CN208081912U - A kind of vibration temperature-controlling reaction apparatus for extracting active substance of plant - Google Patents

A kind of vibration temperature-controlling reaction apparatus for extracting active substance of plant Download PDF

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Publication number
CN208081912U
CN208081912U CN201820372229.1U CN201820372229U CN208081912U CN 208081912 U CN208081912 U CN 208081912U CN 201820372229 U CN201820372229 U CN 201820372229U CN 208081912 U CN208081912 U CN 208081912U
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round
bottomed flask
spherical shell
spherical
drainage conduit
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CN201820372229.1U
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刘仙俊
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Taiyuan University of Science and Technology
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Taiyuan University of Science and Technology
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Abstract

The utility model discloses a kind of vibration temperature-controlling reaction apparatus for extracting active substance of plant, it is related to the extraction reaction unit of active matter, it is the setting spherical shaped transparent shell outside round-bottomed flask, include the pedestal of having heaters and ultrasonic generator in transparent outer cover setting, interlayer is formed between transparent outer cover and round-bottomed flask, water-bath can be placed in interlayer, pass through the indirectly-acting to water-bath and ultrasonic wave to water-bath, the external condition of one stable constant temperature is provided for the extraction reaction inside round-bottomed flask, device is provided with filler, water outlet, charge door and drainage conduit, the operation is more convenient;Reaction vessel and ambient temperature control device are combined into one by the present apparatus, while closed annular-heating keeps internal reaction progress more abundant, and environment is more stable;The substance of present apparatus unstable active components suitable for plant extracts, while the extraction process participated in suitable for active enzyme.

