CN204556366U - Intelligent environmental protection type electric heating counteract appearance - Google Patents

Intelligent environmental protection type electric heating counteract appearance Download PDF

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Publication number
CN204556366U
CN204556366U CN201520159283.4U CN201520159283U CN204556366U CN 204556366 U CN204556366 U CN 204556366U CN 201520159283 U CN201520159283 U CN 201520159283U CN 204556366 U CN204556366 U CN 204556366U
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bottle
clear
waste gas
environmental protection
type electric
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CN201520159283.4U
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胡自胜
曲蓓
孙丽杰
邢红勋
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Abstract

Intelligent environmental protection type electric heating counteract appearance, comprise control panel, heating system, heating plate, clear up a bottle fixing spring, clear up bottle, acid gas sealing reflux, support, recovery waste gas solution used, returnable bottle, returnable bottle pallet, switch; Described switch is connected with control panel, control panel is connected with heating system, heating system is connected with heating plate, heating plate with clear up a bottle fixing spring, clear up bottle and be connected, clear up bottle to seal reflux with acid gas and be connected, acid gas sealing reflux is connected with returnable bottle, and returnable bottle is connected with returnable bottle pallet, and acid gas sealing reflux is connected with support.The utility model adopts temperature programme, steam backflow, waste gas recovery.Make digestion process intelligence, saving, environmental protection.Clear up the direct constant volume of bottle, save the trouble of transfer.

