CN207811927U - The single crystal growing furnace of central reflector layer is set - Google Patents

The single crystal growing furnace of central reflector layer is set Download PDF

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Publication number
CN207811927U
CN207811927U CN201820158387.7U CN201820158387U CN207811927U CN 207811927 U CN207811927 U CN 207811927U CN 201820158387 U CN201820158387 U CN 201820158387U CN 207811927 U CN207811927 U CN 207811927U
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layer
heater
insulating layer
central reflector
reflector layer
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CN201820158387.7U
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Chinese (zh)
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吴学军
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Ningxia Xu Sakura Amperex Technology Ltd
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Ningxia Xu Sakura Amperex Technology Ltd
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Abstract

A kind of single crystal growing furnace of setting central reflector layer,Including two-layer platform,The furnace body being arranged above two-layer platform,The driving part being arranged below two-layer platform,Furnace body includes outer furnace tube and is arranged in internal thermal field,Thermal field includes crucible,Mounting base,Heater,Heat shielding component,Insulating layer,Central reflector layer,The central reflector layer is arranged between heater and insulating layer,Central reflector layer is smooth surface close to the surface of heater,To reflect the heat that heater distributes,The top of central reflector layer is higher than the top of heater,The bottom of central reflector layer is less than the bottom of heater,Heat fully to obstruct heater is transmitted to insulating layer to be scattered and disappeared,Central reflector layer is middle molybdenum cylinder,In the utility model,Heater is isolated with insulating layer using central reflector layer,Not only a large amount of heat is reflexed in crucible,Heat uses abundant,And avoid influence of the insulating layer volatile matter to crystal bar and heater.

Description

The single crystal growing furnace of central reflector layer is set
Technical field
The utility model is related to single crystal growing furnace technical field more particularly to a kind of single crystal growing furnaces of setting central reflector layer.
Background technology
Single crystal growing furnace is the necessary equipment that polysilicon is converted into monocrystalline silicon technical process, and monocrystalline silicon be photovoltaic generation and Basic material in semicon industry.Critical support material of the monocrystalline silicon as advanced information society is most heavy in the world at present One of monocrystal material wanted, it is not only development computer and the major function material and photovoltaic generation of integrated circuit utilize The major function material of solar energy.
In existing single crystal growing furnace, in order to be kept the temperature to heater, avoid heat along furnace body outer barrel heat loss through conduction, usually in stove Insulating layer is arranged in cylinder inside sidewalls, and insulating layer is enclosed in outside heater, to play the role of insulation, but this mode In, not only heat insulation effect is bad, moreover, insulating layer is usually carbon felt, carbon felt belongs to black material, is not only easy heat absorption, moreover, Volatile matter is more, forms impurity and is present in thermal field, causes the influence to molten bath or crystal bar.
Utility model content
It is necessary to propose a kind of single crystal growing furnace of setting central reflector layer.
A kind of single crystal growing furnace of setting central reflector layer, including two-layer platform, the furnace body being arranged above two-layer platform, setting Driving part below two-layer platform, furnace body include outer furnace tube and are arranged in internal thermal field, and outer furnace tube includes from the top down Bell, middle furnace tube and the lower furnace tube of connection be installed successively, lower furnace tube is mounted on two-layer platform, thermal field include crucible, mounting base, Heater, heat shielding component, insulating layer, under mounting base setting in furnace tube, to install crucible, crucible is arranged in middle furnace tube, heating Device encirclement is arranged around crucible, and to carry out heating material to the material in crucible, insulating layer includes setting successively from the top down Upper insulating layer, middle insulating layer, the lower insulating layer set, upper insulating layer are arranged between heat shielding component and middle furnace tube, and middle insulating layer is set It sets between heater and middle furnace tube, lower insulating layer is arranged between mounting base and lower furnace tube, and the upper end of driving part passes