CN207805607U

CN207805607U - A kind of acid dissolution reaction device for making in laboratory Coating Materials

Info

Publication number: CN207805607U
Application number: CN201721703387.2U
Authority: CN
Inventors: 戴和贵
Original assignee: Danyang Koda Coating Material Co Ltd
Current assignee: Danyang Koda Coating Material Co Ltd
Priority date: 2017-12-10
Filing date: 2017-12-10
Publication date: 2018-09-04
Anticipated expiration: 2027-12-10

Abstract

The utility model is related to Coating Materials technical fields; and disclose a kind of acid dissolution reaction device for making in laboratory Coating Materials; including pedestal; the bottom of the pedestal is fixedly connected with protective shell; the right side opening of the protective shell bottom is equipped with bayonet, and the inside of the bayonet is fixedly connected with sprue, gasket is fixedly connected at the top of the protective shell; the hinged seat that passes on left at the top of the protective shell is hinged with lid, and the bottom of hinged seat is fixedly connected with protective shell.This is used for the acid dissolution reaction device of making in laboratory Coating Materials, by the way that agitating paddle, micromotor, acid inlet tube is arranged, experimenter can be effectively set to be slowly stirred while slow acid adding, effectively make reaction rapid heat dissipation, avoids the danger of fried kettle, improve experiment safety, finally by setting windowpane, experimenter can observe and record reaction process constantly, can find and handle accident in time, to effectively raise the safety of experiment.

Description

A kind of acid dissolution reaction device for making in laboratory Coating Materials

Technical field

The utility model is related to Coating Materials technical field, specially a kind of acid for making in laboratory Coating Materials is molten Reaction unit.

Background technology

Coating Materials is usually to heat target surface component is made to be evaporated out with atomic group or ionic species, and settle In substrate surface, film is formed by film forming procedure, it is well known that the technology trends of Coating Materials and downstream application industry Thin film technique development trend it is closely bound up, with technological improvement of the application industry on film product or element, target technology Also should change therewith, the exploitation of proximal segment time low-resistivity thin copper film, it is contemplated that the coming years will significantly replace original aluminium film, In addition, flat-panel screens significantly replaces former computer monitor and TV market based on cathode-ray tube in recent years, also The technology and the market demand of ITO target will be significantly increased.

Existing Coating Materials currently on the market, it is necessary first to Coating Materials of the research staff in product in laboratory small lot For studying, it is therefore desirable to use strong acid, highly basic and the virose noble metal of tool, often be occurred using simple and crude experimental facilities Pacify ring accident, such as during reacting with indium using nitric acid and finally producing indium sesquioxide, adds the excessive velocities of nitric acid, it cannot be timely Stirring heat dissipation, the accident to occur to fry kettle causes injury to personnel, pollution environment and property loss, therefore proposes a kind of for testing The acid dissolution reaction device that room makes Coating Materials is mentioned above to solve the problems, such as to improve experiment safety.

Utility model content

(1) the technical issues of solving

In view of the deficiencies of the prior art, it is molten anti-to provide a kind of acid for making in laboratory Coating Materials for the utility model Device is answered, has the advantages that experiment safety is high, solves the problems, such as that current laboratory equipment experiment is unsafe.

(2) technical solution

To realize that above-mentioned safe purpose, the utility model provide the following technical solutions：One kind being used for laboratory system Make the acid dissolution reaction device of Coating Materials, including pedestal, the bottom of the pedestal is fixedly connected with protective shell, the protective shell bottom The right side opening in portion is equipped with bayonet, and the inside of the bayonet is fixedly connected with sprue, is fixedly connected at the top of the protective shell close Packing, the hinged seat that passes on left at the top of the protective shell are hinged with lid, and the inner wall of the protective shell offers annular groove, institute The inside for stating annular groove is connected with support plate, and the upper surface of the support plate offers through-hole, and the inner bottom wall of the protective shell is set It is equipped with splicing groove, the left side at the top of the support plate is provided with vent gas treatment bottle, the outer right wall of the protective shell and positioned at branch Offer observation panel at the top of fagging, the inside of observation panel is fixedly connected with windowpane, the top of the support plate and is located at tail It is provided with reaction kettle on the right side of gas disposal bottle, left bottle neck, the inside of the left bottle neck are offered on the left of the reaction kettle outer wall It is threaded with left plug, the left side of the left plug offers left through-hole, and the inside of left through-hole is fixedly connected with offgas duct, and tail Tracheae extends to the inside of reaction kettle, and the one end of the offgas duct far from reaction kettle passes through the bottleneck of vent gas treatment bottle and extends to The right side opening of the inside of vent gas treatment bottle, the reaction kettle outer wall is equipped with right bottle neck, and top is offered at the top of the reaction kettle The internal whorl of bottle neck, the right bottle neck is connected with right plug, and the right side of the right plug offers right through-hole, the inside of right through-hole It is fixedly connected with acid inlet tube, the left end of the acid inlet tube extends to the inside of reaction kettle, and the internal whorl of the top bottle neck connects It is connected to top bottle stopper, the inside of the top bottle stopper is fixedly connected with shaft, and the left side at the top of the top bottle stopper is fixedly connected There are micromotor, the output shaft of the micromotor to be fixedly connected with driving gear, the inner rotation of the shaft is connected with master Bar, and the bottom end of mobile jib extends into the inside of reaction kettle, the bottom end of the mobile jib is fixedly connected with agitating paddle, the top of the mobile jib End is fixedly connected with driven gear, and driving gear is engaged with driven gear, the acid inlet tube one end and storage far from reaction kettle The outlet of sour tank is fixedly connected, and the right side of acid storage tank is fixedly connected with supporting rod, and the bottom end of supporting rod is fixedly connected with pedestal.