Description

Intelligent environmental protection type electric heating counteract appearance
Technical field
The utility model relates to the digestion instrument of sample pre-treatments in a kind of laboratory sample analytic process, is exactly specifically a kind of intelligent environmental protection type electric heating counteract appearance.
Background technology
Sample when intelligent environmental protection type electric heating counteract appearance is widely used in unit laboratory, the lab analysis samples such as food security, pharmaceutical production, environmental protection, ore soil, Disease epizootic, quality supervision, commodity inspection, scientific research institutions, institution of higher learning is cleared up early stage.1, traditional Specimen eliminating mode is generally that electrical heating is cleared up or micro-wave digestion; Electrical heating oxidation rate is very slow and want Attended mode, and with a large amount of such as acid solution such as nitric acid, hydrochloric acid, but the acid of really clearing up consumptive use is little, and major part acid is all because high-temperature heating has vapored away with the form of acid gas; And acid gas is healthy very harmful to laboratory personnel; Micro-wave digestion is few with acid, and digestion time is also short, but counteracting tank cleaning is pretty troublesome, transfers to volumetric flask very bothersome, and easily cause sample transfer indfficiency or transfer the pollution from counteracting tank; Must acid be caught up with in addition, also must Attended mode when catching up with acid! It is how many that so overall digestion time clears up province unlike electrical heating.2, traditional Specimen eliminating requirement must in fuming cupboard, and the mouth mask that mouth band has gas defence character could available protecting analytical test worker not injured by toxic and harmful.3, it is constant temperature digestion that traditional electrical heating is cleared up, and clears up effect undesirable; Micro-wave digestion can temperature programme, but temperature, pressure has particular/special requirement, otherwise has explosion danger.4, traditional micro-wave digestion offsets solution sample size strict control, and offseting solution sample kind has requirement, otherwise has explosion danger.
Utility model content
The technical matters that the utility model solves is to provide intelligent environmental protection type electric heating digestion instrument, to solve the problem proposed in above-mentioned technical background.
The technical matters that the utility model solves realizes by the following technical solutions:
The intelligent environmental protection type electric heating counteract appearance in laboratory has: control panel, heating system, heating plate, clear up a bottle fixing spring, clear up bottle, acid gas sealing reflux, support, recovery waste gas solution used, reclaim surge flask, reclaim the compositions such as waste gas bottle, returnable bottle pallet; Described control panel, heating system, in instrument internal, are cleared up bottle fixing spring portion on hot plate, are connected with heating plate.Support with clear up a bottle stationary installation and be connected, clearing up bottle puts on hot plate, middle part is fixed with clearing up a bottle fixing spring, bottleneck is connected with sealing reflux, reflux is connected with pipeline one end, the pipeline other end with recovery surge flask, reclaims waste gas bottle and is connected, reclaim surge flask, reclaim in waste gas bottle to have and reclaim waste gas solution used, recovery surge flask, recovery waste gas bottle are placed on pallet; Wherein heating system connects with control panel.
Further, described control system sets clears up program, will clear up bottle and be fixed on and clear up in bottle fixing spring;
Further, described acid gas sealing reflux is placed on and clears up in bottleneck;
Further, termination exhaust gas recycling tube road on described acid gas sealing reflux, enters and reclaims surge flask, reclaims in waste gas bottle;
Further, recovery waste gas liquid is put in described recovery surge flask, recovery waste gas bottle;
Further, described recovery surge flask, recovery waste gas bottle are placed on pallet.
Intelligent environmental protection type electric heating counteract appearance adds acid solution heat clearing up in bottle sample and institute, clear up beginning, overheated acid gas is got back to clear up in bottle by reflux and is continued to clear up sample, after heating, overheated acid gas rises again arrival reflux, circulation like this reaches province's acid object, the overheated acid gas of complete cooling for reflux is not had in reflux, arrived by waste gas recovery pipeline and reclaim surge flask, reclaim in waste gas bottle, withdrawal liquid in recovery surge flask, recovery waste gas bottle and acid gas effect become harmless liquid, and acid gas is all reclaimed.Temperature programme setting is cleared up program and just sample is cleared up completely, and remaining acid amount is few, reaches and need not catch up with sour object; Usedly clear up the volumetric flask that bottle is a special material, cleared up and to be cooled to after room temperature directly constant volume, reached the object without the direct constant volume of transfer.
beneficial effect
The utility model adopts totally-enclosed pattern to clear up, and the toxic harmful exhaust gas produced in digestion process is reclaimed entirely; Creativeness has invented reflux, the problem that when not only effectively solving Specimen eliminating, reagent consumption is large, also solve reagent recycling problem, save using amount of reagent greatly, and mode, thoroughly solve the problem that the acid gas because clearing up generation injures laboratory personnel; What the use of temperature programme reached sample had cleared up not only thoroughly but also fast object, solved digestion process or caught up with acid must the problem of Attended mode.The use of volumetric flask special material, changing volumetric flask can not heat, and can not clear up the history of sample, has very large initiative, eliminates the history cleared up sample and must shift.The use of waste gas recovering device changes clears up and must have ventilation, and the traditional type that acid gas will take precautions against injury laboratory personnel clears up understanding, really accomplishes that environmental protection is cleared up, no pollution discharge is cleared up.
Accompanying drawing explanation
Fig. 1 is fundamental diagram of the present utility model;
Fig. 2 is structural representation of the present utility model;
Fig. 3 is the vertical view of Fig. 2.
Embodiment
In order to make actualizing technology means of the present utility model, creation characteristic, object and effect easy to understand, below in conjunction with concrete diagram, set forth the utility model further.
As Figure 1-3, intelligent environmental protection type electric heating counteract appearance, comprises control panel 1, heating system 2, heating plate 3, clears up bottle fixing spring 4, clears up bottle 5, acid gas sealing reflux 6, support 7, reclaims surge flask 8, reclaims waste gas bottle 9, reclaims waste gas solution 10 used, returnable bottle pallet 11, switch 12.
Described control panel 1 and the left end of switch 12 at foot.Switch 12 controls the energising of whole counteract appearance.Control panel 1 controls heating system 2.
Further, control panel 1 top is heating system 2, and heating system 2 top is heating plate 3.Heating system 2, control panel 1, switch 12, heating plate 3 are heating setpoint, the control section of whole counteract appearance.
Further, clear up bottle fixing spring 4 and clear up the top of bottle 5 at heating plate 3, it is responsible for fixedly clearing up bottle 5.
Further, clear up on bottle 5 and place acid gas sealing reflux 6, in order to realize the backflow of Hydrolytic acid steam, and will clear up the waste gas of generation, the waste gas such as uncondensable oxides of nitrogen are discharged into and reclaim in surge flask 8.Acid gas sealing reflux 6 is fixed by support 7.
Further, waste gas enters to reclaim waste gas bottle 9 and reclaim waste gas liquid 10 through recovery surge flask 8 and reacts, and is processed.Expendable oxygen, nitrogen are then put in air by tubes rows.
Further, reclaim waste gas liquid 10 and be contained in recovery surge flask 8 and reclaim in waste gas bottle 9, and be placed in returnable bottle pallet.
More than show and describe ultimate principle of the present utility model, principal character and advantage of the present utility model.The technician of the industry should understand; the utility model is not restricted to the described embodiments; what describe in above-described embodiment and instructions just illustrates principle of the present utility model; under the prerequisite not departing from the utility model spirit and scope; the utility model also has various changes and modifications, and these changes and improvements are all included within the scope of claimed the utility model.Claimed scope of the present utility model is defined by appending claims and equivalent thereof.