through down The bottom of furnace tube to be connect with mounting base, and then drives crucible rotation and lifting, and the heat shielding component includes inner draft tube, outer Guide shell, thermal insulation packing layer, support ring, pressure ring, inner draft tube are the conically shaped of big upper and lower small mouth, and external flow guiding cylinder is cylinder Shape cylinder, the top of external flow guiding cylinder turns down outward forms outer eaves, and the bottom fold inward of external flow guiding cylinder forms inner edge, inner draft tube Bottom is fastened on the inner edge of external flow guiding cylinder, and thermal insulation packing layer is filled between inner draft tube and external flow guiding cylinder, in external flow guiding cylinder Outer eaves above also fill thermal insulation packing layer, the thermal insulation packing layer above outer eaves is connect with the upper insulating layer in middle furnace tube, pressure ring For annular slab, pressure ring is pressed in the thermal insulation packing layer above outer eaves, and the interior edge of pressure ring is contacted with the suitable for reading of inner draft tube, pressure ring Outer is aligned with the edge of the outer eaves of external flow guiding cylinder, and support ring is annular slab, and support ring is arranged under the outer eaves of external flow guiding cylinder Side, the edge of support ring is fixedly connected with the inside of middle furnace tube, to place heat shielding component, inner draft tube, external flow guiding cylinder, support Ring, pressure ring coaxial arrangement, the thermal field further includes central reflector layer, central reflector layer setting heater and insulating layer it Between, central reflector layer is smooth surface close to the surface of heater, to reflect the heat that heater distributes, centre reflection The top of layer is higher than the top of heater, and the bottom of central reflector layer is less than the bottom of heater, fully to obstruct heater Heat is transmitted to insulating layer to be scattered and disappeared, and central reflector layer is middle molybdenum cylinder.
Preferably, the inner draft tube is made of metal molybdenum, and external flow guiding cylinder is made of graphite material, and thermal insulation packing layer is stone Black carbon felt.
Preferably, inner cylinder is isolated in setting also between external flow guiding cylinder and middle insulating layer, and upper end and the support ring of inner cylinder is isolated Contact, is isolated the lower end of inner cylinder and the upper-end contact of central reflector layer, middle insulating layer is isolated with thermal field, avoids graphite material The volatile matter of manufactured middle insulating layer enters in thermal field to be in direct contact with crystal bar.
Preferably, middle molybdenum cylinder is prepared for molybdenum material.
In the utility model, heater is isolated with insulating layer using central reflector layer, not only reflects a large amount of heat To crucible, heat uses fully, and avoids influence of the insulating layer volatile matter to crystal bar and heater.
Description of the drawings
Fig. 1 is the structural schematic diagram of single crystal growing furnace.
Fig. 2 is the structural schematic diagram of the furnace body.
Fig. 3 is the partial enlarged view in Fig. 2.
Fig. 4 is the structural schematic diagram of air exhaust loop.
Fig. 5 is the structural schematic diagram of two-layer platform.
Fig. 6 is the structural schematic diagram of another angle of two-layer platform.
Fig. 7 is the partial enlarged view in Fig. 6.
In figure:Two-layer platform 10, watch window 101, bell 11, middle furnace tube 12, lower furnace tube 13, first row air-casing 131, Two exhaust flanges 132, crucible 21, mounting base 22, heater 23, heat shielding component 24, inner draft tube 241, external flow guiding cylinder 242, outer eaves 2421, inner edge 2422, thermal insulation packing layer 243, support ring 244, pressure ring 245, isolation inner cylinder 246, upper insulating layer 251, middle heat preservation Layer 252, lower insulating layer 253, downtake pipe 261, second exhaust pipe 262, air exhaust loop 263, inside ring wall 264, air inlet 2641, outside ring wall 265, gas outlet 2651, ring bottom 266, lower flange ring 267, central reflector layer 271, connecting plate 31, scale 32, the first guide part 33, mounting plate 331, resin ring 332, housing screw 333, the second guide part 34, pointer 35, counterweight 36.
Specific implementation mode
It, below will be to required use in embodiment in order to illustrate more clearly of the technical solution of the utility model embodiment Attached drawing be briefly described, it should be apparent that, the accompanying drawings in the following description is some embodiments of the utility model, for this For the those of ordinary skill of field, without creative efforts, others are can also be obtained according to these attached drawings Attached drawing.