Preferably, buckle is hinged on the right side of the lid, the outer wall on the right side of the protective shell and the top positioned at windowpane Portion offers card slot, and the bottom end buckled and card slot clamping.

Preferably, tail gas hole is offered on the left of the protective shell bottom, the inside in tail gas hole is fixedly connected with exhaust pipe.

Preferably, the shape of the reaction kettle is spherical in shape and bottom is in plane.

Preferably, the level height of the acid inlet tube from right to left gradually reduces.

Preferably, the shape of the agitating paddle is in elliposoidal.

(3) advantageous effect

Compared with prior art, the utility model provides a kind of molten reaction dress of the acid for making in laboratory Coating Materials It sets, has following advantageous effect：

This is used for the acid dissolution reaction device of making in laboratory Coating Materials, and reality can effectively be isolated by the way that protective shell is arranged The person of testing makes experimenter with environment from testing the harm brought, to improve experiment safety, is then supported by being arranged Plate, through-hole and splicing groove can effectively prevent the secondary destruction that fried kettle is brought, and to improve experiment safety, then pass through Vent gas treatment bottle, offgas duct and exhaust pipe are set, can effectively be absorbed and emission, experimenter and ring are effectively protected Border to improve experiment safety, then by the way that agitating paddle, micromotor, acid inlet tube is arranged, effectively can make experimenter exist It is slowly stirred while slow acid adding, effectively makes reaction rapid heat dissipation, avoided the danger of fried kettle, improve experiment safety, most Afterwards by the way that windowpane is arranged, experimenter can observe and record reaction process, can find in time and handle accident constantly, from And effectively raise the safety of experiment.

Description of the drawings

Fig. 1 is the structural schematic diagram of the utility model；

Fig. 2 is the enlarged drawing in the portions A in the utility model Fig. 1.

In figure：1 pedestal, 2 protective shells, 3 bayonets, 4 sprues, 5 gaskets, 6 lids, 7 annular grooves, 8 support plates, 9 through-holes, 10 splicing grooves, 11 vent gas treatment bottles, 12 windowpanes, 13 reaction kettles, 14 left bottle necks, 15 left plugs, 16 offgas ducts, 17 right bottle necks, 18 Top bottle neck, 19 right plugs, 20 acid inlet tubes, 21 top bottle stoppers, 22 shafts, 23 micromotors, 24 driving gears, 25 mobile jibs, 26 are stirred Mix paddle, 27 driven gears, 28 acid storage tanks.

Specific implementation mode

The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work The every other embodiment obtained, shall fall within the protection scope of the present invention.