Description

A kind of vibration temperature-controlling reaction apparatus for extracting active substance of plant
Technical field
The utility model is related to the extraction elements of natural plant active material, and in particular to one kind is for extracting vegetable active The vibration temperature-controlling reaction apparatus of substance.
Background technology
According to the physicochemical property of bioactive substance molecule itself, such as solubility, charging property, size, volatility progress It isolates and purifies, the extraction of the active material of plant mostly uses:Solvent method, enzyme process extraction, steam distillation, overcritical dioxy Change carbon extraction separation, reflux extraction.Refluxing extraction is a kind of method of the extract compounds from solid matter.Refluxing extraction It is that solid is infiltrated for a long time with solvent and leaches required substance come that is, long-term lixiviation process.This method spends time length, solvent Dosage is big, inefficient.Mostly use extraction equipment for fat in laboratory extract, extraction equipment for fat it is former using solvent refluxing and siphon Reason, i.e., soxhlet extraction makes solid matter continuously be extracted by pure solvent, has not only saved solvent extraction efficiency but also high.This In extraction process, it is often necessary to connect reaction unit, that is, place the reaction vessel of plant and extractant, and usually require to treat The substance of extraction carries out continual heating, particularly with there is the extraction reaction that biological enzyme participates in the uniformity of ambient temperature and Stability requirement is stringenter, and the fluctuation of temperature can bring the decline of enzymatic activity even to inactivate, and extraction yield is caused to decline.
Utility model content
The utility model overcomes the deficiencies in the prior art, provides a kind of vibration constant temperature for extracting active substance of plant Reaction unit is especially adapted for use in the enzymolysis extraction of biological enzyme participation, can be provided for entire reaction process it is stable outside Boundary's environment, in order to achieve the above object, the utility model is achieved by the following technical solution.
A kind of vibration temperature-controlling reaction apparatus for extracting active substance of plant, including spherical shell, round-bottomed flask and bottom Seat, the bottom of the spherical shell are connected with pedestal, the spherical shell be wrapped in the spherical bottom of round-bottomed flask and with Round-bottomed flask forms interlayer, and the spherical shell is connected with the neck part of round-bottomed flask, and the spherical shell upper is set It is equipped with filler, the lower part of the spherical shell is provided with water outlet, the spherical bottom upper end setting of the round-bottomed flask There are charge door, the spherical bottom lower end of the round-bottomed flask to be provided with drainage conduit, the charge door passes through ball with drainage conduit Shape shell is connected with the external world, and the filler, water outlet and charge door are respectively arranged with openable sealing cover, described The position that drainage conduit is connected to round-bottomed flask is provided with baffle, the baffle by the helical structure that is arranged inside drainage conduit with Knob is connected, and the drainage conduit is "u"-shaped, and the drainage conduit is provided with the connection structure that can be bent up and down, institute The chassis interior stated is provided with ultrasonic generator, and the ultrasonic generator is connected with ultrasonic horn, and ultrasonic horn setting exists In interlayer, having heaters is arranged in the chassis interior, and the heater and ultrasonic generator are connected separately with control display Device, the control display device are arranged in the outside of pedestal, and the heater and ultrasonic generator are connected separately with electricity Source, the spherical shell are heat safe clear hard resin material.
Further, the cross section of the interlayer is annular, and the difference in internal diameters of the annular is the spherical shape of round-bottomed flask The 1/2-2/3 of bottom radius.
The utility model has following row advantageous effect compared with prior art.
The present apparatus, can be by the equally distributed round bottom of the water-bath of heating by the way that spherical shaped transparent shell is arranged outside round-bottomed flask The outer wall of flask makes internal temperature uniformity on the one hand make the temperature of water-bath by the Vltrasonic device being arranged in interlayer It is more evenly distributed, the ultrasonic wave of still further aspect, generation also has the function of promoting to the extraction process in flask, makes extraction Process faster, by the way that temperature and ultrasonic frequency control device in base exterior is arranged, is precisely controlled the temperature inside reaction System, more conducively enzyme process are extracted and are effectively extracted to the substance of unstable active components in plant, without destructive enzyme or The activity of substance to be extracted, by the more mild safety of heating water bath, the cross section difference in internal diameters of interlayer annular is round-bottomed flask The 1/2-2/3 of spherical bottom radius makes the heated at constant temperature effect of water-bath reach best.The charge door and drainage conduit of setting are for adding Material and the more convenient operation of blowing process, reaction vessel and ambient temperature control device are combined into one by the present apparatus, using more It is convenient, while closed annular-heating makes the more abundant of internal reaction progress, entire environment is more stablized;The present apparatus is applicable in The substance extraction of unstable active components in plant, while the extraction process participated in suitable for active enzyme.
Description of the drawings
Fig. 1 is the cross section structure schematic diagram of utility model device.
Wherein, 1 is spherical shell, and 2 be round-bottomed flask, and 3 be pedestal, and 4 be interlayer, and 5 be filler, and 6 be water outlet, and 7 are Charge door, 8 be drainage conduit, and 9 be sealing cover, and 10 be baffle, and 11 be knob, and 12 be connection structure, and 13 be ultrasonic generator, and 14 are Ultrasonic horn, 15 heaters, 16 display devices in order to control, 17 be power supply.
Specific implementation mode
In order to make technical problem to be solved in the utility model, technical solution and advantageous effect be more clearly understood, tie Embodiment and attached drawing are closed, the present invention will be further described in detail.It should be appreciated that specific embodiment described herein It is only used to explain the utility model, is not used to limit the utility model.This is described in detail with reference to embodiment and attached drawing The technical solution of utility model, but protection domain is not limited by this.
A kind of vibration temperature-controlling reaction apparatus for extracting active substance of plant, including spherical shell 1,2 and of round-bottomed flask The bottom of pedestal 3, spherical shell 1 is connected with pedestal 3, and spherical shell 1 is wrapped in the spherical bottom of round-bottomed flask 2 and is burnt with round bottom Bottle 2 forms interlayer 4, and spherical shell 1 is connected with the neck part of round-bottomed flask 2, and 1 top of spherical shell is provided with filler 5, ball The lower part of shape shell 1 is provided with water outlet 6, and the spherical bottom upper end of round-bottomed flask 2 is provided with charge door 7, the ball of round-bottomed flask 2 Shape bottom lower end is provided with drainage conduit 8, and charge door 7 is connected by spherical shell 1 with the external world with drainage conduit 8, and filler 5 goes out The mouth of a river 6 and charge door 7 are respectively arranged with openable sealing cover 9, and the position that drainage conduit 8 is connected to round-bottomed flask 2 is provided with gear Plate 10, baffle 10 are connected by the helical structure that the inside of drainage conduit 8 is arranged with knob 11, by can be to baffle to knob 11 10 controls opened and closed, drainage conduit 8 are "u"-shaped, and drainage conduit 8 is provided with the connection structure 12 that can be bent up and down, passes through Pulling connection structure 12 can by the opening up of drainage conduit 8 or downward, and pedestal 3 is internally provided with ultrasonic generator 13, surpasses Acoustic generator 13 is connected with ultrasonic horn 14, and ultrasonic horn 14 is arranged in interlayer 4, and pedestal 3 is internally provided with heater 15, heater 15 and ultrasonic generator 13 be connected separately with control display device 16, control display device 16 is arranged in the outside of pedestal 3, heating Device 15 and ultrasonic generator 13 are connected separately with power supply 17, and spherical shell 1 is heat safe clear hard resin material, interlayer 4 Cross section be annular, annular difference in internal diameters is the 1/2 of the spherical bottom radius of round-bottomed flask 2.
Specific work process is:When being operated, retracting device will be connected on the bottleneck of round-bottomed flask, then first The nozzle of discharge gate 8 is arranged upward by pulling connection structure 12, baffle 10 is closed by the control of knob 11, then will be waited for The substance and extractant of extraction are placed in by charge door 7 in round-bottomed flask 12, and charge door 7 is closed.Water outlet 6 is closed, water is led to It crosses filler 5 to inject in interlayer 4, closes filler 5, ultrasonic generator 13 and heater are opened by controlling display device 16 15, the temperature and supersonic frequency of reservation are set, extract is treated and extracts;After extraction, closes heater 15 and surpass The nozzle of discharge gate 8 is arranged acoustic generator 13 downward by pulling connection structure 12, and baffle is opened by the control of knob 11 10, the residue after extraction is discharged;Open water outlet 6, draining.
The above content is the further descriptions done to the utility model in conjunction with specific preferred embodiment, cannot Assert that specific embodiment of the present utility model is only limitted to this, for the utility model person of an ordinary skill in the technical field For, under the premise of not departing from the utility model, several simple deduction or replace can also be made, all shall be regarded as belonging to The utility model determines scope of patent protection by the claims submitted.