Referring to Fig. 1 to Fig. 7, the utility model embodiment provides a kind of single crystal growing furnace, including two-layer platform 10, setting two The furnace body of 10 top of layer platform, the driving part being arranged below two-layer platform 10, furnace body include outer furnace tube and are arranged in inside Thermal field, outer furnace tube includes the bell 11 for installing connection successively from the top down, middle furnace tube 12 and lower furnace tube 13, and lower furnace tube 13 is installed On two-layer platform 10, thermal field includes crucible 21, mounting base 22, heater 23, heat shielding component 24, insulating layer, and mounting base 22 is set It sets in lower furnace tube 13, to install crucible 21, crucible 21 is arranged in middle furnace tube 12, and heater 23 surrounds the week being arranged in crucible 21 It encloses, to carry out heating material to the material in crucible 21, heat shielding component 24 is arranged in the top of crucible 21, in heat shielding component 24 Between setting crystal bar channel, insulating layer includes the upper insulating layer 251, middle insulating layer 252, lower insulating layer set gradually from the top down 253, upper insulating layer 251 is arranged between heat shielding component 24 and middle furnace tube 12, and middle insulating layer 252 is arranged in heater 23 and middle stove Between cylinder 12, lower insulating layer 253 is arranged between mounting base 22 and lower furnace tube 13, and the upper end of driving part passes through lower furnace tube 13 Bottom to be connect with mounting base 22, and then drives the rotation of crucible 21 and lifting, and the thermal field further includes middle gas deflation assembly, under First row air-casing 131 and second row air-casing 132, one end of first row air-casing 131 and second are symmetrical arranged on the side wall of furnace tube 13 One end of exhaust flange 132 leaks outside outside lower furnace tube 13, for being connect with external extraction sector, first row air-casing 131 it is another End and the other end pass through lower furnace tube 13 and insulating layer, to be connected to middle gas deflation assembly, middle gas deflation assembly includes downtake pipe 261, second exhaust pipe 262, air exhaust loop 263, downtake pipe 261, second exhaust pipe 262 are symmetricly set on the two of heater 23 Side, downtake pipe 261, second exhaust pipe 262 are arranged close to insulating layer, and downtake pipe 261, second exhaust pipe 262 are The lower end of the hollow straight pipe being vertically arranged, downtake pipe 261 is connected to first row air-casing 131, the upper end of downtake pipe 261 Connect with air exhaust loop 263, the lower end of second exhaust pipe 262 is connected to second row air-casing 132, the upper end of second exhaust pipe 262 with Air exhaust loop 263 connects, and air exhaust loop 263 is an annulus, and the thermal field in the top of crucible 21 and heater 23 is arranged in air exhaust loop 263 Interior, air exhaust loop 263 includes inside ring wall 264, outside ring wall 265, ring bottom 266, and inside ring wall 264, outside ring wall 265 are concentric Circle, ring bottom 266 is connected to inside ring wall 264, between outside ring wall 265, to form U-shaped annular groove, also in interior side ring wall 264, outer Air inlet 2641 and gas outlet 2651, gas outlet 2651 and downtake pipe 261, second exhaust are opened up on side ring wall 265 respectively The upper end of pipe 262 is connected to, and air inlet 2641 is connected to the thermal field of 264 inside of inside ring wall, with the heat above 21 oral area of crucible Gas is discharged in.
The bushing position identity device is arranged in the lower section of two-layer platform 10, and bushing position identity device includes lower limit Mechanism and upper limit mechanism, it includes lifting motor, retarder, leading screw, guide sleeve that the driving part below two-layer platform 10, which is arranged, Lifting motor is connect by retarder with leading screw, and to drive leading screw to rotate, leading screw is connect with guide sleeve screw-driven, the upper end of guide sleeve It is connect with mounting base 22, to drive crucible 21 to lift, lower limiting mechanism is fixed at the two-layer platform 10 below driving part Rack on, limited with the extreme lower position of the decline to guide sleeve, upper limit mechanism is fixed above driving part In the rack of two-layer platform 10, limited with the extreme higher position of the decline to guide sleeve.
