CN207918717U - Ammonification production of sulfur-based compound fertilizer equipment based on Klorvess Liquid - Google Patents
Ammonification production of sulfur-based compound fertilizer equipment based on Klorvess Liquid Download PDFInfo
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- CN207918717U CN207918717U CN201820203961.6U CN201820203961U CN207918717U CN 207918717 U CN207918717 U CN 207918717U CN 201820203961 U CN201820203961 U CN 201820203961U CN 207918717 U CN207918717 U CN 207918717U
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- potassium chloride
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Abstract
The utility model discloses a kind of ammonification production of sulfur-based compound fertilizer equipment based on Klorvess Liquid, including sequentially connected potassium acid sulfate reactive tank, mix acid tank, tubular reactor and comminutor, the potassium chloride entrance of the potassium acid sulfate reactive tank is connect with the outlet of potassium chloride fluid bowl, the potassium chloride powdering inlet of the potassium chloride fluid bowl is connected with potassium chloride powder and deposits tank, the Klorvess Liquid outlet of the potassium chloride fluid bowl is connect with the potassium chloride entrance of potassium acid sulfate reactive tank flow tube A in terms of, flowmeter A1 is installed on meter flow tube A, control valve A2, the sulfuric acid entrance of the potassium acid sulfate reactive tank and the sulfuric acid of sulphuric acid tank export the flow tube B connections in terms of, flowmeter B1 is installed on meter flow tube B, control valve B2.Advantageous effect：Potassium chloride powder is set to be dissolved as after Klorvess Liquid again with sulfuric acid reaction, the Klorvess Liquid and sulfuric acid solution homomorphosis of liquid are more easy to calculate proportioning and reaction, greatly improve the quantization work of reaction, and reduce control cost.
Description
Technical field
The utility model is related to production of sulfur-based compound fertilizer equipment technical fields, specifically, are related to being based on Klorvess Liquid
Ammonification production of sulfur-based compound fertilizer equipment.
Background technology
Industrial production sulfenyl fertilizer is to be granulated after the nitration mixture ammonification by potassium acid sulfate to obtain nitrogen, phosphorus, K composite fertilizer, wherein sulphur
Potassium hydrogen phthalate is that potassium chloride and sulfuric acid reaction obtain, and the proportioning of sulfuric acid and potassium chloride need to be kept in a certain range, otherwise raw material
It will slattern, and generate the amount also difficult calculating acquisition of potassium acid sulfate, precise quantification can not achieve to follow-up industrial production and throw
Enter and output.
The prior art is that addition potassium chloride powder and sulfuric acid solution are reacted, and by weighing, potassium chloride powder calculates reaction
The additive amount of material, but the sulfuric acid of the potassium chloride powder of solid and liquid calculates to match and needs multiple conversion, in operation very not
Just.
The shortcomings that prior art：Addition potassium chloride powder is not easy to calculate the ratio of reactive material, keeps raw material availability low,
And subsequent production will spend more cost control reactant ratios.
Utility model content
The purpose of this utility model is to provide a kind of ammonification production of sulfur-based compound fertilizer equipment based on Klorvess Liquid, makes chlorine
Change potassium powder be dissolved as after Klorvess Liquid again with sulfuric acid reaction, the Klorvess Liquid and sulfuric acid solution homomorphosis of liquid, more
Proportioning and reaction are easily calculated, greatly improves the quantization work of reaction, and reduce control cost.
In order to achieve the above objectives, the specific technical solution that the utility model uses is as follows：
A kind of ammonification production of sulfur-based compound fertilizer equipment based on Klorvess Liquid, including the reaction of sequentially connected potassium acid sulfate
Slot, mixing acid tank, tubular reactor and comminutor, the potassium chloride entrance of the potassium acid sulfate reactive tank and going out for potassium chloride fluid bowl
Mouth connection, the potassium chloride powdering inlet of the potassium chloride fluid bowl are connected with potassium chloride powder and deposit tank, and the potassium chloride fluid bowl is additionally provided with
Water inlet；
The Klorvess Liquid outlet of the potassium chloride fluid bowl and potassium chloride entrance flow tube A in terms of of potassium acid sulfate reactive tank connect
It connects, flowmeter A1, control valve A2 is installed on meter flow tube A；
The sulfuric acid entrance of the potassium acid sulfate reactive tank and the sulfuric acid of sulphuric acid tank export the flow tube B connections in terms of, meter flow tube B
On flowmeter B1, control valve B2 are installed.
