CN207941512U - A kind of Chemical Manufacture combined reaction kettle - Google Patents

A kind of Chemical Manufacture combined reaction kettle Download PDF

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Publication number
CN207941512U
CN207941512U CN201721742779.XU CN201721742779U CN207941512U CN 207941512 U CN207941512 U CN 207941512U CN 201721742779 U CN201721742779 U CN 201721742779U CN 207941512 U CN207941512 U CN 207941512U
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CN
China
Prior art keywords
reaction kettle
fixedly connected
kettle ontology
chemical manufacture
ontology
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Expired - Fee Related
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CN201721742779.XU
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Chinese (zh)
Inventor
凌春生
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JIANGSU TIANMAI CHEMICAL CO Ltd
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JIANGSU TIANMAI CHEMICAL CO Ltd
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Priority to CN201721742779.XU priority Critical patent/CN207941512U/en
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Publication of CN207941512U publication Critical patent/CN207941512U/en
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Abstract

The utility model is related to chemical equipment technical fields, and disclose a kind of Chemical Manufacture combined reaction kettle, including reaction kettle ontology, the bottom end of the reaction kettle ontology is fixedly connected with pedestal, the bottom end of the reaction kettle ontology is fixedly connected with discharge nozzle, the top of the reaction kettle ontology is fixedly connected with stirring motor, the output end of the stirring motor is fixedly connected with agitating shaft, the surface of the agitating shaft is fixedly connected sequentially from top to bottom horizontal paddle, Stirring leaf and choked flow blade, and the surface of the choked flow blade offers vent.Chemical Manufacture combined reaction kettle, by the way that electric rotating machine, rotary shaft, gravitometer measuring device and isolation board is arranged, by the drive Shaft of electric rotating machine to solid reaction material blend that prevent charging from cohering blocking in solid reaction material, fixed reaction material is on isolation board, gravitometer measuring device weighs solid reaction material, so that feedstock quality is accurate, so that it is guaranteed that the accuracy of additive.