Please refer to Fig.1-2, a kind of acid dissolution reaction device for making in laboratory Coating Materials, including pedestal 1, pedestal 1 Bottom be fixedly connected with protective shell 2, setting protective shell 2 can effective isolation experiment person, make experimenter with environment from reality The harm brought is tested, tail gas hole is offered on the left of 2 bottom of protective shell, the inside in tail gas hole is fixedly connected with exhaust pipe, protection The right side opening of 2 bottom of shell is equipped with bayonet 3, and the inside of bayonet 3 is fixedly connected with sprue 4, and the top of protective shell 2 is fixedly connected with The hinged seat that passes on left of gasket 5,2 top of protective shell is hinged with lid 6, and the right side of lid 6 is hinged with buckle, protective shell 2 The outer wall on right side and the top for being located at windowpane 12 offer card slot, and the bottom end buckled and card slot clamping, the inner wall of protective shell 2 Annular groove 7 is offered, the inside of annular groove 7 is connected with support plate 8, and the upper surface of support plate 8 offers through-hole 9, protective shell 2 Inner bottom wall is provided with splicing groove 10, can effectively prevent the secondary destruction that fried kettle is brought, to improve experiment safety, branch The left side at the top of fagging 8 is provided with vent gas treatment bottle 11, can be with by the way that vent gas treatment bottle 11, offgas duct 16 and exhaust pipe is arranged It is effective to absorb and emission, it is effectively protected experimenter and environment, the outer right wall of protective shell 2 and is located at support plate 8 Top offer observation panel, the inside of observation panel is fixedly connected with windowpane 12, the top of support plate 8 and at tail gas The right side of reason bottle 11 is provided with reaction kettle 13, and the shape of reaction kettle 13 is spherical in shape and bottom is in plane, a left side for 13 outer wall of reaction kettle Side offers left bottle neck 14, and the internal whorl of left bottle neck 14 is connected with left plug 15, and the left side of left plug 15 offers left through-hole, left The inside of through-hole is fixedly connected with offgas duct 16, and offgas duct 16 extends to the inside of reaction kettle 13, and offgas duct 16 is far from reaction One end of kettle 13 passes through the bottleneck of vent gas treatment bottle 11 and extends to the inside of vent gas treatment bottle 11, the right side of 13 outer wall of reaction kettle Side offers right bottle neck 17, and the top of reaction kettle 13 offers top bottle neck 18, and the internal whorl of right bottle neck 17 is connected with right plug 19, the right side of right plug 19 offers right through-hole, and the inside of right through-hole is fixedly connected with acid inlet tube 20, and acid inlet tube 20 is from right to left Level height gradually reduce, the left end of acid inlet tube 20 extends to the inside of reaction kettle 13, and acid inlet tube 20 is far from reaction kettle 13 One end is fixedly connected with the outlet of acid storage tank 28, and the right side of acid storage tank 28 is fixedly connected with supporting rod, the bottom end of supporting rod with Pedestal 1 is fixedly connected, and the internal whorl of top bottle neck 18 is connected with top bottle stopper 21, and the inside of top bottle stopper 21 is fixedly connected There are shaft 22, the left side at 21 top of top bottle stopper to be fixedly connected with micromotor 23, the output shaft of micromotor 23 is fixedly connected There is driving gear 24, the inner rotation of shaft 22 is connected with mobile jib 25, and the bottom end of mobile jib 25 extends into the inside of reaction kettle 13, The bottom end of mobile jib 25 is fixedly connected with agitating paddle 26, and the shape of agitating paddle 26 is in elliposoidal, setting agitating paddle 26, micromotor 23, acid inlet tube 20 can effectively be such that experimenter is slowly stirred while slow acid adding, effectively make reaction rapid heat dissipation, keep away The danger for exempting from fried kettle, improves experiment safety, and the top of mobile jib 25 is fixedly connected with driven gear 27, and driving gear 24 with Driven gear 27 engages, and the one end of the acid inlet tube far from reaction kettle 13 is fixedly connected with the outlet of acid storage tank 28, acid storage tank 28 Right side be fixedly connected with supporting rod, the bottom end of supporting rod is fixedly connected with pedestal, by be arranged windowpane 12, experimenter can To observe and record reaction process constantly, accident can be found and handled in time, to effectively raise the safety of experiment Property.

When in use, user's pull-up buckle makes the bottom of buckle be detached from card slot, then raises lid 6, unscrews top Bottle stopper 21 is slowly added to the object for needing acid molten the bottom of reaction kettle 13, then makes top bottle stopper 21 and top bottle neck 18 are threadedly coupled, and tail gas absorption liquid are added in the inside of vent gas treatment bottle 11, and make offgas duct 16 far from one end of reaction kettle 13 It is inserted under the liquid level of tail gas absorption liquid, opens micromotor 23, the output shaft of micromotor 23 is made to drive driving gear 24, it is main Moving gear 24 is engaged with driven gear 27, is driven propeller 26 to rotate to drive mobile jib 25 to rotate mobile jib 25, is closed the lid 6, The bottom and card slot for making buckle are clamped, then open the outlet of acid storage tank 28, make being flowed to along the inner wall of reaction kettle 13 for slow acid The bottom of reaction kettle 13, acid will react with the molten object of acid is needed while agitating paddle 26 stirs, and experimenter can be with Reaction process is observed and recorded by windowpane 12, can find and handle accident in time, to effectively raise experiment Safety.

In conclusion this is used for the acid dissolution reaction device of making in laboratory Coating Materials, can have by the way that protective shell 2 is arranged The isolation experiment person of effect makes experimenter then pass through to improve experiment safety from testing the harm brought with environment Support plate 8, through-hole 9 and splicing groove 10 are set, the secondary destruction that fried kettle is brought is can effectively prevent, to improve experiment peace Quan Xing, then by the way that vent gas treatment bottle 11, offgas duct 16 and exhaust pipe is arranged, can effectively absorb and emission, effectively Experimenter and environment are protected, to improve experiment safety, then by the way that agitating paddle 26, micromotor 23, acid inlet tube is arranged 20, it so that experimenter is slowly stirred while slow acid adding, effectively make reaction rapid heat dissipation, avoid the danger of fried kettle Danger, improves experiment safety, and finally by setting windowpane 12, experimenter can observe and record reaction process constantly, can be with Accident is found and handles in time, to effectively raise the safety of experiment.