By above-mentioned design, powdered potassium chloride enters potassium chloride fluid bowl and is dissolved into Klorvess Liquid, then inputs sulfuric acid
Hydrogen potassium reaction is reacted with sulfuric acid, and is counted flow tube A and counted flow tube B and be both provided with flowmeter and control valve, and the defeated of solution is made
Enter to measure and intuitively show and control, the input of potassium chloride and sulfuric acid, which is equipped with, is easier calculating and control, facilitates product
The quantization of potassium acid sulfate saves the time cost and production cost calculated again to the addition of subsequent raw material.
It further describing, the flowmeter A1 and control valve A2 is to be installed successively according to solution flow direction in meter flow tube A,
The flowmeter B1 and control valve B2 is to be installed successively according to solution flow direction in meter flow tube B；
The control valve A2 and control valve B2 is connected separately with the control terminal group of controller, the signal end component of the controller
It Lian Jie not flowmeter A1, flowmeter B1.
By above-mentioned design, the additive amount of potassium chloride and sulfuric acid can also carry out automatic measurement ＆ calculation addition, control by controller
Device processed need to only pre-set the adding proportion of the two, then by the input quantity of real-time detection stream gauge A1 and flowmeter B1 to control
Valve A2, control valve B2 controls open or close, it is ensured that the input quantity of potassium chloride and sulfuric acid realizes industry within the scope of adding proportion
Production automation reduces cost of labor.
It is further described, at least two tubular reactor is set side by side between mixing acid tank and the comminutor, increase
The quantum of output of fertilizer.
It is further described, the potassium acid sulfate reactive tank is provided with the jet chimney of coiled coil groove body outer wall N circles.
By above-mentioned design, jet chimney heats potassium acid sulfate reactive tank after being passed through high-temperature steam and is controlled suitable
It within the temperature range of preferably reacting, and is added, then reacts more purely, and product will not be contaminated without extra substance in reactive tank
And dilution, proportioning is calculated convenient for the subsequent reactions of potassium acid sulfate, collection hydrogen chloride is also allowed for and carries out accurate hydrochloric acid making.
It is further described, the hydrogen chloride outlet of the potassium acid sulfate reactive tank connects the HCl of hydrochloric acid spray column through pipeline
Entrance；
It is additionally provided with spraying entrance on hydrochloric acid spray column, the steam (vapor) outlet of the spraying entrance and jet chimney connects through pipeline
It connects.
The existing hydrochloric acid spray column for collecting hydrogen chloride is equipped with waterjet inlet, but steam is underused, and cold water absorbs
The efficiency of hydrogen chloride is relatively low, and by above-mentioned design, the steam in jet chimney declines for reactive tank temperature after heating, forms mist
The steam of change, then these misty steam are passed through hydrochloric acid spray column, atomized steam mixes the water that waterjet inlet enters and forms water mist
Admixture absorbing hydrogen chloride, the state of water mist mixing are more easy to absorbing hydrogen chloride and form hydrochloric acid solution, meanwhile, steam recycling
Reduce cost.
Be further described, the steam inlet of the jet chimney in upper, steam (vapor) outlet under, steam flow direction be from
Top to bottm convoluted flow.
It can liquefy after exporting heat due to steam, then by above-mentioned design, liquefied condensed water will not be flowed out along input port,
But spiral flow to pipe outlet downwards, facilitate the collection of condensed water.
As the optimum temperature of reaction, temperature range is 125 DEG C -135 DEG C in the slot of the potassium acid sulfate reactive tank.
It is further described, the spraying entrance of the hydrochloric acid spray column is arranged in hydrochloric acid spray column top position.