Further, the air inlet 2641 on the inside ring wall 264 is symmetrically arranged at least four, the outside ring wall Gas outlet 2651 on 265 is symmetrically arranged two, uniformly to be aspirated to the gas in thermal field, the gas outlet 2651 and into Gas port 2641 shifts to install.Air exhaust loop 263 is set as U-shaped annular groove, and when outside is evacuated, gas in thermal field is from air inlet 2641 It into U-shaped annular groove, is discharged by the blocking of outside ring wall 265, then by gas outlet 2651, what carrying was mingled in such gas waves Hair object or impurity encounter outside ring wall 265 blocking after be easily adhered or be deposited in U-shaped annular groove, convenient for volatile matter concentration receive Collection, without entering exhaust pipe and external system, this makes the collection of volatile matter guidance quality, reduction be adhered to thermal field other component On probability, when clearing up furnace body, only need to by the substance clearing and retrieving in U-shaped annular groove, due in volatile matter majority be carbonaceous and Silicon also helps the recycling of these substances, increases operation rate.
Further, the thermal field further includes central reflector layer 271, the setting of the central reflector layer 271 heater 23 with Between insulating layer, central reflector layer 271 is smooth surface close to the surface of heater 23, with heat that heater 23 is distributed into Row reflection, the top of central reflector layer 271 are higher than the top of heater 23, and the bottom of central reflector layer 271 is less than heater 23 Bottom, scattered and disappeared with fully obstructing the heat of heater 23 and being transmitted to insulating layer.
Since insulating layer is made of graphite material, graphite material belongs to black material, is easy to absorb heat, although playing Insulation effect, but partial heat is also absorbed, cause the non-power consumption loss of heat;And graphite material heating time is long, and it is crisp Property is big, fragile, and when carrying is easy to breakage, and service life is short;Also, during use, under long-time hot environment, graphite Material volatile matter is more, and volatile matter is adhered on heater 23, causes 23 local pyrexia of heater serious, scaling loss is serious, Huo Zhehui Hair object passes through heater 23 to enter 21 top of crucible or be adhered to crystal bar surface, pollutes crystal bar, is influenced more on the quality of crystal bar Seriously.In the utility model, molybdenum cylinder is isolated by heater 23 with insulating layer in, and a large amount of heat is not only reflexed to crucible In 21, heat uses fully, and avoids influence of the insulating layer volatile matter to crystal bar and heater 23.
Further, central reflector layer 271 is middle molybdenum cylinder, and middle molybdenum cylinder is prepared for molybdenum material.Since metal material molybdenum is resistance to High-temperature behavior is good, and heat-proof quality is good, and the reflection of heat is convenient on smooth surface, and then reduces scattering and disappearing for heat.
Further, the outside ring wall 265 of air exhaust loop 263 is downwardly extending lower flange ring 267, lower flange ring 267 and ring Annular groove is formed between bottom 266, the central reflector layer 271 is the hollow cylinder being enclosed in around heater 23, central reflector layer 271 top is embedded in the annular groove between lower flange ring 267 and ring bottom 266.
Air exhaust loop 263 is embedding between lower flange ring 267 and central reflector layer 271 while playing to form exhaust passage Enter connection, a closed separation layer being enclosed in around heater 23 is collectively formed, since middle insulating layer 252 is enclosed in crucible Around 21 and around heater 23, and it is also around heater 23 to radiate the most serious, and the upper end of the separation layer is covered The top of lid heater 23, the bottom of the lower end covering heating of separation layer, completely by the horizontal heat radiation of 23 most serious of heater Region overlay avoids heat and scatters and disappears to the radiation of middle insulating layer 252, scatters and disappears so as to avoid the idle work of heat.