Description

A kind of Chemical Manufacture combined reaction kettle
Technical field
The utility model is related to chemical equipment technical field, specially a kind of Chemical Manufacture combined reaction kettle.
Background technology
Generally reaction mass from feed inlet enter reaction kettle it is agitated, reaction after, discharge port of the material from reaction kettle Discharge, during discharging, due to the intrinsic construction of reaction kettle itself, agitated material drastically falls under the effect of gravity Aggregation to material outlet, often there is discharge port solid accumulation, cause to discharge it is unsmooth, production efficiency decline, or even under the influence of one Process is normally carried out, and present reaction kettle is monolithic construction, and a reaction kettle is generally only used for a kind of production of product, And the heating device being arranged in General reactions kettle is in reactor bottom, it is difficult to which suitable for being evenly heated for high request, and some are changed It learns raw material and be easy to cause that local concentration is excessively high, and General reactions kettle tissue exhaust gas is directly discharged in air when entering reaction kettle, Pernicious gas may be contained, endanger the safety of staff.
Utility model content
(One)The technical issues of solution
In view of the deficiencies of the prior art, the utility model provides a kind of Chemical Manufacture combined reaction kettle, has synthesis The advantages that reaction and exhaust-gas treatment, solve the problems, such as that existing reaction kettle reactive material is single.
(Two)Technical solution
To realize that the purpose of above-mentioned combined reaction and exhaust-gas treatment, the utility model provide the following technical solutions:A kind ofization Work production uses combined reaction kettle, including reaction kettle ontology, the bottom end of the reaction kettle ontology to be fixedly connected with pedestal, the reaction The bottom end of kettle ontology is fixedly connected with discharge nozzle, and the top of the reaction kettle ontology is fixedly connected with stirring motor, the stirring The output end of motor is fixedly connected with agitating shaft, and the surface of the agitating shaft is fixedly connected sequentially has horizontal stirring from top to bottom The surface of leaf, Stirring leaf and choked flow blade, the choked flow blade offers vent, and the inside of the reaction kettle ontology is solid Dingan County is equipped with heater, and the both sides of the reaction kettle ontology are both provided with condenser pipe, and the top of the reaction kettle ontology is provided with One end of feeding-in solid body pipe, the feeding-in solid body pipe is provided with electric rotating machine, and the output end of the electric rotating machine is fixedly connected with Rotary shaft is fixedly connected with gravitometer measuring device below the electric rotating machine, and the side of the gravitometer measuring device is provided with isolation The inside of plate, the reaction kettle ontology is fixedly connected with drip tray, and one end of the drip tray is fixedly connected with minim pipette, described The other end of drip tray is fixedly connected with feed liquor funnel, and the feed liquor funnel is internally provided with graduation mark, the reaction kettle sheet The top of body is provided with exhaust pipe, and one end of the exhaust pipe and reaction kettle ontology interface is provided with dehumidifier, the exhaust pipe One end be fixedly connected with suction ventilator, the air outlet of the suction ventilator is extended to by exhaust pipe to be neutralized inside liquid case.
Preferably, the surface of the discharge nozzle, feeding-in solid body pipe, feed liquor funnel and exhaust pipe is both provided with check valve.
Preferably, it is provided with corrosion-inhibiting coating on the inner wall of the reaction kettle ontology, and the inner wall of reaction kettle ontology is filled with Thermal insulation material.
Preferably, the surface of the rotary shaft is fixedly connected with pivoting leaf, and pivoting leaf is zigzag.
Preferably, one end of the condenser pipe is connected with water tank, and the other end of the condenser pipe is connected to instead by valve Answer the top of kettle ontology.
Preferably, the bottom end side of the reaction kettle ontology is provided with temperature sensor.
(Three)Advantageous effect
Compared with prior art, the utility model provides a kind of Chemical Manufacture combined reaction kettle, has following beneficial Effect:
1, Chemical Manufacture combined reaction kettle, by the way that electric rotating machine, rotary shaft, gravitometer measuring device and isolation board is arranged, By the drive Shaft of electric rotating machine to solid reaction material blend that prevent charging from cohering blocking in solid reaction material, Gu Reaction material is determined on isolation board, gravitometer measuring device weighs solid reaction material so that feedstock quality is accurate, so that it is guaranteed that adding The accuracy of charging.
