraitia grosvenorii according to claim 1 purifies chromatographic column, it is characterised in that:The temperature sensor(12)It surveys Amount end is located at chromatographic column(1)It is internal.
3. a kind of Siraitia grosvenorii according to claim 1 purifies chromatographic column, it is characterised in that:The chromatographic column(1)For inner wall The chromatographic column of heat preservation is equipped between outer wall.
4. a kind of Siraitia grosvenorii according to claim 1 purifies chromatographic column, it is characterised in that:The chromatographic column(1)By organic Glass material is constituted.
5. a kind of Siraitia grosvenorii according to claim 1 purifies chromatographic column, it is characterised in that:The agitating roller(9)And stirring Tooth(10)It is made of the rubber material that stability is strong and thermal conductivity is good.
CN201721897778.2U 2017-12-29 2017-12-29 A kind of Siraitia grosvenorii purification chromatographic column Active CN208130559U (en)

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CN201721897778.2U CN208130559U (en) 2017-12-29 2017-12-29 A kind of Siraitia grosvenorii purification chromatographic column

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Application Number Priority Date Filing Date Title
CN201721897778.2U CN208130559U (en) 2017-12-29 2017-12-29 A kind of Siraitia grosvenorii purification chromatographic column

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111857203A (en) * 2019-04-29 2020-10-30 深圳市帝迈生物技术有限公司 Glycosylated hemoglobin analyzer and temperature control system thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111857203A (en) * 2019-04-29 2020-10-30 深圳市帝迈生物技术有限公司 Glycosylated hemoglobin analyzer and temperature control system thereof

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