CN207798712U - A kind of measured hole adjustable x-ray fluorescence analysis dress test sample - Google Patents

A kind of measured hole adjustable x-ray fluorescence analysis dress test sample Download PDF

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Publication number
CN207798712U
CN207798712U CN201721741660.0U CN201721741660U CN207798712U CN 207798712 U CN207798712 U CN 207798712U CN 201721741660 U CN201721741660 U CN 201721741660U CN 207798712 U CN207798712 U CN 207798712U
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China
Prior art keywords
measured hole
sample
peephole
hole
ray fluorescence
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CN201721741660.0U
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Inventor
李�杰
张穗忠
李洁
于录军
谢芬
夏念平
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Wuhan Iron and Steel Co Ltd
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Wuhan Iron and Steel Co Ltd
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Abstract

A kind of measured hole adjustable x-ray fluorescence analysis dress test sample, it is mainly made of, is the spring placed on the peephole one on sample holder, the end cap set on sample holder upper end, end cap, the spring backing plate in sample holder, spring backing plate, the sample backing plate placed on spring:It is connected with cyclic annular convex block in the lower face of end cap, is connected with measured hole adjuster in the lower end of cyclic annular convex block, measured hole adjuster is connected by screw thread and sample holder.The utility model is simple in structure, it is only necessary to which set of device reduces the quantity of the sample box needed to configure, to improve analysis efficiency, and makes to be parsed into reduction originally;It is suitable for different size of samples, the size of measured hole are adjusted by screwing end cap, it is ensured that measurement sensitivity.