The beneficial effects of the utility model：Powdered potassium chloride enters potassium chloride fluid bowl and is dissolved into Klorvess Liquid, makes
The input quantity of solution intuitively shown and controlled, and the input of potassium chloride and sulfuric acid, which is equipped with, to be easier to calculate and control, convenient
The quantization of product potassium acid sulfate saves the time cost and production cost calculated again to the addition of subsequent raw material；Also
Automated control operation can be carried out connection controller to the input quantity of potassium chloride and sulfuric acid in meter flow tube；Potassium acid sulfate reactive tank
It is not re-introduced into new substance in addition to reactive material, ensures the accurate of reaction, and product will not be contaminated, will not be diluted,
Whole industrial production quantity can be more preferably controlled to calculate and match；Dilute hydrochloric acid is can be used for after steam heating, reduces production
Cost.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model
Specific implementation mode
Below in conjunction with the accompanying drawings and specific embodiment is described in further detail the utility model：
As shown in Figure 1, a kind of ammonification production of sulfur-based compound fertilizer equipment based on Klorvess Liquid, including sequentially connected sulphur
Potassium hydrogen phthalate reactive tank 1, mixing acid tank 2, tubular reactor 3 and comminutor, wherein the potassium chloride of the potassium acid sulfate reactive tank 1
Entrance 1a is connect with the outlet of potassium chloride fluid bowl 6, and the potassium chloride powdering inlet of the potassium chloride fluid bowl 6 is connected with potassium chloride powder and deposits
Tank 5, the potassium chloride fluid bowl 6 are additionally provided with water inlet；
The Klorvess Liquid outlet of the potassium chloride fluid bowl 6 and the potassium chloride entrance 1a of potassium acid sulfate reactive tank 1 flow in terms of
Pipe A connections are equipped with flowmeter A1 on meter flow tube A, control valve A2, the flowmeter A1 and control valve A2 are according to meter flow tube
Solution flow direction is installed successively in A；
The sulfuric acid entrance 1b of the potassium acid sulfate reactive tank 1 is connect with the sulfuric acid of sulphuric acid tank 7 outlet flow tube B in terms of, the meter
Flowmeter B1 is installed, control valve B2, the flowmeter B1 and control valve B2 are to be flowed according to solution in meter flow tube B on flow tube B
It installs successively in direction.
Preferably, control valve A2 described in the present embodiment and control valve B2 are connected separately with the control terminal group of controller,
Signal end group difference connection flow gauge A1, the flowmeter B1 of the controller.
It is set side by side with 2 tubular reactors 3 preferably, being mixed described in the present embodiment between acid tank 2 and comminutor.
Preferably, the potassium acid sulfate reactive tank 1 is provided with the jet chimney 11 of coiled coil groove body outer wall N circles, described
HCl entrance of the hydrogen chloride outlet of potassium acid sulfate reactive tank 1 through pipeline connection hydrochloric acid spray column 4；
It is additionally provided with spraying entrance on hydrochloric acid spray column 4, the steam (vapor) outlet of the spraying entrance and jet chimney 11 is through pipe
Road connects.
Preferably, the steam inlet of jet chimney 11 described in the present embodiment in upper, steam (vapor) outlet under, steam flowing
Direction is convoluted flow from top to bottom.
Temperature range is 125 DEG C -135 DEG C in the slot of the potassium acid sulfate reactive tank 1.
Preferably, the spraying entrance and waterjet inlet of hydrochloric acid spray column described in the present embodiment 4 are arranged at hydrochloric acid spray
Drench 4 top position of tower.
The operation principle of the utility model：
Potassium chloride powder, which is deposited the potassium chloride powder in tank 5 and is added in potassium chloride fluid bowl 6, to be dissolved, dissolved Klorvess Liquid
It is added in potassium acid sulfate reactive tank 1 by controller control with the sulfuric acid in sulphuric acid tank 7, jet chimney 11 is passed through high-temperature steam pair
Potassium acid sulfate reactive tank 1 is heated to 125 DEG C -135 DEG C, then potassium chloride generates potassium acid sulfate and hydrogen chloride, sulfuric acid with sulfuric acid reaction
Hydrogen potassium enters mixing acid tank 2 and dust technology and is mixed into nitration mixture, and nitration mixture is passed through 3 aminating reaction of tubular reactor, and to obtain sulfenyl compound
Fertilizer finally obtains the fertilizer of solid granular in comminutor；
The byproduct hydrogen chloride that potassium acid sulfate reactive tank 1 generates enters hydrochloric acid spray column 4, the steaming of jet chimney 11 through pipeline
Vapour forms misty vapour and is passed through hydrochloric acid spray column 4 after also reducing phlegm and internal heat, the steam of water mist mixing dissolves to obtain dilute hydrochloric acid with hydrogen chloride.