Further, the heat shielding component 24 includes inner draft tube 241, external flow guiding cylinder 242, thermal insulation packing layer 243, support ring 244, pressure ring 245, inner draft tube 241 are the conically shaped of big upper and lower small mouth, and external flow guiding cylinder 242 is cylindrical tube, external flow guiding cylinder 242 top turns down outward forms outer eaves 2421, and the bottom fold inward of external flow guiding cylinder 242 forms inner edge 2422, inner draft tube 241 bottom is fastened on the inner edge 2422 of external flow guiding cylinder 242, and thermal insulation packing layer 243 is filled in inner draft tube 241 and outer water conservancy diversion Between cylinder 242, thermal insulation packing layer 243 is also filled above the outer eaves 2421 of external flow guiding cylinder 242, the heat preservation of 2421 top of outer eaves is filled out It fills layer 243 to connect with the upper insulating layer 251 in middle furnace tube 12, pressure ring 245 is annular slab, and pressure ring 245 is pressed in 2421 top of outer eaves Thermal insulation packing layer 243 on, the interior edge of pressure ring 245 is contacted with the suitable for reading of inner draft tube 241, the outer of pressure ring 245 and outer water conservancy diversion The edge alignment of the outer eaves 2421 of cylinder 242, support ring 244 is annular slab, and the outer eaves in external flow guiding cylinder 242 is arranged in support ring 244 2421 lower section, the edge of support ring 244 are fixedly connected with the inside of middle furnace tube 12, to place heat shielding component 24, inner draft tube 241, external flow guiding cylinder 242, support ring 244, pressure ring 245 are coaxially disposed.
Insulating layer described in text is carbon felt.
Further, the inner draft tube 241 is made of metal molybdenum, and external flow guiding cylinder 242 is made of graphite material, heat preservation filling Layer 243 is graphite carbon felt.Inner draft tube 241 is isolated by the thermal insulation packing layer 243 of graphite material and external flow guiding cylinder 242 with crystal bar, It avoids volatile matter from being in direct contact with crystal bar, pollutes crystal bar.
Further, inner cylinder 246 is isolated in setting also between external flow guiding cylinder 242 and middle insulating layer 252, isolation inner cylinder 246 Upper end is contacted with support ring 244, be isolated inner cylinder 246 lower end and central reflector layer upper-end contact, by middle insulating layer 252 with Thermal field is isolated, and is avoided the volatile matter of middle insulating layer 252 made of graphite material from entering in thermal field and is in direct contact with crystal bar.
Further, upper limit mechanism includes connecting plate 31, scale 32, the first guide part 33, the second guide part 34, pointer 35, counterweight 36, connecting plate 31 are fixedly connected along horizontal direction with guide sleeve, with guide sleeve synchronization lifting, scale 32 is one flexible One end of elongated scale 32, scale 32 is fixedly connected with connecting plate 31, and the other end of scale 32 is connect with counterweight 36, and first is oriented to Part 33, the second guide part 34 are fixedly connected with the rack of two-layer platform 10, and the setting of pointer 35 is led in the first guide part 33 and second To between part 34, and pointer 35 is fixedly connected with the rack of two-layer platform 10, and the middle section of scale 32 is overlapped on the first guiding On part 33 and the second guide part 34, scale marker is set on scale 32, shows that guide sleeve and crucible 21 rise to coordinate with pointer 35 Position.
Further, watch window 101 is also opened up on the table top of two-layer platform 10, watch window 101 is slot, is seen The Opening length for examining window 101 is more than opening width, and one end of pointer 35 is fixedly connected with rack, and the other end of pointer 35 is point The pointed end of sharp end, pointer 35 is arranged close to the mark of scale 32, with the position of accurate display mark.
Further, the first guide part 33,34 mechanism having the same of the second guide part, the first guide part 33 include mounting plate 331, resin ring 332, housing screw 333, one end of mounting plate 331 are fixedly connected with rack, and the other end of mounting plate 331 is used for Resin ring 332 is installed, resin ring 332 is hollow cylinder, and resin ring 332 has smooth surface, the surface of resin ring 332 wide Degree is more than the width of scale 32, so that scale 32 is slided along the surface of resin ring 332, the end of housing screw 333 passes through tree Alicyclic ring 332, resin ring 332 is fixed on mounting plate 331, the resin ring 332 of the first guide part 33 and the second guide part 34 Resin ring 332 be mounted on rack identical horizontal plane in so that the mark between the first guide part 33 and the second guide part 34 Ruler 32 is also in horizontal plane.
In silicon single crystal pulling process, needs to estimate remaining silicon material in crucible 21, calculate remaining crystal bar and elongated Degree, bushing position identity device are exactly to be designed accurately to calculate the position of remaining silicon material in positioning crucible 21.