It should be noted that the terms "include", "comprise" or its any other variant are intended to the packet of nonexcludability Contain, so that the process, method, article or equipment including a series of elements includes not only those elements, but also includes Other elements that are not explicitly listed, or further include for elements inherent to such a process, method, article, or device. In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that including the element Process, method, article or equipment in there is also other identical elements.

While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art, It is appreciated that can these embodiments be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaiied Change, replace and modification, the scope of the utility model are defined by the appended claims and the equivalents thereof.

Claims

1. a kind of acid dissolution reaction device for making in laboratory Coating Materials, including pedestal (1), it is characterised in that：The bottom The bottom of seat (1) is fixedly connected with protective shell (2), and the right side opening of protective shell (2) bottom is equipped with bayonet (3), the bayonet (3) inside is fixedly connected with sprue (4), and gasket (5), the protective shell are fixedly connected at the top of the protective shell (2) (2) hinged seat that passes on left at the top of is hinged with lid (6), and the inner wall of the protective shell (2) offers annular groove (7), described The inside of annular groove (7) is connected with support plate (8), and the upper surface of the support plate (8) offers through-hole (9), the protective shell (2) inner bottom wall is provided with splicing groove (10), and the left side at the top of the support plate (8) is provided with vent gas treatment bottle (11), described The outer right wall of protective shell (2) and observation panel is offered at the top of the support plate (8), the inside of observation panel is fixedly connected with glass Glass window (12), the top of the support plate (8) and is provided with reaction kettle (13) on the right side of the vent gas treatment bottle (11), described anti- It answers and offers left bottle neck (14) on the left of kettle (13) outer wall, the internal whorl of the left bottle neck (14) is connected with left plug (15), institute The left side for stating left plug (15) offers left through-hole, and the inside of left through-hole is fixedly connected with offgas duct (16), and offgas duct (16) The inside of reaction kettle (13) is extended to, the one end of the offgas duct (16) far from reaction kettle (13) passes through vent gas treatment bottle (11) The right side opening of bottleneck and the inside for extending to vent gas treatment bottle (11), reaction kettle (13) outer wall is equipped with right bottle neck (17), institute It states and offers top bottle neck (18) at the top of reaction kettle (13), the internal whorl of the right bottle neck (17) is connected with right plug (19), The right side of the right plug (19) offers right through-hole, and the inside of right through-hole is fixedly connected with acid inlet tube (20), the acid inlet tube (20) left end extends to the inside of reaction kettle (13), and the internal whorl of the top bottle neck (18) is connected with top bottle stopper (21), the inside of the top bottle stopper (21) is fixedly connected with shaft (22), and the left side at the top of the top bottle stopper (21) is fixed It is connected with micromotor (23), the output shaft of the micromotor (23) is fixedly connected with driving gear (24), the shaft (22) inner rotation is connected with mobile jib (25), and the bottom end of mobile jib (25) extends into the inside of reaction kettle (13), the mobile jib (25) bottom end is fixedly connected with agitating paddle (26), and the top of the mobile jib (25) is fixedly connected with driven gear (27), and main Moving gear (24) is engaged with driven gear (27), the one end of the acid inlet tube (20) far from reaction kettle (13) and acid storage tank (28) Outlet is fixedly connected, and the right side of acid storage tank (28) is fixedly connected with supporting rod, bottom end and the fixed company of pedestal (1) of supporting rod It connects.

2. a kind of acid dissolution reaction device for making in laboratory Coating Materials according to claim 1, it is characterised in that： It is hinged with buckle on the right side of the lid (6), the outer wall on the right side of the protective shell (2) and opens up at the top of the windowpane (12) There are card slot, and the bottom end buckled and card slot clamping.

3. a kind of acid dissolution reaction device for making in laboratory Coating Materials according to claim 1, it is characterised in that： Tail gas hole is offered on the left of protective shell (2) bottom, the inside in tail gas hole is fixedly connected with exhaust pipe.

4. a kind of acid dissolution reaction device for making in laboratory Coating Materials according to claim 1, it is characterised in that： The shape of the reaction kettle (13) is spherical in shape and bottom is in plane.

5. a kind of acid dissolution reaction device for making in laboratory Coating Materials according to claim 1, it is characterised in that： The level height of the acid inlet tube (20) from right to left gradually reduces.

6. a kind of acid dissolution reaction device for making in laboratory Coating Materials according to claim 1, it is characterised in that： The shape of the agitating paddle (26) is in elliposoidal.