2, Chemical Manufacture combined reaction kettle, by the way that drip tray, minim pipette, feed liquor funnel and graduation mark, liquid is arranged The minim pipette that drip tray bottom end is passed into from loading hopper is added liquid reactions material to reaction kettle body interior, prevents liquid Precursor reactant material is directly entered reaction kettle ontology hot-spot and causes reaction incomplete, and there are some potential safety problems, scales Line can refer to the volume of addition reaction solution, it is ensured that the accuracy of reaction, to achieve the purpose that concentrated expression.
3, Chemical Manufacture combined reaction kettle is being passed through by the way that exhaust pipe, dehumidifier, suction ventilator is arranged and neutralizes liquid case After crossing reaction kettle bulk reaction, the gas of generation through exhaust pipe by under the action of suction ventilator, being discharged, dehumidifier can be to containing heat The gas of amount dehumidifies, and so that the water droplet to be formed is entered in reaction kettle ontology when reaching certain humidity, gas enters neutralization Liquid case is discharged after neutralizing, to prevent gas from containing noxious material, to achieve the purpose that safety dumping exhaust gas.
Description of the drawings
FIG. 1 is a schematic structural view of the utility model;
Fig. 2 is partial structurtes enlarged diagram at A in the utility model Fig. 1.
In figure:1 reaction kettle ontology, 2 pedestals, 3 discharge nozzles, 4 stirring motors, 5 agitating shafts, 6 horizontal paddles, 7 rotations are stirred Mix leaf, 8 choked flow blades, 9 vents, 10 heaters, 11 condenser pipes, 12 feeding-in solid body pipes, 13 electric rotating machines, 14 rotary shafts, 15 Gravitometer measuring device, 16 isolation boards, 17 drip trays, 18 minim pipettes, 19 feed liquor funnels, 20 graduation marks, 21 exhaust pipes, 22 dehumidifiers, In 23 suction ventilators, 24 and liquid case, 25 temperature sensors.
Specific implementation mode
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work The every other embodiment obtained, shall fall within the protection scope of the present invention.
Please refer to Fig.1-2, a kind of Chemical Manufacture combined reaction kettle, including reaction kettle ontology 1, the bottom of reaction kettle ontology 1 End is fixedly connected with pedestal 2, corrosion-inhibiting coating is provided on the inner wall of reaction kettle ontology 1, and the inner wall of reaction kettle ontology 1 is filled with The bottom end of thermal insulation material, reaction kettle ontology 1 is fixedly connected with discharge nozzle 3, and the top of reaction kettle ontology 1 is fixedly connected with stirring electricity The output end of machine 4, stirring motor 4 is fixedly connected with agitating shaft 5, and the surface of agitating shaft 5 is fixedly connected sequentially has water from top to bottom The surface of flat paddle 6, Stirring leaf 7 and choked flow blade 8, choked flow blade 8 offers vent 9, is opened up on choked flow blade 8 There is vent 9, in view of the load-bearing capacity of choked flow blade 8 while choked flow, therefore opens up the decompression that diameter is more than material diameter Hole 9 can allow small part material to pass through out of hole, achieve the purpose that choked flow blade 8, the inside of reaction kettle ontology 1 is protected to fix peace Equipped with heater 10, the both sides of reaction kettle ontology 1 are both provided with condenser pipe 11, and one end of condenser pipe 11 is connected with water tank, condensation The other end of pipe 11 is connected to the top of reaction kettle ontology 1 by valve, and there are two valves, controls water circulation and leads to reaction In kettle, the top of reaction kettle ontology 1 is provided with feeding-in solid body pipe 12, and one end of feeding-in solid body pipe 12 is provided with electric rotating machine 13, The output end of electric rotating machine 13 is fixedly connected with rotary shaft 14, and the surface of rotary shaft 14 is fixedly connected with pivoting leaf, and pivoting leaf Lower section for zigzag, electric rotating machine 13 is fixedly connected with gravitometer measuring device 15, and the side of gravitometer measuring device 15 is provided with isolation Plate 16 passes through rotation by the way that electric rotating machine 13, rotary shaft 14, gravitometer measuring device 15 and isolation board 16 is arranged in solid reaction material The drive Shaft 14 of motor 13 to solid reaction material blend that prevent charging from cohering blocking, and fixed reaction material is in isolation board On 16, gravitometer measuring device 15 weighs solid reaction material so that feedstock quality is accurate, so that it is guaranteed that additive is accurate Property, the inside of reaction kettle ontology 1 are fixedly connected with drip tray 17, and one end of drip tray 17 is fixedly connected with minim pipette 18, dropping liquid The other end of disk 17 is fixedly connected with feed liquor funnel 19, and feed liquor funnel 19 is internally provided with graduation mark 20, by the way that dropping liquid is arranged Disk 17, minim pipette 18, feed liquor funnel 19 