When putting into the progress crystal pulling later of a certain amount of silicon material in crucible 21 every time, crucible 21 drops to preset minimum Position, but no more than the position of lower limit mechanism setting, the silicon material at the end of crystal pulling soon, that is, in crucible 21 is remaining few When 3kg, it may appear that cause crystal bar that cannot grow according to predetermined dimensions because the silicon material in crucible 21 is very little, need at this time The ending of crystal pulling, that is, the ending of crystal pulling program are carried out, but if the remaining extra scheduled amount of silicon material in crucible 21, such as 3kg, and the round-off work of crystal pulling is carried out in advance, and the silicon material in crucible 21 that causes of meeting is underused, and the wave of silicon material is caused Take, in the prior art, the control of this time point usually requires manually to calculate, to control, manually to combine computer program and crystal bar Growth size, growth time COMPREHENSIVE CALCULATING obtain the amount of remaining silicon material in crucible 21, controlled again after obtaining this remaining amount Program finishes up, this calculating process is not only due to the calculating time is longer and leads to result of calculation and real surplus object in crucible 21 There are gaps for material, and exist and artificially calculate inevitable error, inaccurate so as to cause the starting point control of program ending.
In the utility model, bushing position identity device is devised, the connecting plate 31 in the device and 21 liters of crucible of driving The guide sleeve of drop is fixedly connected so that scale 32 and 21 synchronization lifting of crucible, and the sliding of scale 32 is overlapped in the first guide part 33, the On two guide parts 34, the first guide part 33, the second guide part 34 are fixedly connected with rack, and during crystal pulling, crucible 21 is according to pre- Determine program rising, at this point, the scale 32 in 33 left side of the first guide part is also synchronized under the action of counterweight 36 and moved up, second leads It being moved downward simultaneously under the action of counterweight 36 to the scale 32 on 34 right side of part, the home position that pointer 35 indicates also is changing, Certain position is risen to crucible 21, at this time in crucible 21 when remaining scheduled surplus, which is a fixed determination Position, pointer 35, which corresponds to, at this time indicates a fixed home position, and operating personnel need to only observe the instruction of pointer 35 without calculating Physical location arrived the fixed home position, you can operation sequence start epilogue.
Using the device, it converts the amount of surplus material in crucible 21 to the fixed flag that scale 32 is shown It sets, which marks as one, only need to observe the label, you can the ending of control crystal pulling program starts the time Point operates accurate difference, nor can cause the problem of surplus material wastes more in crucible 21.
Wherein, the fixed home position is different because of the difference of the amount of the material of input crucible 21, such as by multiple After Test Summary, after putting into the material of 150kg, scheduled surplus is that 2kg starts epilogue after crystal pulling, is corresponded at this time Home position be " 10 ";After putting into the material of 180kg, scheduled surplus is that 3kg starts epilogue after crystal pulling, this When corresponding home position be " 11 ".
For example, an ending mark and the crystal bar table of comparisons can be made, the table of comparisons includes crystal bar size column, input silicon material Column, scale 32 mark column, and the size for waiting for pulled crystal stick is listed in crystal bar size column, and input silicon material column is listed and monocrystal rod ruler The amount of the very little corresponding silicon material put into crucible 21, it is opposite with crystal bar size column, input silicon material column that scale 32 marks column to list The mark position for the scale 32 answered.
The fixed home position marked on the scale 32 of startup epilogue is indicated in above-mentioned apparatus, in production different shaped When number product, operating personnel need to only search crystal bar size, the amount of the silicon material of input in the table of comparisons, you can lookup is corresponded to Label mark, when the position on 35 indicator scale 32 of pointer reaches the label home position, start epilogue.
Module or unit in the utility model embodiment device can be merged, divide and be deleted according to actual needs Subtract.
Above disclosures are merely preferred embodiments of the utility model, with this utility model cannot be limited certainly Interest field, those skilled in the art can understand all or part of the processes for realizing the above embodiment, and according to this reality The equivalent variations made by novel claim, still fall within the scope of the utility model.