Claims (8)
1. a kind of ammonification production of sulfur-based compound fertilizer equipment based on Klorvess Liquid, including sequentially connected potassium acid sulfate reactive tank
(1), mixing acid tank (2), tubular reactor (3) and comminutor, it is characterised in that：The chlorination of the potassium acid sulfate reactive tank (1)
Potassium entrance (1a) is connect with the outlet of potassium chloride fluid bowl (6), and the potassium chloride powdering inlet of the potassium chloride fluid bowl (6) is connected with chlorination
Potassium powder deposits tank (5), and the potassium chloride fluid bowl (6) is additionally provided with water inlet；
The Klorvess Liquid outlet of the potassium chloride fluid bowl (6) is with the potassium chloride entrance (1a) of potassium acid sulfate reactive tank (1) in terms of
Flow tube A connections are equipped with flowmeter A1, control valve A2 on meter flow tube A；
The sulfuric acid entrance (1b) of the potassium acid sulfate reactive tank (1) is connect with the sulfuric acid of sulphuric acid tank (7) outlet flow tube B in terms of, should
Flowmeter B1, control valve B2 are installed on meter flow tube B.
2. the ammonification production of sulfur-based compound fertilizer equipment according to claim 1 based on Klorvess Liquid, it is characterised in that：Institute
It is to be installed successively according to solution flow direction in meter flow tube A to state flowmeter A1 and control valve A2, the flowmeter B1 and control valve
B2 is to be installed successively according to solution flow direction in meter flow tube B；
The control valve A2 and control valve B2 is connected separately with the control terminal group of controller, and the signal end group of the controller connects respectively
Meet flowmeter A1, flowmeter B1.
3. the ammonification production of sulfur-based compound fertilizer equipment according to claim 1 based on Klorvess Liquid, it is characterised in that：Institute
It states mixing acid tank (2) and is set side by side at least two tubular reactor (3) between comminutor.
4. the ammonification production of sulfur-based compound fertilizer equipment according to claim 1 based on Klorvess Liquid, it is characterised in that：Institute
State the jet chimney (11) that potassium acid sulfate reactive tank (1) is provided with coiled coil groove body outer wall N circles.
5. the ammonification production of sulfur-based compound fertilizer equipment according to claim 4 based on Klorvess Liquid, it is characterised in that：Institute
State HCl entrance of the hydrogen chloride outlet through pipeline connection hydrochloric acid spray column (4) of potassium acid sulfate reactive tank (1)；
It is additionally provided with spraying entrance on hydrochloric acid spray column (4), the steam (vapor) outlet of the spraying entrance and jet chimney (11) is through pipe
Road connects.
6. the ammonification production of sulfur-based compound fertilizer equipment according to claim 4 based on Klorvess Liquid, it is characterised in that：Institute
The steam inlet of jet chimney (11) is stated in upper, steam (vapor) outlet under, steam flow direction is convoluted flow from top to bottom.
7. the ammonification production of sulfur-based compound fertilizer equipment according to claim 1 based on Klorvess Liquid, it is characterised in that：Institute
It is 125 DEG C -135 DEG C to state temperature range in the slot of potassium acid sulfate reactive tank (1).
8. the ammonification production of sulfur-based compound fertilizer equipment according to claim 5 based on Klorvess Liquid, it is characterised in that：Institute
The spraying entrance for stating hydrochloric acid spray column (4) is arranged in hydrochloric acid spray column (4) top position.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820203961.6U CN207918717U (en) | 2018-02-06 | 2018-02-06 | Ammonification production of sulfur-based compound fertilizer equipment based on Klorvess Liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820203961.6U CN207918717U (en) | 2018-02-06 | 2018-02-06 | Ammonification production of sulfur-based compound fertilizer equipment based on Klorvess Liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207918717U true CN207918717U (en) | 2018-09-28 |
Family
ID=63603363
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820203961.6U Active CN207918717U (en) | 2018-02-06 | 2018-02-06 | Ammonification production of sulfur-based compound fertilizer equipment based on Klorvess Liquid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207918717U (en) |
-
2018
- 2018-02-06 CN CN201820203961.6U patent/CN207918717U/en active Active
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