CN208032572U - A kind of manganese chloride solution exclusion device - Google Patents
A kind of manganese chloride solution exclusion device Download PDFInfo
- Publication number
- CN208032572U CN208032572U CN201820252411.3U CN201820252411U CN208032572U CN 208032572 U CN208032572 U CN 208032572U CN 201820252411 U CN201820252411 U CN 201820252411U CN 208032572 U CN208032572 U CN 208032572U
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- China
- Prior art keywords
- settling tank
- reaction kettle
- chloride solution
- manganese chloride
- exclusion device
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Abstract
A kind of manganese chloride solution exclusion device, including reaction kettle, the side wall of the reaction kettle includes madial wall and lateral wall, and electric heating wire is equipped between madial wall and lateral wall, it is equipped with feed inlet and ammonium hydroxide feed pipe on the top of reaction kettle, agitating device is additionally provided in reaction kettle；The bottom of the reaction kettle is connect by connecting tube with settling tank, and control valve is equipped in connecting tube；It is equipped with filter device in the settling tank, constant temperature heating device is equipped in the bottom of settling tank, drain pipe is equipped in the lower part of settling tank.The utility model provides a kind of manganese chloride solution exclusion device, and the manganese chloride solution without removal of impurities is mixed with ammonium hydroxide in a kettle, heated, stirred, and the iron in solution is precipitated, is then filtered out iron by filter screen, and precipitated in settling tank.
Description
Technical field
The utility model is related to chemical technology field, more particularly to a kind of manganese chloride solution exclusion device.
Background technology
Now with the increasingly depleted of rich manganese resource, comprehensive utilization middle-low grade manganese resource just seems more and more heavier
It has been wanted that, there are a large amount of impurity, common device to go deimpurity difficulty in process of production in the production process of manganese chloride solution
Degree is big, and of high cost, step is more.
Invention content
The technical issues of the utility model is solved is to provide a kind of manganese chloride solution exclusion device, can be quickly and effectively
Remove the impurity in manganese chloride solution.
In order to solve the above technical problems, the technical solution that the utility model is taken is as follows：
A kind of manganese chloride solution exclusion device, including reaction kettle, the side wall of the reaction kettle include madial wall and lateral wall,
It is equipped with electric heating wire between madial wall and lateral wall, is equipped with feed inlet and ammonium hydroxide feed pipe on the top of reaction kettle, is reacting
Agitating device is additionally provided in kettle；The bottom of the reaction kettle is connect by connecting tube with settling tank, and control is equipped in connecting tube
Valve；It is equipped with filter device in the settling tank, is equipped with constant temperature heating device in the bottom of settling tank, is equipped in the lower part of settling tank
Drain pipe.
Preferably, it includes agitating shaft to state agitating device, and multiple agitating paddles are equipped on agitating shaft, are set at the top of reaction kettle
There are stirring motor, the output axis connection of the agitating shaft and stirring motor.
Preferably, the bottom of the reaction kettle is equipped with PH meters and thermometer.
Preferably, settling tank feed pipe is additionally provided on the settling tank, settling tank feed tube mouth is located at filter device
Lower section.
Preferably, the liquid feeding end of the drain pipe is equipped with sieve, and valve is additionally provided on drain pipe.
Preferably, the filter device be can in settling tank pull drawer-type structure, the filter device includes frame
Frame has filter screen on the inside of frame, and knob is equipped in the outside of frame.
The utility model provides a kind of manganese chloride solution exclusion device, in a kettle by the manganese chloride solution without removal of impurities
Mixed with ammonium hydroxide, heated, stirred, be precipitated solution in iron, then iron is filtered out by filter screen, and in settling tank into
Row precipitation.
Description of the drawings
FIG. 1 is a schematic structural view of the utility model；
Fig. 2 is the structural schematic diagram of the utility model filter device；
In figure：Reaction kettle 1, electric heating wire 2, feed inlet 3, ammonium hydroxide feed pipe 4, connecting tube 5, settling tank 6, filter device 7,
Control valve 8, heating device 9, drain pipe 10, agitating shaft 11, agitating paddle 12, stirring motor 13, PH meters 14, thermometer 15, precipitation
Case feed pipe 16, sieve 17, valve 18, frame 19, filter screen 20, knob 21.
Specific implementation mode
The side wall of a kind of manganese chloride solution exclusion device, including reaction kettle 1, the reaction kettle 1 includes madial wall and outside
Wall is equipped with electric heating wire 2 between madial wall and lateral wall, and feed inlet 3 and ammonium hydroxide feed pipe 4 are equipped on the top of reaction kettle 1,
It is additionally provided with agitating device in reaction kettle 1；The bottom of the reaction kettle 1 is connect by connecting tube 5 with settling tank 6, in connecting tube 5
It is equipped with control valve 8；It is equipped with filter device 7 in the settling tank 6, constant temperature heating device 9 is equipped in the bottom of settling tank 6,
The lower part of settling tank 6 is equipped with drain pipe 10.
Preferably, it includes agitating shaft 11 to state agitating device, multiple agitating paddles 12 is equipped on agitating shaft 11, in reaction kettle 1
Top be equipped with stirring motor 13, the output axis connection of the agitating shaft 11 and stirring motor 13.
Preferably, the bottom of the reaction kettle 1 is equipped with PH meters 14 and thermometer 15.For observing the acid-base value in reaction kettle
Temperature is counted, is regulated and controled convenient for staff.
