CN207816632U - A kind of liquid closed sampler containing solid particle - Google Patents

A kind of liquid closed sampler containing solid particle Download PDF

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Publication number
CN207816632U
CN207816632U CN201820117611.8U CN201820117611U CN207816632U CN 207816632 U CN207816632 U CN 207816632U CN 201820117611 U CN201820117611 U CN 201820117611U CN 207816632 U CN207816632 U CN 207816632U
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China
Prior art keywords
valve
surge flask
sampling
bottle
solid particle
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Application number
CN201820117611.8U
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Chinese (zh)
Inventor
安军林
曹岩德
陈兆峰
王海礼
魏东亮
李伟珍
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Asia Silicon Qinghai Co Ltd
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Asia Silicon Qinghai Co Ltd
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Priority to CN201820117611.8U priority Critical patent/CN207816632U/en
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Abstract

The utility model discloses a kind of liquid closed sampler containing solid particle, includes sampling bottle, surge flask and absorption bottle, and surge flask is connect with material pipeline, and valve is equipped with before entering surge flask;The sampling bottle is connect with surge flask, and connecting pipeline between the two is equipped with valve, and the absorption bottle is connected between this valve and surge flask, and another valve is equipped with before entering absorption bottle;The surge flask is also associated with nitrogen blowing mechanism.The utility model is to be directed to highly pressurised liquid material, and in material solid content in 10% (w%) sampler below, by installing a surge flask, one reduces pressure, two to avoid valve from failure occur when taking high-pressure material to be directed to dangerous, thus the utility model has many advantages, such as closed, time-consuming environment short, clean, safe, not easy to pollute, and can intuitively observe material liquid level in surge tank, clean and maintenance easy to disassemble.