and graduation mark 20, liquid pass into the dropping liquid of 17 bottom end of drip tray from loading hopper 19 Pipe 18 prevents liquid reactions material to be directly entered 1 part of reaction kettle ontology to being added liquid reactions material inside reaction kettle ontology 1 It overheats and causes reaction incomplete, and there are some potential safety problems, graduation mark 20 can refer to the volume of addition reaction solution, it is ensured that The accuracy of reaction, to achieve the purpose that concentrated expression, the top of reaction kettle ontology 1 is provided with exhaust pipe 21, discharge nozzle 3, The surface of feeding-in solid body pipe 12, feed liquor funnel 19 and exhaust pipe 21 is both provided with check valve, and exhaust pipe 21 connects with reaction kettle ontology 1 One end of mouth is provided with dehumidifier 22, and one end of exhaust pipe 21 is fixedly connected with suction ventilator 23, and the air outlet of suction ventilator 23 passes through Exhaust pipe 21, which extends to, to be neutralized inside liquid case 24, by the way that exhaust pipe 21, dehumidifier 22, suction ventilator 23 is arranged and neutralizes liquid case 24, After the reaction of reaction kettle ontology 1, the gas of generation through exhaust pipe 21 by under the action of suction ventilator 23, being discharged, dehumidifier 22 can dehumidify to the gas containing heat, so that the water droplet to be formed is entered in reaction kettle ontology 1 when reaching certain humidity, gas Body is entered to neutralize after liquid case 24 neutralizes and be discharged, to prevent gas from containing noxious material, to reach the mesh of safety dumping exhaust gas , the bottom end side of reaction kettle ontology 1 is provided with temperature sensor 25.
The electric elements occurred in this article are electrically connected with extraneous main controller and 220V alternating currents, and main controller can be meter Calculation machine etc. plays the conventionally known equipment of control.
When in use, solid reaction material is stirred it crushing, liquid by the rotary shaft 14 that electric rotating machine 13 drives Reaction material passes into drip tray 17 and minim pipette 18 to being added reaction solution inside reaction kettle ontology 1 from feed liquor funnel 19, By the rotation of stirring motor 4, the horizontal paddle 6 of 5 drive of agitating shaft, Stirring leaf 7 and choked flow blade 8 is set to rotate, then Temperature sensor 25 incudes temperature in reaction kettle ontology 1, when the temperature is low, is heated by heater 10, when When reaction temperature is higher, cooled down to it by condenser pipe 11, is stopped when until reaching reaction optimum temperature, after reaction High-temperature reacting gas, under the action of suction ventilator 23, by exhaust pipe 21 to neutralize liquid case 24 after be discharged, in reaction process Check valve be completely in closed state, after reaction reaction material by discharge nozzle 3 be discharged, then the condensed water in condenser pipe 11 can With to being cleaned inside reaction kettle ontology 1.
In conclusion Chemical Manufacture combined reaction kettle, by the way that electric rotating machine 13, rotary shaft 14, gravimetric is arranged Device 15 and isolation board 16 blend solid reaction material by the drive Shaft 14 of electric rotating machine 13 in solid reaction material Prevent charging from cohering blocking, for fixed reaction material on isolation board 16, gravitometer measuring device 15 weighs solid reaction material so that Feedstock quality is accurate, so that it is guaranteed that the accuracy of additive, by the way that drip tray 17, minim pipette 18, feed liquor funnel 19 is arranged and carves Line 20 is spent, liquid passes into the minim pipette 18 of 17 bottom end of drip tray to adding inside reaction kettle ontology 1 from loading hopper 19 Liquid feeding precursor reactant material prevents liquid reactions material to be directly entered 1 hot-spot of reaction kettle ontology and causes reaction incomplete, and exists Some potential safety problems, graduation mark 20 can refer to the volume of addition reaction solution, it is ensured that the accuracy of reaction, it is comprehensive anti-to reach The purpose reflected is reacted by the way that exhaust pipe 21, dehumidifier 22, suction ventilator 23 is arranged and neutralizes liquid case 24 by reaction kettle ontology 1 Afterwards, the gas of generation is through exhaust pipe 21 by under the action of suction ventilator 23, being discharged, dehumidifier 22 can to the gas containing heat into Row dehumidifying, makes the water droplet to be formed enter in reaction kettle ontology 1 when reaching certain humidity, and gas, which enters, neutralizes the neutralization of liquid case 24 After discharge, to prevent gas from containing noxious material, to achieve the purpose that safety dumping exhaust gas.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art, It is appreciated that can these embodiments be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaiied Change, replace and modification, the scope of the utility model are defined by the appended claims and the equivalents thereof.