Claims (3)

1. intelligent environmental protection type electric heating counteract appearance, comprise control panel (1), heating system (2), heating plate (3), clear up a bottle fixing spring (4), clear up bottle (5), acid gas sealing reflux (6), support (7), reclaim surge flask (8), reclaim waste gas bottle (9), reclaim waste gas solution used (10), returnable bottle pallet (11), switch (12), it is characterized in that, described intelligent environmental protection type electric heating counteract appearance bottom is switch (12), control panel (1), control panel (1) top is heating system (2), heating system (2) top is heating plate (3), clear up bottle (5) to fix by clearing up a bottle fixing spring (4), be placed in heating plate (3) top, clear up bottle (5) and seal reflux (6) sealing by acid gas, waste gas is through reclaiming surge flask (8), emptying after reclaiming recovery waste gas liquid (10) process in waste gas bottle (9), described acid gas sealing reflux (6) is fixed by support (7).
2. according to claim 1, intelligent environmental protection type electric heating counteract appearance, is characterized in that clearing up bottle is fixed by spring clamp, place, convenient to remove, clearing up bottle can not topple over.
3. according to claim 1, intelligent environmental protection type electric heating counteract appearance, is characterized in that clearing up bottle is volumetric flask, can heat, the constancy of volume after cooling, saves subsequent transfer trouble.
CN201520159283.4U 2015-03-20 2015-03-20 Intelligent environmental protection type electric heating counteract appearance Active CN204556366U (en)

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CN201520159283.4U CN204556366U (en) 2015-03-20 2015-03-20 Intelligent environmental protection type electric heating counteract appearance

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105651587A (en) * 2016-02-26 2016-06-08 杨冠丽 Environment-friendly digestion reflux device
CN105973687A (en) * 2016-06-13 2016-09-28 山东思睿环境设备科技有限公司 High temperature and high pressure digestion system with quadruple safety protection
CN106596245A (en) * 2017-02-08 2017-04-26 朱山 Continuous liquid feeding type digestion instrument
CN109342173A (en) * 2018-12-13 2019-02-15 北京连华永兴科技发展有限公司 COD reflux resolution instrument
CN112539990A (en) * 2020-12-14 2021-03-23 浙江拓捷仪器设备有限公司 Environment-friendly full-automatic electric heating high-temperature high-pressure digestion instrument combination device
CN116609147A (en) * 2023-05-19 2023-08-18 中国科学技术大学 Low background digestion device for single-particle minerals and application method

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105651587A (en) * 2016-02-26 2016-06-08 杨冠丽 Environment-friendly digestion reflux device
CN105973687A (en) * 2016-06-13 2016-09-28 山东思睿环境设备科技有限公司 High temperature and high pressure digestion system with quadruple safety protection
CN106596245A (en) * 2017-02-08 2017-04-26 朱山 Continuous liquid feeding type digestion instrument
CN109342173A (en) * 2018-12-13 2019-02-15 北京连华永兴科技发展有限公司 COD reflux resolution instrument
CN112539990A (en) * 2020-12-14 2021-03-23 浙江拓捷仪器设备有限公司 Environment-friendly full-automatic electric heating high-temperature high-pressure digestion instrument combination device
CN116609147A (en) * 2023-05-19 2023-08-18 中国科学技术大学 Low background digestion device for single-particle minerals and application method
CN116609147B (en) * 2023-05-19 2024-03-12 中国科学技术大学 Low background digestion device for single-particle minerals and application method

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