Description

A kind of liquid closed sampler containing solid particle
Technical field
The utility model is related to chemical industry sampling equipment technical fields, and in particular to a kind of to be taken for the liquid with solid particle Sampling device.
Background technology
In chemical process, it can determine whether product is qualified, and whether chemical plant installations operates steadily by sampling analysis, And according to the timely adjusting process parameter of analysis result, the safe and stable operation of ensuring equipment, therefore there is very high want to sampler It asks.For chemical plant installations sampler, be critical to consider how it is timely, accurate, conveniently, safely get representative sample Product.Sampler has a unenclosed construction and closed structure at present, and open type is only applicable to nontoxic material, closed Suitable for poisonous and harmful or inflammable and explosive material, or to high temperature and pressure material that human body may damage.If material Matter is poisonous and harmful or inflammable and explosive material, or is consolidated containing certain in the high temperature and pressure material that may be damaged to human body Body particle by sampling analysis, will determine the content size of solid particle in material to instruct technique to give birth in actual production process When production, open type is just not suitable for, and sampler closed at present leads to the sampling to this class I liquid I there are this defect It operates extremely difficult.Therefore, for the material of such special nature, it is necessary to improve sampling mode, design and produce one kind and be directed to Closed sampling device containing solid particle in liquid.
Utility model content
The technical problem to be solved by the present invention is to provide it is a kind of it is simple in structure, safe and reliable, will not pollute, just In the liquid closed sampler containing solid particle of clean and maintenance.
In order to solve the above technical problems, the utility model adopts the following technical solution:A kind of liquid containing solid particle Closed sampling device, it is characterised in that:Include sampling bottle, surge flask and absorption bottle, surge flask is connect with material pipeline, into Enter and be equipped with valve before surge flask, can thus reduce pressure, two take sample, safety higher from surge flask;It is described Sampling bottle is connect with surge flask, and connecting pipeline between the two is equipped with valve, and the absorption bottle is connected to this valve and buffering Between bottle, and another valve is equipped with before entering absorption bottle;The surge flask is also associated with nitrogen blowing mechanism.
Further, it is equipped with displacement sampling line between surge flask and material pipeline, replaces sampling line and materail tube Line connects, and valve G, valve A and valve B is respectively set on displacement sampling line, is replaced at two and a valve is arranged among sampling line For valve C, it is connected with surge flask;Cleaning solution mechanism is connected with by valve G between valve A and material pipeline.
Further, the valve being arranged between sampling bottle and surge flask is valve F, and the valve being arranged in absorption bottle front For valve E;Valve D is then equipped between surge flask and nitrogen blowing mechanism.
Further, the surge flask is the interior polishing stainless steel storage tank of 500ml, interior to carry magnetic float liquidlevel meter, just In the liquid measure of observation surge flask.
Further, the inlet and outlet interface of the surge flask carries silk head, and surge flask passes through its head and materail tube Line connects.
Further, a sampling adapter, the sampling are installed at the connecting pipeline between the sampling bottle and surge flask Adapter is between valve F and sampling bottle.
Further, the sampling adapter is made of tetrafluoro material, is connected by the interface of internal thread and sampling bottle It is fixed, and be connected and fixed by outer silk and the connecting pipeline.
In use, being first turned on valve B when sampling, valve A is then opened, material enters displacement sampling line, to be replaced suitable The triple valve (i.e. valve C) before surge flask is opened afterwards to be sampled, and is closed valve C when liquid level reaches 2/3 in bottle to be buffered, is closed valve A closes valve B.At this moment sampling bottle is connected, valve F is opened and takes the material in surge flask into sampling bottle, be then shut off valve F.It takes down Sampling bottle covers bottle cap.Remaining liquid in surge flask is taken to in absorption bottle, first opens valve G, valve A, valve B, then open valve C and valve E clean sampling line and surge flask, and cleaning solution drains into absorption bottle, closed after the completion of rinsing valve C, valve E, valve G, Valve A and valve B.Next valve D is opened, surge flask is purged with nitrogen, valve F is opened after purging several minutes to sampling adapter It is purged.Valve F is first closed after purging is clean, turns off valve D, finally closes valve E.Material pipeline is taken after sample in this way with being free of The material of solid particle rinses, while being also rinsed to surge flask, and the liquid of flushing is discharged to absorption bottle and is handled, it is ensured that every Sub-sampling has higher representativeness, while preventing from polluting the environment.Surge flask is carried out with nitrogen again after rinsing with washing lotion Displacement is clean, while being purged to sampling adapter, ensures that noresidue liquid in surge flask, sampling adapter are tieed up convenient for cleaning Shield, is replaced in time when inconvenient for use.
The utility model is to be directed to highly pressurised liquid material, and solid content is filled in 10% (w%) samplings below in material It sets, by installing a surge flask, one reduces pressure, and two avoid valve from failure occur when taking high-pressure material to be directed to has danger Danger, thus the utility model has many advantages, such as closed, time-consuming environment short, clean, safe, not easy to pollute, and can intuitively observe Material liquid level in surge tank, clean and maintenance easy to disassemble.
Description of the drawings
FIG. 1 is a schematic structural view of the utility model.
In figure, 1 is surge flask, and 2 be absorption bottle, and 3 be sampling adapter, and 4 be sampling bottle.
Specific implementation mode
In the present embodiment, referring to Fig.1, the liquid closed sampler containing solid particle, include sampling bottle 4, Surge flask 1 and absorption bottle 2, surge flask 1 are connect with material pipeline, and valve is equipped with before entering surge flask 2, can thus be dropped Low-pressure, two take the sample, safety higher from surge flask;The sampling bottle 4 is connect with surge flask 1, company between the two Take over line is equipped with valve, and the absorption bottle 2 is connected between this valve and surge flask 1, and is equipped with before entering absorption bottle 2 Another valve;The surge flask 1 is also associated with nitrogen blowing mechanism (not shown).
Between surge flask 1 and material pipeline be equipped with displacement sampling line, displacement sampling line split change sampling line with Material pipeline connects, and valve G, valve A and valve B is respectively set on displacement sampling line, replaces at two and is arranged among sampling line One valve is valve C, is connected with surge flask 1;Cleaning solution mechanism is connected with by valve G between valve A and material pipeline.
The valve being arranged between sampling bottle 4 and surge flask 1 is valve F, and the valve being arranged in 2 front of absorption bottle is valve E; Valve D is then equipped between surge flask 1 and nitrogen blowing mechanism.
The surge flask 1 is the interior polishing stainless steel storage tank of 500ml, interior to carry magnetic float liquidlevel meter, slow convenient for observation Rush the liquid measure of bottle.
The inlet and outlet interface of the surge flask 1 carries silk head, and surge flask 1 is connect by its head with material pipeline.
One sampling adapter 3 is installed, the sampling adapter 3 at the connecting pipeline between the sampling bottle 4 and surge flask 1 Between valve F and sampling bottle 4.
The sampling adapter 3 is made of tetrafluoro material, is connected and fixed by the interface of internal thread and sampling bottle 4, and It is connected and fixed with connecting pipeline by outer silk.
In use, being first turned on valve B when sampling, valve A is then opened, material enters displacement sampling line, to be replaced suitable The triple valve (i.e. valve C) for opening 1 front of surge flask afterwards is sampled, and is closed valve C when liquid level reaches 2/3 in bottle 1 to be buffered, is closed Valve A closes valve B.At this moment sampling bottle 4 is connected, valve F is opened and takes the material in surge flask 1 into sampling bottle 4, be then shut off valve F.Sampling bottle 4 is taken down, bottle cap is covered.Remaining liquid in surge flask is taken to in absorption bottle, valve G, valve A, valve B are first opened, Valve C and valve E are opened again, sampling line and surge flask 1 are cleaned, and cleaning solution drains into absorption bottle 2, is first closed after the completion of rinsing Valve C, valve E, valve G, valve A and valve B are turned off.Next valve D is opened, surge flask 2 is purged with nitrogen, after purging several minutes Valve F is opened to purge sampling adapter 3.Valve F is first closed after purging is clean, turns off valve D, finally closes valve E.
The utility model is described in detail above, it is described above, only the preferred embodiment of the utility model and , when the utility model practical range cannot be limited, i.e., all according to the made equivalent changes and modifications of the application range, it all should still belong to this In utility model covering scope.