Claims (6)

1. a kind of Chemical Manufacture combined reaction kettle, including reaction kettle ontology(1), it is characterised in that:The reaction kettle ontology(1) Bottom end be fixedly connected with pedestal(2), the reaction kettle ontology(1)Bottom end be fixedly connected with discharge nozzle(3), the reaction kettle Ontology(1)Top be fixedly connected with stirring motor(4), the stirring motor(4)Output end be fixedly connected with agitating shaft (5), the agitating shaft(5)Surface be fixedly connected sequentially have horizontal paddle from top to bottom(6), Stirring leaf(7)And resistance Flow blade(8), the choked flow blade(8)Surface offer vent(9), the reaction kettle ontology(1)Inside fix peace Equipped with heater(10), the reaction kettle ontology(1)Both sides be both provided with condenser pipe(11), the reaction kettle ontology(1)'s Top is provided with feeding-in solid body pipe(12), the feeding-in solid body pipe(12)One end be provided with electric rotating machine(13), the rotation Motor(13)Output end be fixedly connected with rotary shaft(14), the electric rotating machine(13)Lower section be fixedly connected with gravimetric Device(15), the gravitometer measuring device(15)Side be provided with isolation board(16), the reaction kettle ontology(1)Inside fix connect It is connected to drip tray(17), the drip tray(17)One end be fixedly connected with minim pipette(18), the drip tray(17)It is another End is fixedly connected with feed liquor funnel(19), the feed liquor funnel(19)Be internally provided with graduation mark(20), the reaction kettle sheet Body(1)Top be provided with exhaust pipe(21), the exhaust pipe(21)With reaction kettle ontology(1)One end of interface is provided with dehumidifying Device(22), the exhaust pipe(21)One end be fixedly connected with suction ventilator(23), the suction ventilator(23)Air outlet pass through row Tracheae(21)Extend to neutralization liquid case(24)It is internal.
2. a kind of Chemical Manufacture combined reaction kettle according to claim 1, it is characterised in that:The discharge nozzle(3), it is solid Body feed pipe(12), feed liquor funnel(19)And exhaust pipe(21)Surface be both provided with check valve.
3. a kind of Chemical Manufacture combined reaction kettle according to claim 1, it is characterised in that:The reaction kettle ontology (1)Inner wall on be provided with corrosion-inhibiting coating, and reaction kettle ontology(1)Inner wall be filled with thermal insulation material.
4. a kind of Chemical Manufacture combined reaction kettle according to claim 1, it is characterised in that:The rotary shaft(14)'s Surface is fixedly connected with pivoting leaf, and pivoting leaf is zigzag.
5. a kind of Chemical Manufacture combined reaction kettle according to claim 1, it is characterised in that:The condenser pipe(11)'s One end is connected with water tank, the condenser pipe(11)The other end reaction kettle ontology is connected to by valve(1)Top.
6. a kind of Chemical Manufacture combined reaction kettle according to claim 1, it is characterised in that:The reaction kettle ontology (1)Bottom end side be provided with temperature sensor(25).
CN201721742779.XU 2017-12-14 2017-12-14 A kind of Chemical Manufacture combined reaction kettle Expired - Fee Related CN207941512U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721742779.XU CN207941512U (en) 2017-12-14 2017-12-14 A kind of Chemical Manufacture combined reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721742779.XU CN207941512U (en) 2017-12-14 2017-12-14 A kind of Chemical Manufacture combined reaction kettle

Publications (1)

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CN207941512U true CN207941512U (en) 2018-10-09

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110002635A (en) * 2019-04-30 2019-07-12 宁波渤川废液处置有限公司 Waste alkali liquor treatment device
CN110252229A (en) * 2019-05-31 2019-09-20 陈小勇 A kind of chemical production equipment reaction kettle

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110002635A (en) * 2019-04-30 2019-07-12 宁波渤川废液处置有限公司 Waste alkali liquor treatment device
CN110252229A (en) * 2019-05-31 2019-09-20 陈小勇 A kind of chemical production equipment reaction kettle

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20181009

Termination date: 20201214

CF01 Termination of patent right due to non-payment of annual fee