Preferably, settling tank feed pipe 16 is additionally provided on the settling tank 6,16 feed inlet of settling tank feed pipe is located at filtering
The lower section of device 7.
Preferably, the liquid feeding end of the drain pipe 10 is equipped with sieve 17, and valve 18 is additionally provided on drain pipe 10.Sieve is used
In stopping the sediment in settling tank.
Preferably, the filter device 7 be can in settling tank 6 pull drawer-type structure, the filter device 7 includes
Frame 19 has filter screen 20 in 19 inside of frame, knob 21 is equipped in the outside of frame 19.Drawer-type structure is convenient for that dress will be filtered
Taking-up is set, the iron on filter screen is removed.
It is put into manganese chloride solution in use, going out from feed inlet 3, and a certain amount of manganese dioxide is added, be stirred and is added
Heat, is heated to 80-90 degree, reacts 30 minutes, then goes out ammonium hydroxide is added from ammonium hydroxide feed pipe 4, makes solution pH value to 4.0-4.5,
Continue stirring 30 minutes, is then turned on control valve 8, solution flow to settling tank 6, and iron is filtered out at filter screen 20, and solution is flow to
In settling tank.Then manganese sulfate is added into filtrate by settling tank feed pipe 16 and tentatively removes calcium ion, add ammonium fluoride
Make calcium and magnesium precipitate, is then turned on valve 18, filtrate is made to be discharged.
Embodiment described above is only the preferred embodiment of the utility model, does not therefore limit the guarantor of the utility model
Range is protected, thus it is all according to equivalence changes made by the shape of the utility model, construction and principle, the utility model should all be covered by
In protection domain.
Claims (6)
1. a kind of manganese chloride solution exclusion device, it is characterised in that：Including reaction kettle（1）, the reaction kettle（1）Side wall include
Madial wall and lateral wall are equipped with electric heating wire between madial wall and lateral wall（2）, in reaction kettle（1）Top be equipped with charging
Mouthful（3）And ammonium hydroxide feed pipe（4）, in reaction kettle（1）Inside it is additionally provided with agitating device；The reaction kettle（1）Bottom pass through connection
Pipe（5）With settling tank（6）Connection, in connecting tube（5）It is equipped with control valve（8）；The settling tank（6）It is interior to be equipped with filter device
（7）, in settling tank（6）Bottom be equipped with constant temperature heating device（9）, in settling tank（6）Lower part be equipped with drain pipe（10）.
2. a kind of manganese chloride solution exclusion device according to claim 1, it is characterised in that：The agitating device includes stirring
Axis（11）, in agitating shaft（11）It is equipped with multiple agitating paddles（12）, in reaction kettle（1）Top be equipped with stirring motor（13）, institute
State agitating shaft（11）With stirring motor（13）Output axis connection.
3. a kind of manganese chloride solution exclusion device according to claim 1, it is characterised in that：The reaction kettle（1）Bottom
It is counted equipped with PH（14）And thermometer（15）.
4. a kind of manganese chloride solution exclusion device according to claim 1, it is characterised in that：The settling tank（6）On also set
There is settling tank feed pipe（16）, settling tank feed pipe（16）Feed inlet is located at filter device（7）Lower section.
5. a kind of manganese chloride solution exclusion device according to claim 4, it is characterised in that：The drain pipe（10）Feed liquor
End is equipped with sieve（17）, in drain pipe（10）On be additionally provided with valve（18）.
6. a kind of manganese chloride solution exclusion device according to claim 1, it is characterised in that：The filter device（7）For can
In settling tank（6）The drawer-type structure of interior pull, the filter device（7）Including frame（19）, in frame（19）Inside had
Strainer（20）, in frame（19）Outside be equipped with knob（21）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820252411.3U CN208032572U (en) | 2018-02-12 | 2018-02-12 | A kind of manganese chloride solution exclusion device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820252411.3U CN208032572U (en) | 2018-02-12 | 2018-02-12 | A kind of manganese chloride solution exclusion device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208032572U true CN208032572U (en) | 2018-11-02 |
Family
ID=63953086
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820252411.3U Active CN208032572U (en) | 2018-02-12 | 2018-02-12 | A kind of manganese chloride solution exclusion device |
Country Status (1)
| Country | Link |
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| CN (1) | CN208032572U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109179794A (en) * | 2018-11-19 | 2019-01-11 | 四川中哲新材料科技有限公司 | A kind of waste water treatment process of mangano-manganic oxide |
| CN112717868A (en) * | 2020-12-11 | 2021-04-30 | 普林斯(安庆)医药科技有限公司 | 2-diethylaminoethoxyethanol production line and production method thereof |
| CN114849630A (en) * | 2022-05-10 | 2022-08-05 | 安徽广信农化股份有限公司 | Recycling device and recycling method for dimethylamine in hexazinone production process |
-
2018
- 2018-02-12 CN CN201820252411.3U patent/CN208032572U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109179794A (en) * | 2018-11-19 | 2019-01-11 | 四川中哲新材料科技有限公司 | A kind of waste water treatment process of mangano-manganic oxide |
| CN112717868A (en) * | 2020-12-11 | 2021-04-30 | 普林斯(安庆)医药科技有限公司 | 2-diethylaminoethoxyethanol production line and production method thereof |
| CN114849630A (en) * | 2022-05-10 | 2022-08-05 | 安徽广信农化股份有限公司 | Recycling device and recycling method for dimethylamine in hexazinone production process |
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