Description

A kind of measured hole adjustable x-ray fluorescence analysis dress test sample
Technical field
The utility model is related to a kind of specimen test analysis devices, particularly belong to a kind of x-ray fluorescence analysis dress examination Sample device.
Background technology
X-ray fluorescence analysis is a kind of common rapid analysis method to sample chemical composition, with good steady Qualitative and precision, wider measurement range, higher sensitivity, can multielement quickly measure simultaneously, and almost to sample The features such as not causing loss, is widely used in each field such as metallurgy, mine, geology, metal material.In industrial and mining enterprises and scientific research Institutes is using very extensive.
During x-ray fluorescence analysis, the sample processed needs to be fixed to be contained in sample box, and exposes certain The flat surface of area is measured for analyzing.The X-ray that light source emits when measurement is irradiated to sample by the measured hole on lid Surface, excitation sample generate fluorescence spectrum, the chemical composition of sample are determined according to the wavelength of the fluorescent line of generation and intensity. The size that sample box covers measured hole determines the flux that can be irradiated to the X-ray on sample, to determine the sensitive of measurement Degree.Therefore with regard to present circumstances, those skilled in the art are to select larger measured hole as possible to obtain higher measurement Sensitivity.But the size of sample can limit the size of measured hole, and for various sizes of sample, people take at present It selects different sample boxs or replaces the sample box lid with different pore size, to ensure that sample can be by good fixation.This It must cause to need to prepare sample box or the sample box cover of a series of different models from big to small to adapt to various sizes of sample.One It is that laboratory's acquisition cost is caused to increase, second is that also needing to more placement space.
Utility model content
The utility model is in view of the deficienciess of the prior art, provide a kind of simple in structure, it is only necessary to which set of device can fit For different size of sample, the size of measured hole is adjusted by screwing end cap, to ensure the measurement of measurement sensitivity requirement The adjustable x-ray fluorescence analysis in hole dress test sample.
Realize the technical measures of above-mentioned purpose:
A kind of measured hole adjustable x-ray fluorescence analysis dress test sample, is mainly placed by sample holder, set on sample The end cap of box upper end, the peephole one on end cap, the spring backing plate in sample holder, spring, the bullet placed on spring backing plate The sample backing plate composition placed on spring, is:It is connected with cyclic annular convex block in the lower face of end cap, is connected in the lower end of cyclic annular convex block It is connected to measured hole adjuster, measured hole adjuster is connected by screw thread and sample holder.
It is:Card slot that the measured hole adjuster is equipped with by shell, cover top portion, the fixation of connection inside the shell The survey that plate, the connecting hole being equipped in fixed plate and peephole two, the arc shaped blade installed by connecting hole, arc shaped blade are formed The axis pin that is equipped in mounting hole and adjustment hole, mounting hole and the adjustment hole being arranged on metering-orifice, arc shaped blade, arc shaped blade upper surface Annular pressing plate, the annular pressing plate groove, regulating tank and the peephole three that are equipped with form.
It is:The ring-type convex block is located at the latch on the outside of annulus, peephole four and is coordinated with groove convex by annulus Item forms;The lower face of annular pressing plate and raised line is in same plane installation;Latch is matched with card slot.
It is:The arc shaped blade is at least 3;Mounting hole and adjustment hole are arranged at the big end of arc shaped blade.
It is:Peephole one, peephole two, peephole three, peephole four and measured hole are laid out for concentric circles.
The characteristics of the utility model:It is simple in structure, it is only necessary to set of device reduces the quantity of the sample box needed to configure, To improve analysis efficiency, and make to be parsed into reduction originally;It is suitable for different size of samples, and survey is adjusted by screwing end cap The size of metering-orifice, it is ensured that measurement sensitivity.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is the structural schematic diagram of measured hole adjuster in Fig. 1;
Fig. 3 is end cap structural schematic diagram in Fig. 1;
Fig. 4 is the present invention looks up structural representation of end cap in Fig. 3;
Fig. 5 is the structural schematic diagram of shell and fixed plate in Fig. 2;
Fig. 6 is the structural schematic diagram of annular pressing plate in Fig. 2;
Fig. 7 is the schematic shapes after the installation of Fig. 2 arc shaped blades;
In figure:1-sample holder, 2-end caps, 3-peepholes, 4-spring backing plates, 5-springs, 6-sample backing plates, 7-measured hole adjusters, 8-cyclic annular convex blocks, 9-shells, 10-card slots, 11-fixed plates, 12-connecting holes, 13-arc-shaped leafs Piece, 14-peepholes two, 15-measured holes, 16-mounting holes, 17-adjustment holes, 18-axis pins, 19-annular pressing plates, 20-is recessed Slot, 21-regulating tanks, 22-peepholes three, 23-annulus, 24-latches, 25-peepholes four, 26-raised lines.
Specific implementation mode
It is described further below in conjunction with the accompanying drawings:
A kind of measured hole adjustable x-ray fluorescence analysis dress test sample, mainly puts by sample holder 1, set on sample It sets the end cap 2 of 4 upper end of box, the peephole 1 on end cap 2, the spring backing plate 4 in sample holder 1, placed on spring backing plate 4 Spring 5, the sample backing plate 6 placed on spring 5 form, have cyclic annular convex block 8 in the lower face overall processing of end cap 2, in ring The lower end of shape convex block 8 is connected with measured hole adjuster 7, and measured hole adjuster 7 is connected by screw thread and sample holder 1.
The measured hole adjuster 7 is interior using whole or welding by card slot 10, the shell 9 that shell 9,9 top of shell process The fixed plate 11 of connection, the connecting hole 12 and peephole 2 14 processed in fixed plate 11 are connected by the bolt in connecting hole 12 The mounting hole 16 and adjustment hole 17 processed on measured hole 15 that the arc shaped blade 13 that connects, arc shaped blade 13 are formed, arc shaped blade 13, On the annular pressing plate 19 of the axis pin 18,13 upper surface of arc shaped blade that are equipped in mounting hole 16 and adjustment hole 17, annular pressing plate 19 plus Groove 20, regulating tank 21 and the peephole 3 22 of work form.
The ring-type convex block 8 is matched by annulus 23 in the latch 24 of 23 outside processing of annulus, peephole 4 25 and with groove 20 The raised line 26 of conjunction forms;The lower face of annular pressing plate 19 and raised line 26 is in same plane installation;Latch 24 matches with card slot 10 It closes.
The arc shaped blade 13 is at least 3;Mounting hole 16 and adjustment hole 17 are arranged at the big end of arc shaped blade 13.
Peephole 1, peephole 2 14, peephole 3 22, peephole 4 25 and measured hole 15 are laid out for concentric circles.
Practical principle
When measuring sample, sample is placed on sample backing plate 6, then rotating end cap 2, under the drive of end cap 2, annular Pressing plate 19 rotates with, and then the axis pin 18 in the adjustment hole 17 of arc shaped blade 13 is driven to be moved in regulating tank 21, makes simultaneously It obtains axis pin 18 of the arc shaped blade 13 in mounting hole 16 to rotate, until the measured hole 15 that arc shaped blade 13 is formed is made to be less than sample Until diameter is no more than 3mm, to make sample be consolidated;Measured hole adjuster 7 is twisted by screw thread and sample holder 1 again Tightly, it is measured at this point, can be put into Xray fluorescence spectrometer.
Present embodiment is only the best example, not to the restricted implementation of technical solutions of the utility model.