Claims (2)

1. a kind of vibration temperature-controlling reaction apparatus for extracting active substance of plant, which is characterized in that including spherical shell(1), Round-bottomed flask(2)And pedestal(3), the spherical shell(1)Bottom be connected with pedestal(3), the spherical shell(1)Packet It is wrapped in round-bottomed flask(2)Spherical bottom and and round-bottomed flask(2)Form interlayer(4), the spherical shell(1)It is burnt with round bottom Bottle(2)Neck part be connected, the spherical shell(1)Top is provided with filler(5), the spherical shell(1)'s Lower part is provided with water outlet(6), the round-bottomed flask(2)Spherical bottom upper end be provided with charge door(7), the round bottom Flask(2)Spherical bottom lower end be provided with drainage conduit(8), the charge door(7)With drainage conduit(8)Pass through spherical shell (1)It is connected with the external world, the filler(5), water outlet(6)And charge door(7)It is respectively arranged with openable sealing cover (9), the drainage conduit(8)With round-bottomed flask(2)The position of connection is provided with baffle(10), the baffle(10)Pass through row Expects pipe(8)The helical structure and knob of inside setting(11)It is connected, the drainage conduit(8)For "u"-shaped, the row Expects pipe(8)It is provided with the connection structure that can be bent up and down(12), the pedestal(3)It is internally provided with ultrasonic generator(13), The ultrasonic generator(13)It is connected with ultrasonic horn(14), the ultrasonic horn(14)It is arranged in interlayer(4)Interior, described bottom Seat(3)It is internally provided with heater(15), the heater(15)And ultrasonic generator(13)It is connected separately with control display Device(16), the control display device(16)It is arranged in pedestal(3)Outside, the heater(15)Occur with ultrasound Device(13)It is connected separately with power supply(17), the spherical shell(1)For heat safe clear hard resin material.
2. a kind of vibration temperature-controlling reaction apparatus for extracting active substance of plant according to claim 1, feature exist In the interlayer(4)Cross section be annular, the difference in internal diameters of the described annular is round-bottomed flask(2)Spherical bottom radius 1/2-2/3.
CN201820372229.1U 2018-03-19 2018-03-19 A kind of vibration temperature-controlling reaction apparatus for extracting active substance of plant Active CN208081912U (en)

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CN201820372229.1U CN208081912U (en) 2018-03-19 2018-03-19 A kind of vibration temperature-controlling reaction apparatus for extracting active substance of plant

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Application Number Priority Date Filing Date Title
CN201820372229.1U CN208081912U (en) 2018-03-19 2018-03-19 A kind of vibration temperature-controlling reaction apparatus for extracting active substance of plant

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109646994A (en) * 2019-02-15 2019-04-19 南通市建设工程质量检测站有限公司 A kind of waterproof roll solubles content extraction equipment

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109646994A (en) * 2019-02-15 2019-04-19 南通市建设工程质量检测站有限公司 A kind of waterproof roll solubles content extraction equipment

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