Claims (7)

1. a kind of liquid closed sampler containing solid particle, it is characterised in that:Include sampling bottle, surge flask and absorption Bottle, surge flask are connect with material pipeline, and valve is equipped with before entering surge flask;The sampling bottle is connect with surge flask, the two Between connecting pipeline be equipped with valve, the absorption bottle is connected between this valve and surge flask, and enter absorption bottle it It is preceding to be equipped with another valve;The surge flask is also associated with nitrogen blowing mechanism.
2. the liquid closed sampler according to claim 1 containing solid particle, it is characterised in that:Surge flask with Displacement sampling line is equipped between material pipeline, displacement sampling line is connect with material pipeline, on displacement sampling line respectively Valve G, valve A and valve B are set, is replaced at two and a valve is set among sampling line for valve C, be connected with surge flask;Valve A with Cleaning solution mechanism is connected with by valve G between material pipeline, cleaning solution is the material without solid particle.
3. the liquid closed sampler according to claim 2 containing solid particle, it is characterised in that:Sampling bottle with The valve being arranged between surge flask is valve F, and the valve being arranged in absorption bottle front is valve E;Surge flask and nitrogen blowing mechanism Between then be equipped with valve D.
4. the liquid closed sampler according to claim 1 containing solid particle, it is characterised in that:The surge flask It is interior to carry magnetic float liquidlevel meter for the interior polishing stainless steel tap web storage tank of 500ml.
5. the liquid closed sampler according to claim 1 containing solid particle, it is characterised in that:The surge flask Inlet and outlet interface carry silk head, surge flask connect by its head with material pipeline.
6. the liquid closed sampler according to claim 3 containing solid particle, it is characterised in that:The sampling bottle One sampling adapter is installed, the sampling adapter is between valve F and sampling bottle at the connecting pipeline between surge flask.
7. the liquid closed sampler according to claim 6 containing solid particle, it is characterised in that:The sampling turns Connector is made of tetrafluoro material, is connected and fixed by the interface of internal thread and sampling bottle, and passes through outer silk and the connecting tube Line is connected and fixed.
CN201820117611.8U 2018-01-24 2018-01-24 A kind of liquid closed sampler containing solid particle Active CN207816632U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820117611.8U CN207816632U (en) 2018-01-24 2018-01-24 A kind of liquid closed sampler containing solid particle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820117611.8U CN207816632U (en) 2018-01-24 2018-01-24 A kind of liquid closed sampler containing solid particle

Publications (1)

Publication Number Publication Date
CN207816632U true CN207816632U (en) 2018-09-04

Family

ID=63324737

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820117611.8U Active CN207816632U (en) 2018-01-24 2018-01-24 A kind of liquid closed sampler containing solid particle

Country Status (1)

Country Link
CN (1) CN207816632U (en)

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Address after: 810007 No.1, Jinsi Road, Chengdong economic and Technological Development Zone, Xining City, Qinghai Province

Patentee after: Asia silicon (Qinghai) Co.,Ltd.

Address before: 810007 Qinghai city of Xining Province Economic and Technological Development Zone No. 1 gold Guilu

Patentee before: ASIA SILICON (QINGHAI) Co.,Ltd.