Claims (5)

1. a kind of measured hole adjustable x-ray fluorescence analysis dress test sample, mainly by sample holder, set on sample holder The end cap of upper end, the peephole one on end cap, the spring backing plate in sample holder, spring, the spring placed on spring backing plate The sample backing plate of upper placement forms, it is characterised in that:It is connected with cyclic annular convex block in the lower face of end cap, in the lower end of cyclic annular convex block It is connected with measured hole adjuster, measured hole adjuster is connected by screw thread and sample holder.
2. a kind of measured hole adjustable x-ray fluorescence analysis dress test sample as described in claim 1, it is characterised in that:Institute It states card slot, connection that measured hole adjuster is equipped with by shell, cover top portion fixed plate inside the shell, be equipped in fixed plate It is arranged on measured hole that connecting hole and peephole two, the arc shaped blade installed by connecting hole, arc shaped blade are formed, arc shaped blade Mounting hole and adjustment hole, mounting hole and adjustment hole in be equipped with axis pin, arc shaped blade upper surface annular pressing plate, annular pressing plate Groove, regulating tank and the peephole three being equipped with form.
3. a kind of measured hole adjustable x-ray fluorescence analysis dress test sample as claimed in claim 1 or 2, it is characterised in that: The ring-type convex block is located at the latch on the outside of annulus, peephole four and the raised line composition coordinated with groove by annulus;Annular pressing plate It is in same plane installation with the lower face of raised line;Latch is matched with card slot.
4. a kind of measured hole adjustable x-ray fluorescence analysis dress test sample as claimed in claim 2, it is characterised in that:Institute It states arc shaped blade and is at least 3;Mounting hole and adjustment hole are arranged at the big end of arc shaped blade.
5. a kind of measured hole adjustable x-ray fluorescence analysis dress test sample as claimed in claim 1 or 2, it is characterised in that: Peephole one, peephole two, peephole three, peephole four and measured hole are laid out for concentric circles.
CN201721741660.0U 2017-12-14 2017-12-14 A kind of measured hole adjustable x-ray fluorescence analysis dress test sample Active CN207798712U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721741660.0U CN207798712U (en) 2017-12-14 2017-12-14 A kind of measured hole adjustable x-ray fluorescence analysis dress test sample

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721741660.0U CN207798712U (en) 2017-12-14 2017-12-14 A kind of measured hole adjustable x-ray fluorescence analysis dress test sample

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CN207798712U true CN207798712U (en) 2018-08-31

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110208197A (en) * 2019-06-30 2019-09-06 江苏省沙钢钢铁研究院有限公司 The clamping device and method for making sample of small size and irregular sample

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110208197A (en) * 2019-06-30 2019-09-06 江苏省沙钢钢铁研究院有限公司 The clamping device and method for making sample of small size and irregular sample
CN110208197B (en) * 2019-06-30 2021-08-10 江苏省沙钢钢铁研究院有限公司 Sample preparation method for small-size and irregular samples

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