Claims (4)

1. a kind of single crystal growing furnace of setting central reflector layer, it is characterised in that:Including two-layer platform, it is arranged above two-layer platform Furnace body, the driving part being arranged below two-layer platform, furnace body include outer furnace tube and are arranged in internal thermal field, and outer furnace tube includes Bell, middle furnace tube and the lower furnace tube of connection are installed successively from the top down, lower furnace tube is mounted on two-layer platform, and thermal field includes earthenware Crucible, mounting base, heater, heat shielding component, insulating layer, under mounting base setting in furnace tube, to install crucible, crucible is arranged in middle stove In cylinder, heater encirclement is arranged around crucible, to carry out heating material to the material in crucible, insulating layer include on to Under the upper insulating layer, middle insulating layer, the lower insulating layer that set gradually, upper insulating layer is arranged between heat shielding component and middle furnace tube, in Insulating layer is arranged between heater and middle furnace tube, and lower insulating layer is arranged between mounting base and lower furnace tube, driving part it is upper End is across the bottom of lower furnace tube, to be connect with mounting base, and then drives crucible rotation and lifting, and the heat shielding component includes interior leads Flow cartridge, external flow guiding cylinder, thermal insulation packing layer, support ring, pressure ring, inner draft tube are the conically shaped of big upper and lower small mouth, external flow guiding cylinder For cylindrical tube, the top of external flow guiding cylinder turns down outward forms outer eaves, and the bottom fold inward of external flow guiding cylinder forms inner edge, inside leads The bottom of flow cartridge is fastened on the inner edge of external flow guiding cylinder, and thermal insulation packing layer is filled between inner draft tube and external flow guiding cylinder, outside Thermal insulation packing layer is also filled above the outer eaves of guide shell, the thermal insulation packing layer above outer eaves connects with the upper insulating layer in middle furnace tube It connects, pressure ring is annular slab, and pressure ring is pressed in the thermal insulation packing layer above outer eaves, and interior edge and the suitable for reading of inner draft tube of pressure ring connect It touches, the outer of pressure ring is aligned with the edge of the outer eaves of external flow guiding cylinder, and support ring is annular slab, and support ring is arranged in external flow guiding cylinder The lower section of outer eaves, the edge of support ring are fixedly connected with the inside of middle furnace tube, to place heat shielding component, inner draft tube, outer water conservancy diversion Cylinder, support ring, pressure ring coaxial arrangement, the thermal field further includes central reflector layer, central reflector layer setting heater with Between insulating layer, central reflector layer is smooth surface close to the surface of heater, to reflect the heat that heater distributes, The top of central reflector layer is higher than the top of heater, and the bottom of central reflector layer is less than the bottom of heater, fully to obstruct The heat of heater is transmitted to insulating layer to be scattered and disappeared, and central reflector layer is middle molybdenum cylinder.
2. the single crystal growing furnace of setting central reflector layer as described in claim 1, it is characterised in that:The inner draft tube is metal molybdenum It is made, external flow guiding cylinder is made of graphite material, and thermal insulation packing layer is graphite carbon felt.
3. the single crystal growing furnace of setting central reflector layer as claimed in claim 2, it is characterised in that:Also in external flow guiding cylinder and middle heat preservation Setting isolation inner cylinder between layer, the upper end that inner cylinder is isolated contacts with support ring, be isolated inner cylinder lower end and central reflector layer it is upper End in contact is isolated by middle insulating layer with thermal field, avoid the volatile matter of middle insulating layer made of graphite material enter in thermal field with Crystal bar is in direct contact.
4. the single crystal growing furnace of setting central reflector layer as described in claim 1, it is characterised in that:Middle molybdenum cylinder for molybdenum material prepare and At.
CN201820158387.7U 2018-01-30 2018-01-30 The single crystal growing furnace of central reflector layer is set Active CN207811927U (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113970243A (en) * 2021-10-14 2022-01-25 中国科学院沈阳科学仪器股份有限公司 Thin-wall heat-insulating layer structure of beam source furnace
CN114574944A (en) * 2022-03-21 2022-06-03 北京晶格领域半导体有限公司 Silicon carbide single crystal liquid phase growth device and method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113970243A (en) * 2021-10-14 2022-01-25 中国科学院沈阳科学仪器股份有限公司 Thin-wall heat-insulating layer structure of beam source furnace
CN114574944A (en) * 2022-03-21 2022-06-03 北京晶格领域半导体有限公司 Silicon carbide single crystal liquid phase growth device and method

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